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Browse AllThere are three main methods for preparing chlorinated polyethylene: the solution method, suspension method, and solid-phase method. This article studies the process of preparing chlorinated polyethylene by the aqueous suspension method, introduces the production process of chlorinated polyethylene, first understands the reaction mechanism of the chlorination reaction, then explores the production process of chlorinated polyethylene by the suspension method, and finds the optimal process conditions through experiments. The results showed that the optimal reaction temperature for the chlorination reaction of chlorinated polyethylene was 135°C, the optimal amount of initiator was 3%, and the optimal amount of chlorine gas added was 1.5%/min. This article explores the influencing factors of the optimal reaction conditions, laying a theoretical foundation for industrial production after the suspension method.
Steady advancement is observed in global research on eco-friendly and sustainable transportation. Rapid technological evolution of hybrid electric vehicles (HEVs) is documented. Lower overall noise output and more compact structures are achieved in HEV engines relative to conventional internal combustion engines. The perceptibility of harmonic impulsive sounds is significantly enhanced by these design characteristics. A close correlation is observed between these acoustic phenomena and negative human auditory perceptions. These events are treated as a core focus for HEV noise, vibration, and harshness optimization. Accurate quantification of harmonic impulsive sounds is not achieved by conventional objective indicators. A favorable balance between reliability and accuracy is not established by existing subjective prediction models. Practical engineering applications of these methods are severely restricted. A novel objective quantification method for harmonic impulsive sounds is proposed in this study. The method is established based on time–frequency masking theory and tonal strength. Bench tests in a semi-anechoic chamber and subjective evaluation experiments with standardized rating scales are performed for data collection. Collected sound signals are decomposed through an integrated approach of wavelet transform and variational mode decomposition. Targeted feature extraction is completed for harmonic impulsive sounds. A quantitative index incorporating human auditory temporal and frequency masking effects is developed. The proposed index exhibits a significantly stronger correlation with subjective evaluation results than traditional objective metrics, confirming its superior ability to reflect actual perceived sound quality. An interval prediction model for sound quality evaluation is established based on support vector machines and kernel density estimation. Traditional objective metrics and the proposed index are introduced as key input parameters. Effective and reliable prediction of HEV engine noise subjective satisfaction is achieved by the model.
The scheme of photocatalysis of water, a way of hydrogen generation as a clean, high-efficiency fuel source for aircraft and long-range transport systems has received considerable interest. The development of the covalent organic framework (COF) - derived materials for hydrogen evolution reaction (HER) has since become a research highlight. Compared to traditional methods, photocatalytic hydrogen evolution systems based on COFs can provide ways of generating hydrogen gas without depending upon noble metal catalysts, thereby enhancing the sustainability and prospects of this technology for future aerospace energy applications.In this work, two covalent organic frameworks (COFs) with distinct linkages—a vinylene-linked COF A (via Knoevenagel condensation) and an imine-linked COF B (via Schiff-base reaction)—were designed and synthesized to compare their performance in the photocatalystic hydrogen evolution reaction (HER). Structural and electrochemical characterizations confirmed that, despite lower crystallinity and specific surface area due to pore blockage, COF A exhibited a suitable band structure for photocatalysis and achieved an HER rate of 56 μmol h^–1 g^–1 under simulated sunlight. In contrast, COF B was ineffective. This study experimentally validates the superior photocatalytic potential of vinylene-linked COFs over imine-linked counterparts for HER, highlighting their potential as non-noble-metal catalysts for aerospace and transport-oriented fuel generation.
Ultrasonic TOFD detection is one of the most important non-destructive testing techniques for welds. However, the complex beam deflection, scattering, and attenuation of ultrasonic waves in the heterogeneous weld structure lead to the weak signal of the defect diffraction wave received by the probe and the low signal-to-noise ratio, which has a negative impact on the engineering application of ultrasonic TOFD detection technology in austenitic stainless steel welds. In this study, a numerical model of the ultrasonic TOFD detection process for austenitic stainless steel welds was established based on the finite element method. Combined with the test method, the interaction mechanism between the ultrasonic wave and weld structure is analyzed, and the probe arrangement method to reduce the interference of weld scattering noise is proposed. The results show that the finite element model can simulate the anisotropic characteristics of ultrasonic waves in austenitic stainless steel welds, including sound field distortion, sound energy scattering, and attenuation. Combined with the detection test, it has been proven that the adverse effect of the weld structure on the TOFD detection signal can be reduced by changing the probe detection surface.