Browse Topic: Alloys
Additive manufacturing (AM) processes facilitate the production of components with high geometrical complexity, presenting substantial opportunities for innovation in demanding sectors such as aerospace and biomedical engineering. A significant challenge impeding their broader application is the characteristic surface roughness of as-fabricated parts, which results from the layer-wise construction and the presence of partially melted powder particles. While electrochemical polishing (EP) represents a viable post-processing technique for achieving a smooth surface finish, a comprehensive understanding of how the non-equilibrium microstructures characteristic of AM materials interact with the EP process remains incomplete. This investigation centers on the electrochemical polishing behavior of Ti-6Al-4V alloy fabricated by direct energy deposition (DED), utilizing a sodium chloride-ethylene glycol electrolyte. The findings reveal that the material's distinct engenders anisotropic anodic dissolution. This behavior is attributed to the differential electrochemical potentials among the constituent phases and their crystallographic orientations, which consequently narrows the operational process window for effective, uniform polishing. This preferential dissolution of certain phases results in the formation of a subtle, micro-scale topographical variation that mirrors the orientation of the original columnar grain structure. Notwithstanding this microstructural influence, the EP treatment proved highly successful in refining the surface finish, substantially decreasing the average surface roughness from 0.350 μm to 0.042 μm. Concurrently, the treatment led to a significant enhancement in the alloy's corrosion resistance, attributed to an oxide layer. These findings underscore the critical necessity of accounting for microstructural characteristics when developing optimized electrochemical polishing protocols for additively manufactured components.
To facilitate the development and application of bulb-flat titanium alloys in aerospace and automotive industries, this study selects TC4 as the research material and employs finite element simulation software to simulate the hot rolling process of TC4 bulb flat titanium. The temperature field, strain field, and metal flow velocity in each rolling pass are analyzed, and rolling experiments are conducted after optimizing the roll pass system. The results indicate that during the rolling process of TC4 bulb flat titanium, the head undergoes relatively smaller deformation, resulting in a slower temperature decrease, whereas the waist experiences greater deformation and a faster temperature drop. A significant temperature difference exists between the core and surface, which can be mitigated by appropriately increasing the roll temperature to reduce heat transfer. Prior to the K4 pass, the billet temperature drops to a level that may affect rolling performance, necessitating furnace reheating. Strain increases progressively with each rolling pass, with higher values observed at the waist compared to the head. A gradual strain transition occurs at the interface between the head and waist. Furthermore, the irregular design of the roll pass leads to a considerable difference in metal flow velocity between the upper and lower surfaces. During the K1 pass rolling, this imbalance can cause the guide guard to be displaced upward and result in roll wrapping. Without altering the roll diameter, shifting the entire roll pass system toward the side with higher metal flow velocity effectively reduces the linear velocity and prevents these issues, ensuring stable billet rolling. Rolling experiments successfully produced the final TC4 bulb flat titanium, thereby validating the feasibility of the optimized roll pass system and the rationality of the selected rolling parameters. It provides the possibility for its development and application in fields such as aircraft and automobiles.
Blended metal powders offer a compelling alternative to pre-alloyed powders in metal additive manufacturing by providing access to a wider range of alloy compositions and avoiding the high costs in producing pre-alloyed powders. In this work, a new and crack-free Ti-5AlMnScZrMgSiFe alloy (in wt.%) was manufactured by laser powder bed fusion (L-PBF) from mixed powders to investigate the microstructures, mechanical performance of printed parts. Ti-5 AlMnScZrMgSiFe alloy contains both alpha (α) and alpha prime (α′) phases. Further microstructural characterizations show that the L-PBF Ti-5 AlMnScZrMgSiFe contain dense dislocations and twins formed in additive manufacturing process. The as-printed Ti-5 AlMnScZrMgSiFe alloy exhibits a tensile fracture strength of ~950 MPa with a fracture elongation of ~12.5%. The eye-catching properties are attributed to the dense dislocations, nano-twins and solid-solution strengthening.
Cu-Fe alloys exhibit excellent performance, and increasing Fe content reduces costs. However, high-Fe Cu-Fe alloys exhibit limited formability at room temperature, while warm rolling improves their processability. This research investigates the effect of rolling temperature on the microstructural transformations and texture development in the Cu-10Fe alloys. The experimental result is that during cold rolling, the morphology of Fe phases is mainly fibrous. With the rolling temperature rising, the microstructural morphology of Fe phases becomes globular / elliptical. The difference is that with the increase in rolling temperature, the average grain size of the Cu-10Fe alloy first decreases and then increases. The matrix microstructure remains dominated by deformed grains, with significant recovery observed at 500 °C. The Fe-phase microstructure primarily consists of substructured grains, and dynamic recovery intensifies with rising temperature. During cold rolling, high dislocation density and localized strain heterogeneity lead to dispersed texture orientations and low strength. In contrast, warm rolling promotes dislocation climb and dynamic recovery, triggering partial recrystallization. This reduces randomly oriented grains, enhances the strength and continuity of specific textures, and establishes a more concentrated texture distribution. This forms a structure with fine recrystallized grains embedded within deformed grains, exhibiting slightly lower strength than cold-rolled samples but better elongation. These findings reveal the crucial role of deformation temperature in controlling microstructure transformation and texture evolution, especially by regulating the recovery and recrystallization behaviors of Cu-10Fe alloys. The above results hope to provide some theoretical and experimental basis for a new approach to improve processing technologies for new Cu-Fe-based composites.
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