Browse Topic: Metallurgy
Powder metallurgy hot isostatic pressing (PM HIP) is a novel manufacturing process extensively utilized in oil & gas and aerospace industries. With the evolution of this advanced manufacturing process, many other industrial sectors including defence are benefiting from the clear strategic advantages of PM HIP compared to conventional manufacturing processes. This paper is intended to give an overview of PM HIP technologies and highlight the potential of this process for the manufacture of components for land based military systems. The study will focus on a brief introduction of PM HIP technology followed by more detailed description of some key benefits of adopting PM HIP in defence sectors. These include easier processability of Ti-alloys, generation of high-performance metal matrix composites (MMCs), manufacturing of complex shape parts and generation of multi-materials structures via HIP diffusion bonding (DB). Finally, the paper will focus on future prospectives of PM HIP.
A unified thermomechanical fatigue (TMF) life-prediction methodology is presented for lamellar graphite (grey) cast iron brake rotors operating under the severe transient thermal loads that arise in brake dynamometer durability testing. The workflow links four ingredients within a single rotor-level framework: transient nonlinear finite-element analysis, temperature-dependent inelastic constitutive modeling, a mechanism-based short-crack TMF damage model, and an elastic-plastic (nonlinear) fracture-mechanics crack-growth simulation. Two constitutive descriptions are exercised for the structural analysis — the standard rate-dependent Chaboche viscoplastic model available in Abaqus, and a user material subroutine (UMAT) that couples Chaboche viscoplasticity with continuum damage in order to reproduce the tension–compression asymmetry of cast iron. The resulting stress, strain, and temperature histories drive a multiaxial thermomechanical fatigue Damage (DTMF) computation that estimates crack initiation and early extension, after which a nonlinear fracture-mechanics procedure simulates crack-front advance toward through-thickness failure. Both constitutive models correctly localize the crack-initiation site on the rotor inner diameter, consistent with the dynamometer observations; for the loading histories examined, the standard Chaboche model yields lives in closer agreement with test. The crack-growth simulation reproduces the rapid post-initiation propagation seen experimentally and resolves branch-wise differences in crack-front evolution through the rotor section.
Impacts of laser shock peening (LSP) on the evolution characteristics of microstructure in commercially pure α-phase titanium (α-Ti) are explored by molecular dynamics (MD) simulations of high strain-rate compression. The EAM potential (Zhou potential) is selected for its ability to capture the evolution of microstructures. Considering the LSP-induced peak plasma pressure, the strain rate during the simulated shock compression process is set at 10^9 s-1 to replicate the LSP process. The stress-strain curve of the α-Ti under high strain-rate compression is obtained. The maximum equivalent stress reaches 3.6 GPa, consistent with the theoretically calculated value. The simulation results reveal that mechanical twins (MTs) are activated at a strain of 3%. The number of mechanical twins increases and eventually stabilizes, forming a network structure throughout the grains. In the meantime, numerous partial dislocations are generated adjacent to the grain boundaries. The dislocation density also increases with strain and dislocation reactions occur. Moreover, grain refinement is identified. The grain size is refined from the initial ~ 8 nm to ~ 4 nm in the polycrystalline α-Ti. Twinning, together with dislocation-mediated plasticity, drives the refinement of grain size. Gradients of twin density, dislocation density, and grain size density are induced by LSP on the surface of α-Ti. This study comprehensively investigates how LSP influences the evolution of microstructures by MD simulations. It develops an innovative numerical strategy that offers a foundation for elucidating the underlying mechanisms of LSP.
g-C₃N₄, a metal-free semiconductor photocatalyst, demonstrates remarkable potential, but its practical application in pollutant degradation is significantly limited by the rapid recombination of photogenerated electron-hole pairs and low photocatalytic efficiency. To address this, a series of magnetic recyclable g-C₃N₄/CoFe₂O₄ composite photocatalysts with different CoFe₂O₄ doping ratios were innovatively designed and prepared via thermal polymerization, sol- gel, and combined with ultrasonic and heat treatment processes. The novelty of this composite design lies in the effective integration of magnetic CoFe₂O₄ with g-C₃N₄ through a heterojunction structure. It substantially boosts the absorption of visible light. Concurrently, it effectively fosters the separation and mobility of photo-induced charge carriers. The composite materials were systematically characterized by X-ray diffraction, thermogravimetric analysis, scanning electron microscopy with energy-dispersive X-ray spectroscopy, photoluminescence spectroscopy, and ultraviolet-visible diffuse reflectance spectroscopy. Using tetracycline hydrochloride as the target pollutant, the photocatalytic activity of the composites was evaluated under visible light irradiation, and the effects of initial concentration, catalyst dosage, and the influence of solution pH on degradation efficiency were also examined. The results indicated that the composite with a CoFe₂O₄ to g-C₃N₄ mass ratio of 1:3 (denoted as 3-CN/CFO) exhibited the optimal performance: a TCH degradation rate of 80.29 % within 105 minutes and a total organic carbon removal rate of 61.63 %. After five consecutive cycling experiments, the degradation efficiency remained above 70 %, demonstrating good reusability and stability. The performance improvement is attributed to the formation of heterojunctions in the composite, which effectively facilitates charge separation, inhibits carrier recombination, and enhances visible light absorption. Furthermore, the inherent magnetism of the composite permits efficient recovery, streamlining its integration into practical applications. Toward the purification of antibiotic-contaminated water, this research proposes a viable method for fabricating highly effective and recyclable photocatalysts.
Wirtgen Group hosted select media at its training and technology center near Nashville to demonstrate the full road-building workflow - from milling and paving to compaction - and how connected machines, automation and real-time data are helping crews to work more efficiently. As part of John Deere's construction equipment portfolio, Wirtgen Group's specialized machinery combines with Deere's TechStack and digital fleet management technology to improve productivity, efficiency, safety and pavement quality. Wirtgen (rehabilitation), Vögele (paving) and Hamm (compaction) machines were in action for the roadbuilding demo. Other Group brands not demoed include Kleeman for crushers and screening plants for processing, and Benninghoven, which is not part of the portfolio in the U.S., for mixing and recycling plants.
This study carefully designed and successfully developed a mechanical voltage stabilizing control device. The device uses silicone oil as the key component material of the liquid spring and 1Cr13 as the main material of the pressure control unit, enhancing its high-pressure resistance (up to 35 MPa), oxidation resistance, and acid-alkali corrosion resistance. By optimizing the transmission mechanism and simplifying the pressure regulation module, the device achieves a pressure regulation range of 0.1–21 MPa with an accuracy of ±0.01 MPa, significantly broader and more precise than traditional devices. To address manufacturing challenges, advanced CNC machine tools, ceramic cutting tools, and optimized heat treatment processes (e.g., quenching and tempering) were adopted, ensuring component machining accuracy within ±0.02 mm. Field applications in 13 oil wells demonstrated a 15.6% increase in daily oil production (from 25.5 t/d to 29.5 t/d) and a 17.9% increase in daily gas production (from 2800 m^3/d to 3300 m^3/d), with stable casing pressure control at 5.3 MPa. The device has created 1.225 million yuan in economic benefits while eliminating safety hazards, providing critical technical support for efficient and environmentally friendly oil and gas production.
Blended metal powders offer a compelling alternative to pre-alloyed powders in metal additive manufacturing by providing access to a wider range of alloy compositions and avoiding the high costs in producing pre-alloyed powders. In this work, a new and crack-free Ti-5AlMnScZrMgSiFe alloy (in wt.%) was manufactured by laser powder bed fusion (L-PBF) from mixed powders to investigate the microstructures, mechanical performance of printed parts. Ti-5 AlMnScZrMgSiFe alloy contains both alpha (α) and alpha prime (α′) phases. Further microstructural characterizations show that the L-PBF Ti-5 AlMnScZrMgSiFe contain dense dislocations and twins formed in additive manufacturing process. The as-printed Ti-5 AlMnScZrMgSiFe alloy exhibits a tensile fracture strength of ~950 MPa with a fracture elongation of ~12.5%. The eye-catching properties are attributed to the dense dislocations, nano-twins and solid-solution strengthening.
This specification, in conjunction with the general requirements for steel heat treatment covered in AMS2759, establishes the requirements for heat treatment of precipitation-hardening corrosion-resistant, maraging, and secondary hardening steel parts. Parts are defined in AMS2759. Parts made from steels other than those specified in this specification may be heat treated in accordance with the applicable requirements herein using processing temperatures, times, and other parameters recommended by the material producer unless otherwise specified by the cognizant engineering organization. General ordering instructions are specified in AMS2759.
Current lithium-ion batteries should generally only be charged above 0 °C, as charging below this temperature can promote lithium plating and irreversible degradation. However, conventional pack-level heating elements increase system mass and design complexity. In addition, heat is transferred from outside into the cell, causing the temperature inside the cell to rise slowly. This study evaluates internal Joule heating of cylindrical Li-ion cells using a zero-mean square-wave current excitation and quantifies the associated aging impact. LG INR21700-M50L cells were tested at 0 °C, −10 °C, and −20 °C with three excitation frequencies (50 Hz, 1 Hz, 10 mHz) at 5 A amplitude. Each cycle consisted of 30 min heating followed by 60 min cooling; reference capacity-based state of health (SOH) was assessed every 50 cycles up to 400 cycles. A maximum surface temperature rise of 14.3 K was achieved, with larger temperature rise at lower ambient temperature and lower excitation frequency. Capacity fade remained below approximately 1% for most conditions; however, at −20 °C and 10 mHz a pronounced SOH decrease to 87% was observed, indicating a critical operating regime. The results provide practical guidance for pulse-heating parameter selection and highlight the need for safeguards and further diagnostics in extreme low-frequency excitation at very low temperatures. This heating approach is particularly suitable for simpler battery-electric applications without thermal management, such as e-bikes or power tools. However, it may also be relevant for applications with existing thermal management systems, as it simplifies battery pack design.
This specification, in conjunction with the general requirements for steel heat treatment covered in AMS2759, establishes the requirements and procedures for three classes of gas, vacuum, liquid, and low-pressure carburizing (LPC) and related heat treatment of parts fabricated from carburizing-grade steels. Parts made from steels other than those specified in the detail specifications may be heat treated in accordance with the applicable requirements using processing temperatures, times, and other parameters recommended by the material producer. This specification does not cover pack carburizing.
For brake and clutch components of aircraft vehicles which require higher mechanical strength and wear resilient, light-weight aluminium composites were developed infusing solid lubricant. In this study, hybrid composites were developed using powder metallurgy route with aluminum alloy AA356 and various amounts of zirconium oxide (ZrO2) (0, 5, 10, 15, and 20 wt.%) as reinforcements. A solid lubricant hexagonal boron nitride (hBN) at a fixed 5 wt.% is considered. Following the appropriate ASTM guidelines, the specimens were mechanically characterized by measuring their density, porosity, micro-hardness, compression strength, impact strength, and flexural strength, among other properties. The findings showed that the composites' mechanical and physical behaviour were greatly affected by the inclusion of ZrO2. Porosity increased as a result of particle clustering and interfacial voids, while density increased gradually as ceramic content increased. Consistently increasing ZrO2 addition led to micro-hardness improvements; at 20 wt.% reinforcement, values reached their maximum, indicating that the hard ceramic phase contributed to better surface resistance. The best balance between particle reinforcement and matrix continuity was suggested by the compression and flexural strengths peaking at 15 wt.% ZrO2. However, when the addition was raised to 20 wt.%, brittleness and porosity began to marginally deteriorate. Unreinforced and lower ZrO2 composites had superior toughness in impact, whereas materials with a higher content had a poorer energy absorption capacity. The 5 wt.% hBN improved fracture arresting capabilities and helped load transmission over the interface. Inclusion of hBN provides solid-lubricating tribofilm formation that enhances the tribological performance. This study reveals that AA356/ZrO2-hBN hybrid composites have good hardness and compressive strength improvements, with 15 wt.% ZrO2 being the best composition with good strength, toughness, and wear resistance.
Researchers at Columbia Engineering have developed a new gel electrolyte that both improves the lifetime and safety of anode-free lithium batteries, an emerging battery architecture that could dramatically boost energy density while simplifying manufacturing. Although such design promises higher energy density and lower cost, the approach has long been plagued by short battery life and safety concerns caused by unstable lithium plating and parasitic reactions at the electrode-electrolyte interface.
Machina Labs recently closed its latest round of financing with $124 million, enough to develop a facility featuring up to 50 of its RoboCraftsman cells capable of producing thousands of complex structural assemblies for aerospace and defense customers - a list that already includes Lockheed Martin and the U.S. Air Force, among others. Founded in 2019, Machina Labs is a California-based company that seeks to reinvent metal manufacturing with a robot that uses artificial intelligence (AI) to rapidly form and assemble complex military grade structures directly from digital design files. RoboCraftsman is the company's manufacturing robot that leverages its proprietary “RoboForming” process to integrate multiple manufacturing processes - including metal forming, trimming, scanning, and heat treating - into a single containerized machine.
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