Browse Topic: Materials properties
This research demonstrates a facile method for fabricating an anti-icing coating through spray deposition on a metallic substrate. A dual-layer structure was designed to enhance icephobic properties: a primer layer incorporating fluorocarbon resin, butyl acetate, and rod-shaped micrometer-sized metal oxides to establish a secondary roughness morphology, followed by a topcoat composed of butyl acetate and nano-scaled superhydrophobic particles. Evaluation of the coating performance revealed a maximum water contact angle of 171.9°, indicating exceptional hydrophobicity. Furthermore, the coating exhibited notable abrasion resistance and anti-icing capabilities against overlaying ice.
This paper examines the temperature distribution during pipe cutting and the impact of the heat-affected zone on the mechanical microstructure and properties of steel pipes. Utilizing testing equipment such as K-type thermocouples, a MESTL-WELD thermocouple spot welding machine, and a DC5516H 16-channel temperature data logger, temperature tests were conducted on Φ 1016 × 17.5 mm X70M spiral seam submerged arc welded steel pipes and Φ 1016 × 21 mm X70M straight-seam submerged arc welded steel pipes. The results indicate that the maximum test temperatures during cutting were 953.8 °C and 1216.6 °C, respectively, with the duration of temperatures exceeding 400 °C at each test point not exceeding 30 seconds. By fitting the relationship curve between the peak temperatures of each test point and the cutting distance using the ExpDec3 model, it was found that the cutting distance corresponding to a temperature of 580 °C was 12 mm. Furthermore, mechanical microstructure and property tests were performed on the pipe body at different positions of the HAZ. Except for an anomaly in the yield strength of the rod-shaped tensile specimens of the Φ 1016 × 21 mm X70M welded pipe body, no other abnormalities were detected. Macroscopic metallographic examination revealed that the axial length of the HAZ at the end of the cut pipe did not exceed 7 mm. Microhardness testing showed significant fluctuations in the microhardness of the pipe body at the end of the cut pipe, while the microhardness of the pipe body beyond 10 mm from the end gradually returned to normal.
Blended metal powders offer a compelling alternative to pre-alloyed powders in metal additive manufacturing by providing access to a wider range of alloy compositions and avoiding the high costs in producing pre-alloyed powders. In this work, a new and crack-free Ti-5AlMnScZrMgSiFe alloy (in wt.%) was manufactured by laser powder bed fusion (L-PBF) from mixed powders to investigate the microstructures, mechanical performance of printed parts. Ti-5 AlMnScZrMgSiFe alloy contains both alpha (α) and alpha prime (α′) phases. Further microstructural characterizations show that the L-PBF Ti-5 AlMnScZrMgSiFe contain dense dislocations and twins formed in additive manufacturing process. The as-printed Ti-5 AlMnScZrMgSiFe alloy exhibits a tensile fracture strength of ~950 MPa with a fracture elongation of ~12.5%. The eye-catching properties are attributed to the dense dislocations, nano-twins and solid-solution strengthening.
This study carefully designed and successfully developed a mechanical voltage stabilizing control device. The device uses silicone oil as the key component material of the liquid spring and 1Cr13 as the main material of the pressure control unit, enhancing its high-pressure resistance (up to 35 MPa), oxidation resistance, and acid-alkali corrosion resistance. By optimizing the transmission mechanism and simplifying the pressure regulation module, the device achieves a pressure regulation range of 0.1–21 MPa with an accuracy of ±0.01 MPa, significantly broader and more precise than traditional devices. To address manufacturing challenges, advanced CNC machine tools, ceramic cutting tools, and optimized heat treatment processes (e.g., quenching and tempering) were adopted, ensuring component machining accuracy within ±0.02 mm. Field applications in 13 oil wells demonstrated a 15.6% increase in daily oil production (from 25.5 t/d to 29.5 t/d) and a 17.9% increase in daily gas production (from 2800 m^3/d to 3300 m^3/d), with stable casing pressure control at 5.3 MPa. The device has created 1.225 million yuan in economic benefits while eliminating safety hazards, providing critical technical support for efficient and environmentally friendly oil and gas production.
SiC-based power devices are favored for high-voltage and high-power applications due to their superior material properties. However, the demand for higher breakdown voltages and improved channel mobility presents significant challenges to the etching process, especially the micro-trenching effect. In this study, etching results from inductively coupled plasma (ICP) have been presents, which focused on using various SF6/O2/Ar gas ratios to eliminate micro-trenching effect. The profile analysis of micro-trench was taken by cross-sectional scanning electron microscopy (SEM). The results demonstrate that micro-trenches primarily originate from the coupling effect between ion multi-reflection from sidewalls and redeposition of etch byproducts. Based on this mechanism, we propose a quasi-Bosch process: a combined polymerization and etching step in oxygen-fluorine-rich plasma deposits polymer on exposed SiC and the mask, while removing it from the structure bottom via ion bombardment to enable etching and passivation; then alternates with a short fluorine-plasma step, which consumes sidewall polymer through ion incidence and prevents SiFxOy charge accumulation, cycle etching gradually deepens the structure without micro-trenches. Different gas ratios and etching time not only change the plasma energy distribution but also affect the temporal synchronization between etching and passivation steps. This approach reduces the special demands on ICP equipment capabilities while achieving superior trench profiles. The optimal etching conditions produced a micro-trench-free SiC structure with a vertical sidewall angle and a surface roughness of less than 1 nm. This methodology and resulting structures significantly advance the manufacturability of high-performance SiC power devices, enabling next-generation applications in electric vehicles and grid infrastructure where device yield and reliability are paramount.
Due to their high specific modulus and specific strength, carbon fiber reinforced polymer (CFRP) composites have been widely adopted in the aviation field. However, CFRP components produced by conventional vacuum assisted resin transfer molding (VARTM) often exhibit defects such as Pores and dry spots. To address these limitations, this study develops a large-area, highly uniform vibration-assisted VARTM (UAVR) system and conducts ultrasound-assisted experiments. The results demonstrate that ultrasonic treatment at various frequencies consistently improves moulding uniformity. In particular, when the ultrasound frequency is 22 kHz, the tensile strength increases by up to 13.23%, and the compressive strength increases by up to 8.48%. This study has practical significance for improving the performance of CFRP.
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