Browse Topic: Coating processes

Items (429)
To develop magnesium matrix composites, ceramic silicon nitride (Si3N4) particles are added to the magnesium (AZ31) matrix at 2 wt.%. The composite is produced via disintegrated melt deposition vacuum-stir-casting procedure. Microstructural studies reveal the presence of Si3N4 particles and their uniform spreading. An L9 orthogonal array, planned using Taguchi’s experimental design, is selected for three wear parameters; axial load (AL), rotational speed (RS), and time duration (TD) with trials as per the G99 standard in the pin-on-disc apparatus to assess the wear resilient of the composite. Experimental results show an increase in axial stress, and wear loss (WL) increases dramatically. Because the area of contact shrinks as RS increases, WL diminishes dramatically. When the AL is low, the friction coefficient (CoF) increases, and when the AL is large, CoF drops. When the RS is increased, CoF decreases. To optimize multiple responses effectively, the TOPSIS (Technique for Order Preference by Similarity to Ideal Solution) approach was adopted. According to the analysis, the ideal combination turned out to be a 10 N A, an RS of 275 rpm, and a TD of 1000 seconds. ANOVA results show that AL (56.99%) and RS (27.2%) contribute more, with a regression coefficient of 92.99%. Abrasive and adhesive wear mechanisms are observed from the worn-out surface micrographs.
Senthilkumar, N.Dhinakar Raj, C K
Cold spray deposition is a kinetic-based deposition method that uses an inert gas flow to accelerate particles, where kinetic energy causes plastic deformation upon impact with a substrate, as discussed in Reference 1. Cold spray has been investigated as a method to deposit metal coatings on polymer-based composites, such as aerospace carbon-fiber-reinforced plastics (CFRP's), as discussed in Reference 2. These methods also exhibit low deposition efficiency (15-45%) as shown in Reference 3. In this work, to achieve high deposition efficiency and create an erosion-resistant coating, we use metal-polymer composite powders for cold spray, to make polymer-on-polymer bonding the dominant and effective bonding mechanism; this method lowers impact velocities relative to pure metal deposition to avoid substrate damage. The polymer can also lower the effect of material mismatch, while the nickel can help enhance the erosion performance of the final coating above that of pure polymer. This paper discusses the development of the cold spray deposition process, sample post-processing, erosion testing, and characterization of the samples. The results validate that this method successfully creates a method of depositing a coating with erosion resistance approaching that of bulk titanium without substrate damage on PEEK substrates. Further work is needed to address the issues with depositing on CF-PEEK substrates.
Fischer, BrandonWolfe, DouglasRyan, CaillinDeSalle, ChrisYamamoto, Namiko
In the design of Rechargeable Energy Storage System (RESS) structures, including battery trays, module side plates, and end plates, there are multiple conflating factors, including: Mechanical requirements necessitating the use of electrically conductive materials (steel and aluminum); proximity between battery module structure and battery cells, necessitating the use of electrical isolation coatings; and, module and pack designs that retain cells via the use of Structural Adhesive Material (SAM). Inherently, with this design approach, organic coatings are placed in a new and perilous position. In a sense, the coating becomes a supplement to an adhesive. As Computer-Aided Engineering (CAE) virtual analysis tools become more sophisticated, there is increasing reliance on these tools to predict the occurrence of structural failures in various load cases. Factors in test method, paint pretreatment, and topcoat affecting adhesion of organic coatings in structural adhesive joints are discussed, including: Adhesive sample preparation; adhesive selection, coating film pretreatment; age of pretreatment bath; acid cleaning; substrate material type (steel vs. aluminum); substrate product form effects within aluminum, and coating thickness. This information is useful for organic coating process development on metallic substrates. It is especially useful for material constructions requiring paint in contact with structural adhesives, as in these joints, paint adhesion is often a limiting factor on the performance of the structural adhesive. The characterization and optimization of this interface is especially important for EV battery modules & packs.
Moceri, CharlesHarper, Jared
This specification covers the requirements for a manganese phosphate coating on ferrous alloys.
AMS B Finishes Processes and Fluids Committee
This specification covers engineering requirements for applying tungsten carbide thermal spray coatings to ultrahigh-strength steels (220 ksi and above) utilizing high-velocity oxygen fuel (HVOF) combustion-driven processes and the properties for such coatings. The processes and procedures herein apply only to the properties of the as-deposited coating.
AMS B Finishes Processes and Fluids Committee
In complex manufacturing processes, reliable & efficient simulation tools are essential to supplement expensive prototyping and physical testing, optimizing the design stage efficiently. The manufacturing industry seeks solutions for e-coating, which involves optimizing design painting process parameters like tank dimensions, part trajectory, line speed, and geometrical part design details. New generation CFD tools, such as Creo Flow Analysis (CFA), which is integrated in PTC (Cre-o) offer high accuracy, efficient workflows, and short computational times. The goal is to gain insights into how design parameters affect the process and optimize them. CFA provides powerful Volume of Fraction (VOF) multiphase simulation techniques along with body motions in a user-friendly process, enabling quick verification of painting processes or part designs. Surface coating protects industrial products from corrosion and other environmental influences. Electrophoretic coating (e-coating) is a surface engineering process used to coat metallic components [1]. The paint deposition process has been studied using traditional Computational Fluid Dynamics (CFD) tools (Star-CCM+) to predict coating effectiveness and determine over/under painting phenomena. The VOF model in Creo Flow Analysis describes impact phenomena on the wall. The process identifies uncoated areas and paint accumulation due to model orientation during dip-in or dip-out or design challenges or speed of dip-in etc., Traditional CFD tools take significant time, from weeks to months, to complete one study. With advanced right fidelity modeling techniques in CFA, timelines are reduced to weeks and days. This innovative approach demonstrates high business impact by enabling decisions on dip-in and dip-out process (speed and part orientations) to improve & optimize painting process speed or/and paint quality. This article explores the paint dip-in and dip-out process and showcases CFA's virtual analysis capabilities in simulating and optimizing fluid-dynamic aspects and also demonstrates the e-coating verification using traditional CFD tool, Star-CCM+.
Rao, Pooja DhavalTirumala, BhaskarSoni, Tanushree
NiCoCrAlY powders were thermally sprayed by combustion flame spray (CFS) and high-velocity oxygen fuel (HVOF) processes on IN 718 alloy substrates. Experimental parameters were fixed to manufacture coatings with a thickness about 200 μm. Microscopy and X-ray diffraction analyses were performed to reveal microstructural characteristics of both developed CFS and HVOF coatings, and it was observed that they were formed by a lamellar morphology composed of β and γ phases. The analyses also revealed lower porosity in the coatings produced by HVOF process while was compared with CFS process. While a microstructure composed of like-deformed powder was developed in HVOF process, in the case of CFS a building layer-by-layer was characteristic. Vickers hardness tests were also performed, and it was found that coating developed by HVOF process showed quite higher hardness values compared with those measured on the coatings developed with the CFS process, nonetheless this difference was small. Hence, the results showed that the coatings by CFS process are very promising for industrial applications, with negligible manufacture costs and very appropriate to be applied in situ.
Juarez-Lopez, FernandoMendoza, Melquisedec VicenteMeléndez, Rubén CuamatziRamírez, Ángel de Jesús Morales
This specification covers tungsten carbide-cobalt in the form of powder.
AMS F Corrosion and Heat Resistant Alloys Committee
This standard establishes the recommended requirements for application of AMS3144 anodic electrodeposition primer to aerospace components. Adherence to these requirements will help facilitate satisfactory performance of the applied primer.
AMS G8 Aerospace Organic Coatings Committee
The aim of this work is to present the overviewing results of the low friction coating technology for modern automotive application with the themes, e.g. electric vehicle (EV), R&D trends and bioethanol fuel application. According to Forbes, China, armed with EV, could have several companies among the top 10 global brands by sales in 2030. EV’s friction is more severe than traditional powertrain friction. For the protection of EV’s wear and friction, the coatings, diamond like carbon (DLC) and CrCuN, are compared in the literature. Global coating companies developed with the keywords: hybrid process, low-temperature coating process for polymer material. Last coating conferences showed R&D trends: coating for polymer materials, tetrahedral amorphous carbon (taC) coating, low-temperature coating process and multi-elements containing coatings. In Korea, research institutions, universities and Hyundai Motor Group have a long-term project for the development of ultralow friction coatings of moving parts incl. EV application. From current friction coefficient of 0.05, candidates of the friction coefficient 0.03 are, e.g. metal-doped carbon based materials. The final target is a friction coefficient of 0.01; recent results are discussed. The object of this work is firstly to overview the R&D status and the new taC coating for fuel injector ball is to investigate for the protection of bioethanol induced corrosion and wear. Furthermore the results of on developing future coatings, nanocomposite coatings, are presented.
Cha, Sung ChulMoon, Kyoung IlKim, JongkukPark, Chang HoKim, Dong Sik
The working conditions of combustion systems have been going extreme under the desire of human beings exploring the unknown. Cold environments can be a significant impact on the spraying of fuel not only by changing the fuel properties including viscosity and surface tension, but also by freezing the parts. In the present study, methanol spray from a commercial injector is studied via high-speed imaging, with the liquid fuel being frozen to sub-zero degrees at the injector tip. It is observed that water components from the environment will freeze at the injector tip, creating crystal structures on the surface. During the injection, the ice components will be flushed by the liquid, and the spray morphology of the starting cycle will be strongly altered, resulting in wider spray angles, much shorter penetrations, and particle structures can be observed in the downstream of the flow field. The results of the experiment provide a clear view and quantified evaluation of the freezing impact on spray development from practical injectors, and gives a sketch of the most extreme condition of the fuel spray before the valve is chilled to the bone and unable to open.
Zeng, TingxiWang, ShangningZhang, YijiaHung, DavidXu, Min
Maintaining the operational readiness of military helicopters demands repair solutions that are fast, reliable, and adaptable. This paper presents the integration of Gamma Alloys' advanced metal matrix composites (MMCs) into additive manufacturing (AM) techniques - specifically Cold Spray and Friction Stir Additive Manufacturing (FSAM) - as a transformative approach to helicopter repair and replace for the US Army.
Peabody, MicahHarrigan, William
In the automotive industry, it is essential to consider not only how well specialty materials perform and are formulated, but also how efficiently and economically they can be applied during manufacturing. This becomes especially important during the early stages of development to prevent issues when these materials are used in new designs by automotive suppliers or manufacturers. With the rapid growth of electric vehicles (EVs), new materials are being used more frequently, and these materials may not have been as thoroughly tested as those used in traditional internal combustion engine (ICE) vehicles. Therefore, it is crucial to ensure that these materials can be applied correctly and efficiently from the start. One way to speed up the development process is through Computational Fluid Dynamics (CFD) modeling. CFD helps predict how materials will behave when dispensed, which is essential for developing the right equipment and conditions for applying these materials. Working with Graco, a leading manufacturer of fluid management and dispense solutions, Dow and Graco have used these models to design better equipment solutions and improve the software used. This ensures high-quality and efficient application at start up. This paper will present two case studies how material models were developed, tested, and validated with real-world data to ensure they work as intended. The goal is to demonstrate how optimizing dispensing equipment based on material characteristics is critical for maintaining process windows and product quality. By doing so, manufacturers can achieve better results, reduce waste, and ensure the reliability of new materials in automotive applications.
Kenney, J. AndyDelgado, RobertoHossain, ArifNg, Sze-SzeThomas, RyanChyasnavichyus, MariusTsang, Chi-WeiHwang, MargaretWu, LanceDietsche, LauraMcmichael, JonathanRaines, KevinNelson, Grant
Metal bipolar plates are important components of fuel cells, playing a role in conducting electricity, gas, and heat during the operation of fuel cells. The sealing and joint quality of the bipolar plates have a significant impact on the performance and service life of fuel cell stacks. In actual production, laser technology is often used for welding bipolar plates, and the welding quality is ensured by laser process parameters when using the same equipment. Therefore, in order to further optimize the laser welding process of metal bipolar plates, this paper selects three laser parameters for single-factor analysis to evaluate the impact of each parameter on laser welding quality. The Box-Behnken design-response surface method is used for multi-factor analysis, with process parameters as inputs and weld quality parameters as outputs, to assess the sensitivity of each laser process parameter to laser welding quality, and to fit a nonlinear function. Based on the results, the optimal welding process window is derived to improve the quality of the welds in the actual welding process. Finally, a comprehensive welding quality assessment system is established on the premise of reducing costs and improving quality.
Li, WeiChang, GuofengXu, HuashengHuang, Ziheng
The solar-based hybrid automotive vehicle represents a trend marked by technological excellence, offering an efficient, cost-effective, and eco-friendly solution. Besides, the enhancement of solar absorption due to poor weather is influenced by poor solar power with reduced photocurrent density. This research focuses on enhancing the solar power and photocurrent density of conventional solar cells featuring aluminium-doped zinc oxide thin films (AZO) using the Mist Chemical Vapor Deposition (MIST CVD) process with a zinc acetate precursor solution processed at temperatures ranging from 200 to 400°C. To investigate the effect of AZO on the functional behaviour of solar cells, microstructural studies utilizing scanning electron microscopy and X-ray diffraction reveal the concentration of AZO and the alignment of Al/ZnO peaks as even. As a result, this research demonstrates a 21% increase in solar power output compared to conventional Cadmium Telluride (CdTe) cells, with an improvement in photocurrent density of 1.24 mA/cm2. This advanced solar cell technology is recommended for use in electric vehicle (EV) applications.
Venkatesh, R.De Poures, Melvin VictorThangamani, P.Manivannan, S.Devanathan, C.Boopathi, M. SugadevaBaranitharan, BalakrishnanMadhu, S.Kaliyaperumal, Gopal
This standard provides the recommended requirements for electrostatic spray application of AMS3143 powder coatings to aerospace components. Adherence to these requirements will facilitate satisfactory performance of the applied powder coating.
AMS G8 Aerospace Organic Coatings Committee
This specification covers the engineering requirements for applying coatings to parts by the plasma spray process and the properties of such coatings.
AMS B Finishes Processes and Fluids Committee
This specification establishes process controls for the repeatable implementation of the CSAM process for the manufacturing of metallic and metal-nonmetal blend components.
AMS AM Additive Manufacturing Metals
Aerospace & Defense Technology: December 202424AERP1212/5/2024
Making a Material Difference in Aerospace & Defense Electronics Acquiring and Telemetering Test Data from Hypersonic Platforms Analog Transformation Complements Open System Designs to Optimize Modern Defense Systems These Speedy Cold Spray Machines Can 3D Print Vehicle Parts in War Zones Researchers Use Ancient Japanese Art Method to Create Tunable Antennas What is Drone Jamming and How Can it Be Countered? AI-Trained Vehicles Can Adjust to Extreme Turbulence on the Fly Researchers at Caltech took an important step toward using reinforcement learning to adaptively learn how turbulent wind can change over time, and then uses that knowledge to control a UAV based on what it is experiencing in real time. 'First of Its Kind' Composite Material to Help Space Vessels Travel Longer Distances A Coventry University design and materials engineer is leading an international team of researchers in the creation of a new material for liquid hydrogen storage tanks that are used to propel rockets into space. Scientists Fuse Simulations and Machine Learning to Accelerate Novel Additively Manufactured Materials Researchers at the Johns Hopkins Applied Physics Laboratory have developed a machine learning method that could have a huge impact on understanding how material is formed during the additive manufacturing process. Aviation Safety Expert Unites Industry to Safeguard Aviation Supply Chain A new aviation supply chain integrity coalition has offered 13 recommended actions to prevent the circulation of non-serialized aircraft parts throughout the global aviation industry. DEVCOM CBC Innovates and Integrates through Autonomous Technologies Researchers and engineers at the U.S. Army Combat Capabilities Development Command Chemical Biological Center have developed a prototype system for decontaminating military combat vehicles.
As “point of need” additive manufacturing emerges as a priority for the Department of Defense (DoD), Australian 3D printing provider SPEE3D is one of several companies demonstrating that its machines can rapidly produce castings, brackets, valves, mountings and other common replacement parts and devices that warfighters often need in an on-demand schedule when deployed near or directly within combat zones. DoD officials describe point of need manufacturing as a concept of operations where infantry and squadron have the equipment, machines, tools and processes to rapidly 3D print parts and devices that are being used in combat. Based in Melbourne, Australia, SPEE3D provides cold spray additive manufacturing (CSAM) machines that use a combination of robotics and high-speed kinetic energy to assemble and quickly bind metal together into 3D-printed parts without the need for specific environmental conditions or post-assembly cooling or temperature requirements. Over the last two years, the company has participated in military point of need manufacturing challenges and demonstrations with military units from the U.S., UK, Australia and Japan among others.
Super Duplex Stainless Steels (SDSS) are attracting attentions of the manufacturing industries due to the excellent corrosion resistance to critical corrosion. But SDSS2507 is the hardest to machine with lowest machinability index among DSS family. Moreover, formation of built-up layer (BUL) and work hardening tendency makes it further difficult to machine. Researchers have the conflict in opinions on using wet machining or dry machining using tool coatings. In this investigation SDSS2507 machining is carried out using uncoated and PVD–TiAlSiN-coated tools. The wet and dry machining environment are compared for increase in cutting speed from 170 m/min to 230 m/min. Excellent properties of PVD–TiAlSiN coatings exhibited microhardness of 39 GPa and adhesion strength of 88 N, which outperformed the uncoated tools. Tool life exhibited by coated tools was four times higher than uncoated tools. Wet machining was found to be ineffective when PVD-coated tools are used, exhibiting the same performance as that of dry machining. Dry machining can be preferred for the machining SDSS2507 with PVD–TiAlSiN-coated tools, eliminating the cost of cutting fluids with enhanced productivity.
Sonawane, Gaurav DinkarBachhav, Radhey
To combat corrosion and wear issues of automotive brake discs, many manufacturers have introduced various surface treatment technologies, such as thermal spraying, laser cladding, and ferritic nitrocarburizing (FNC). Besides those surface treatment technologies, a plasma electrolytic aluminating (PEA) process has also shown to be effective in producing alumina-based ceramic coatings on cast iron substrates, providing an enhanced corrosion resistance. In this study, the PEA-coated brake rotor and FNC-treated brake rotor were comparatively tested in various corrosion conditions, including an electrochemical corrosion test and simulative corrosion experiment, before and after a road driving test. A scanning electron microscope (SEM) and an energy-dispersive X-ray (EDX) were used to observe and analyze morphology and chemical compositions of the surfaces and cross-sections of the tested rotors. The results showed that the new PEA-coated brake rotor demonstrated the best corrosion resistance in the electrochemical corrosion test among all given tested cases. After the vehicle test, the PEA-coated rotor surface had an obvious materials transfer layer which can protect the rotor from abrasive wear. The transfer layer materials sourcing from the low-met brake pads however contained metallic elements, leading to appearance of a lower corrosion resistance during the electrochemical corrosion test. In duration of the vehicle road test (1000 braking events at 0.3-0.4 g), the FNC brake rotor showed some loss of its white layer but maintained its nitrogen diffusion layer, which still showed protection to the brake rotor base material from corrosion. It was also found that some surface areas where the graphite flakes were located on FNC-treated cast iron brake disc surface were exposed to the ambient environment, which may be a reason why the localized corrosion appeared on the FNC-treated rotor in the late stage of the vehicle road test.
Liu, YintingNie, Xueyuan
Graphene has been called “the wonder material of the 21st century.” But graphene has a dirty little secret: it’s dirty. Now, engineers at Columbia University and colleagues at the University of Montreal and the National Institute of Standards and Technology are poised to clean things up with an oxygen-free chemical vapor deposition (OF-CVD) method that can create high-quality graphene samples at scale. Their work, published in Nature, directly demonstrates how trace oxygen affects the growth rate of graphene and identifies the link between oxygen and graphene quality for the first time.
The paramount importance of titanium alloy in implant materials stems from its exceptional qualities, yet the optimization of bone integration and mitigation of wear and corrosion necessitate advanced technologies. Consequently, there has been a surge in research efforts focusing on surface modification of biomaterials to meet these challenges. This project is dedicated to enhancing the surface of titanium alloys by employing shot peening and powder coatings of titanium oxide and zinc oxide. Comparative analyses were meticulously conducted on the mechanical and wear properties of both treated and untreated specimens, ensuring uniformity in pressure, distance, and time parameters across all experiments. The outcomes underscore the efficacy of both methods in modifying the surface of the titanium alloy, leading to substantial alterations in surface properties. Notably, the treated alloy exhibited an impressive nearly 12% increase in surface hardness compared to its untreated counterpart. Moreover, the study elucidated significant reductions in the coefficient of friction for the treated specimens—both shot-peened (0.11) and powder-coated (0.12)—in contrast to the untreated specimen with a maximum coefficient of friction of 0.15. These findings highlight the potential of shot peening and coating techniques to enhance the tribological properties of titanium alloys, crucial for implant applications. The investigation delves into elucidating the likely mechanisms underlying the surface attribute development facilitated by shot peening and coating processes. By emphasizing their transformative impact on the properties of titanium alloy, the study sheds light on avenues for improving implant materials, thus advancing the field of biomaterials and contributing to enhanced patient outcomes in medical implantation procedures.
Balasubramanian, K.Bragadeesvaran, S. R.Raja, R.Jannet, Sabitha
University of Wisconsin–Madison engineers have used a spray coating technology to produce a new workhorse material that can withstand the harsh conditions inside a fusion reactor.
Rotary Bell Atomizers are well established in the automotive industry for top coating applications. This type of atomizer allows to create a uniform coating and is characterized by high productivity. Meanwhile, the effectiveness of the process depends on many complex factors. For instance, the transfer efficiency of the paint material, which is the percentage of the paint reaching the structure surface, ranges from 60-95% depending on the application conditions. Any increase in the transfer efficiency can not only reduce energy and material costs, but also reduce the emission of harmful non-deposited paint particles and the effort to handle them. The use of accurate numerical methods in this process helps to optimize the application process, reduce the number of expensive field experiments, and shortens the development cycle of new vehicles, which ensures predictability of production costs. This paper describes a multidisciplinary framework that allows to simulate the industrial processes of coating paint quickly with high accuracy on complex car geometries. Film deposition of paint droplets on the target, the movement of paint particles between the target and the atomizer and the effect of a swirling air jet on the droplet trajectory are all considered. The complex atomization around the bell cup is replaced by a statistical droplet generator. Furthermore, to speed up the simulation, a simplified version of the complex shaping air system is proposed in the work. To model the process, a coupled multi-physics solver is developed, which combines lattice Boltzmann method for air flow, Lagrangian particle method for paint droplets, and the thin film solver for coating thickness calculation. The paper presents the physical and mathematical model of the process, brief introduction on the numerical methodology, validation results based on experimental data, and the results of modelling practical coating scenarios. Results show that the proposed approach has high reliability and can be applied to accurate top coating simulation and the related process/design optimization.
Panov, DmitriiMenon, MuraleekrishnanZhu, HuaxiangStadik, AlexanderZhang, LingranKotian, AkhileshPeng, ChongMonaco, ErnestoBorra, Ravi KanthBoraey, Mohammed
The wear of the piston ring-cylinder liner system in gasoline engines is inevitable and significantly impacts fuel economy. Utilizing a custom-built linear reciprocating tribometer, this study assesses the wear resistance of newly developed engine cylinder coatings. The custom device offers a cost-effective means for tribological evaluation, optimizing coating process parameters with precise control over critical operational factors such as normal load and sliding frequency. Unlike conventional commercial tribometers, it ensures a more accurate simulation of the engine cylinder system. However, existing research lacks a comprehensive comparative analysis and procedure to establish precision limits for such modified devices. This study evaluates the custom tribometer's repeatability compared to a commercial wear-testing instrument, confirming its potential as a valuable tool for advanced wear testing on engine cylinder samples. The validation tests, achieved through standardized contact geometries, confirm the precision and reliability of the custom tribometer, highlighting its potential for advanced wear testing on engine cylinder samples. Utilizing 2D stylus profilometry, wear progression rates are examined, with a coefficient of variation for wear volume results ranging from ±0.63% to ±2.52% compared to a commercial device across tests, showcasing its precision and reliability.
Sediako, Dimitry G.Banerjee, Siddharth
This study delves into the innovative realm of synthesizing surface alloyed materials by utilizing copper-based metamorphic powders subjected to high-intensity electron beam irradiation. The process involves depositing metamorphic particles onto a stainless-steel substrate, and subsequently exposing the assembly to a powerful electron beam, resulting in the development of distinct surface alloyed layers. A notable advancement was achieved by introducing a second layer of metamorphic powders over the existing alloyed layer, followed by further treatment with the electron beam. The alloyed layers, characterized by a volumetric concentration ranging from 60 to 67%, exhibited a fascinating phenomenon— the formation of abundant borate crystals with the chemical formula Al2.56Fe1.75Ni0.84. This crystal presence significantly elevated the hardness of the surface alloyed layers, showcasing an impressive five to sevenfold increase compared to the substrates. Importantly, the alloyed layers demonstrated remarkable thermal stability, successfully enduring a rigorous test at 450 degrees Celsius. The subsequent Vickers hardness measurement, registering at 300 VHN, underscores the substantial and enduring hardness achieved. Beyond these core findings, this study sheds light on the potential of alloyed-surface materials in demanding applications requiring robust heat resistance and exceptional wear resistance. The methodological synergy of metamorphic powders and electron beam irradiation serves as a promising avenue for the development of advanced materials with heightened mechanical properties. Furthermore, this research opens avenues for future investigations into the specific structural and compositional attributes contributing to the observed material enhancements.
Dinesh Krishnaa, S.Sangeeth Kumar, M.Dhiyaneswaran, J.Rishi Karthikeyan, V.P.Saran Rithik, B.
This specification covers the requirements for vacuum deposited cadmium.
AMS B Finishes Processes and Fluids Committee
Naval Air Systems Command Naval Air Station North Island, CA (619) 545-3415
Simulation tools play a significant role in the automotive industry due to their cost-reducing capabilities in new model development. Computational Fluid Dynamics (CFD) is extensively utilized in various applications, such as vehicle aerodynamics and engine thermal management. However, its application in manufacturing engineering is not yet widespread. One crucial process in automotive manufacturing is the application of the base coat, which provides protection for the final paint layer. This process involves three key steps: bodywork immersion, electrophoretic deposition (E-coat), and bodywork removal from the bath. Each of these steps can be evaluated using appropriate CFD models. During the immersion step, the primary objective is to minimize the presence of trapped air. In the E-coat step, the focus is on controlling the paint layer thickness on the Body-in-white (BIW). Lastly, the drainage analysis aims to minimize the retention of bath fluid, thereby preventing contamination in subsequent baths. In this study, we propose a methodology utilizing Simcenter STAR-CCM+ as the CFD code and a generic car geometry to evaluate these three painting stages. Our methodology demonstrates the effectiveness of Simcenter STAR-CCM+ in predicting the behavior of the BIW throughout the painting process. By simulating the evolution of physical phenomena, our methodology provides valuable information regarding the presence of trapped air during the dipping stage, the thickness of the paint layer during E-coat, and the volume of retained liquid during drainage. This approach offers a promising means to reduce prototype investments by anticipating the behavior of the BIW during the virtual painting process. As a result, potential quality issues can be identified and rectified by making necessary component changes. Moreover, this methodology can be employed to optimize the painting process itself, including the adjustment of parameters related to the generated electric field and the movement of the BIW within the bath. These optimizations aim to enhance energy efficiency and accommodate changes in line speed, maintenance of anodes, and alterations in chemical characteristics of the bath. In conclusion, the use of CFD simulations, specifically employing the presented methodology with Simcenter STAR-CCM+, proves to be highly beneficial in evaluating and optimizing the three critical stages of the automotive painting process. This approach enables the identification and mitigation of quality problems, offers cost savings in prototype development, and facilitates process adjustments for improved efficiency and adaptability.
Vieira, Tiago Augusto SantiagoAraújo, Pedro HenriqueAbdu, Aline Amaral QuintellaCury, Davi MachadoMonteiro, Henrique Carlos
Graphene is a two-dimensional carbon material made of carbon by covalent bonds, where carbon atoms are arranged in a honeycomb lattice. Graphene has promising electronic and mechanical properties. There are many processes available for the formation of the graphene. CVD (Chemical Vapor Deposition) process for the formation of graphene over the metal surface is most compatible. Graphene is being investigated for its application in space electronics. In space, there are many irradiation particles and waves like x-rays, gamma rays, alpha particles, and beta particles. Single particle like neutron can create single event upset in electronic devices. Graphene can work as a radiation shielding material. Graphene-metal, graphene and epsilon near zero metamaterials structure can be used for electromagnetic wave absorbent.
NASA instrumentation is at risk for contamination from dusty space environments. Additionally, contamination from water and ice buildup can affect instrumentation function. Researchers at the Goddard Space Flight Center have developed a viable dust, water, and ice mitigation optical coating for space flight, aeronautical, and ground applications. The innovation of the LOTUS coating prevents contamination on sensitive surfaces, like optics, that cannot be cleaned during space missions.
High-temperature corrosion is a crucial issue in power plant components such as boilers and superheaters when they operate in high-temperature aggressive environments leading to early component failure. As a result, surface modification is critical to protect parts against various types of degradations and increase operational performance at the lowest possible cost. The present study deals with Metco 42C and cenosphere-based composite coating on ASME A387 Grade 22 boiler steel material. The coating compositions were prepared by weight fraction of 5% and 10% cenosphere with Metco 42C and coated on T22 boiler tube material by plasma spray technique. To check the performance a high-temperature cyclic oxidation study at 600°C for 20 cycles in a molten salt environment of sodium sulfate (40%Na2SO4) and vanadium pentoxide (60%V2O5) was carried out and simultaneously corrosion kinetics was evaluated after each cycle. Neutral salt spray (NSS) and cyclic corrosion tests were carried out at defined temperature and humidity cycles in a salt mist environment to understand the relative corrosion resistance of coated and uncoated substrates. The characterization techniques such as scanning electron microscope (SEM) and X-ray diffraction (XRD) were utilized to check the morphology of tested samples. The bond strength, porosity, and hardness tests were done independently to characterize the coating. The results of the high-temperature oxidation test showed protective oxide layers formation on coated samples, improving high-temperature oxidation resistance. Additionally, the neutral salt spray and cyclic corrosion test results of coated substrate showed higher relative corrosion resistance as compared to uncoated substrate.
Lakkannavar, Virupakshappa K.Yogesha, K.B.
This specification covers engineering requirements for the grinding of tungsten carbide high velocity oxygen/fuel (HVOF) thermal spray coatings applied to high strength steels (220 ksi and above).
AMS B Finishes Processes and Fluids Committee
Engineers, managers, technicians and other automation professionals at most manufacturers understand the value of pretreating metal surfaces of parts to remove corrosion, grease, residue, old coatings, or to roughen the surface of metals prior to coating. By ensuring the items are cleaned down to bare metal, manufacturers can avoid costly warranty issues that result when coatings peel, flake, bubble, or otherwise fail prematurely.
Chemical Vapor Deposition (CVD) and Atomic Layer Deposition (ALD) processes deposit material on all surfaces in a process chamber. Over time, the thickness of these deposits increases to the point that material begins to delaminate, producing gas-phase particulates that negatively impact process yield. Remote and in situ chemical etching processes are used to periodically remove these deposits from chamber walls, maintaining chamber cleanliness.
Quasicrystalline (QC) coatings were evaluated as leading-edge protection materials for rotor craft blades. The QC coatings were deposited using high velocity oxy-fuel thermal spray and predominantly Al-based compositions. Ice adhesion, interfacial toughness with ice, wettability, topography, and durability were assessed. QC-coated sand-blasted carbon steel exhibited better performance in terms of low surface roughness (Sa ~ 0.2 μm), liquid repellency (water contact angles: θadv ~85°, θrec ~23°), and better substrate adhesion compared to stainless steel substrates. To enhance coating performance, QC-coated sand-blasted carbon steel was further exposed to grinding and polishing, followed by measuring surface roughness, wettability, and ice adhesion strength. This reduced the surface roughness of the QC coating by 75%, resulting in lower ice adhesion strengths similar to previously reported values (~400 kPa). The durability of polished QC coating was evaluated using sand and rain erosion. The sand erosion test was conducted per ASTM D823. The thickness of the QC coating remained unchanged post-erosion, indicating the QC coating is quite resistant to abrasion from sand. Rain erosion tests were conducted following the Icephobic Comparative Jet Pulsating Rain Erosion test (ICPjet) at the Anti-icing Materials International Laboratory, Quebec. The coating remained intact even after 190,000 impacts demonstrating extreme durability against rain erosion, and the coating outperformed current erosion-resistant aircraft paint (SAE AMS-C-83231A). Overall, the extreme erosion resistance of the easy-to-spray coating, combined with its de-icing properties and ability to be repaired using standard polishing techniques, makes the developed quasicrystalline coatings extremely promising for the protection of rotor-craft blades and other aircraft components.
Yang, QimengDolatabadi, AliGolovin, Kevin
Electroplating is a process whereby an object is coated with one or more relatively thin, tightly adherent layers of one or more metals. It is accomplished by placing the object to be coated on a plating rack or a fixture, or in a basket or in a rotating container in such a manner that a suitable current may flow through it, and then immersing it in a series of solutions and rinses in planned sequence. The advantage to be gained by electroplating may be considerable; broadly speaking, the process is used when it is desired to endow the basis material (selected for cost, material conservation, and physical property reasons) with surface properties it does not possess. It should be noted that although electroplating is the most widely used process for applying metals to a substrate, they may also be applied by spraying, vacuum deposition, cladding, hot dipping, chemical reduction, mechanical plating, etc. The purpose for applying an electroplate and the metals used for various applications follow.
Metals Technical Committee
The present investigation has been conducted to study the tribological and adhesion properties of X10CrNi18-8 austenitic stainless steel (ASTM 301) coatings deposited on aluminum alloys such as AU4G by using the arc-spraying process. These coatings were made with and without a bond-coat layer, which is constituted by NiAl. The structure of the phases that are present in coatings was characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The measurements of microhardness and tribological behavior at different loads were also performed on the surface of the coatings. Adherence test was also carried out using four-point bending tests. The SEM showed that the dense microstructures of coatings have a homogeneous lamellar morphology with the presence of porosities and unmelted particles. The main phase of coating corresponds to a solid solution as a face-centered cubic (fcc). The microhardness of coatings is nearly four times that of the two substrates of aluminum alloys. The four-point bending test results showed that the NiAl bond layer increases the critical interfacial fracture energy GIC, the force to share the multilayer is more important.
Sadki, AbdallahYounes, RassimBradai, Mohand AmokraneMesrati, Nadir
This specification covers nonfluorescent magnetic particles in the form of a mixed, ready-to-use suspension in an odorless oil vehicle and packaged in aerosol cans.
AMS K Non Destructive Methods and Processes Committee
China VI emission standards (Limits and measurement methods for emissions from diesel fueled heavy-duty vehicles, China VI, GB17691-2018) have strict particle number (PN) emission standards and so the coated diesel particulate filter (DPF) technology from the EU and US market has challenge in meeting the regulation. Hence, a coated DPF with higher PN filtration efficiency (FE) is required. Currently, there are two approaches. One is from the DPF substrate standpoint by using small pore size DPF substrate. The other is from the coating side to develop a novel coating technology. Through the second approach, a layer coating process has been developed. The coated DPF has an on-wall catalytic layer from inlet side and an in-wall catalytic coating from outlet side. The DPF has improved PN filtration efficiency and can meet China VI regulation without any pre-treatment. It has lowered soot loading back pressure (SLBP), compared to the DPF with small pore size. The paper will discuss the design concept, the impact of key parameters and some application cases.
Zhao, ChuangWang, LifengLou, DimingRen, Yedi
The sunrise vision for hydrogen economy lies in efficient, lightweight and durable devices which can convert hydrogen energy into electrical energy. Proton Exchange Membrane fuel cell (PEMFC) is a key hydrogen energy conversion system for transport sector. The efficiency and durability of PEM fuel cell largely depends on cathode electrode and membrane and Bipolar plates (BP Plates) plays an important role in it. BP plates perform the important functions of transporting fuel gases to reactive sites, collecting charges and thus conducting electricity from cell to cell, moisture adjustment of membrane, transport of produced water and provides essential mechanical strength to fuel cell stack. It makes BP plates the backbone of PEM Fuel cell power stack. For BP plates to perform intended functions, it is highly desirable BP plates to possess excellent properties on corrosion resistance, electrical conductivity, thermal conductivity, water wettability, weldability and formability. There is a conventional wisdom to use graphite plates as BP plates for the obvious advantages of high electrical conductivity and corrosion resistance. However, the unavoidable disadvantages, durability against shock and vibrations, cost and weight, machinability and limited design flexibility associated with Graphite BP plates shifted the focus to metallic BP plates. In recent times, numerous metallic BP plates are being developed. However bare metallic BP plates lack the basic performance requirements of corrosion resistance and surface/contact electrical conductivity. In order to improve these properties, specifically corrosion resistance in fuel cell environment, multiple coating systems and coatings processes are being developed. The development in BP plates coatings is primarily focused on reducing or eliminating Interfacial Contact Resistance (ICR) and improving corrosion and oxidation resistance. This paper reviews numerous coating systems, which are being developed for metallic BP plates including the process for coating deposition and key characterization techniques to evaluate the performance of metallic bipolar plate.
Chauhan, ShivPonkshe, Shripadraj
Cooling loss reduction is essential to enable further increases in thermal efficiency of reciprocating internal combustion engines. Many in-cylinder cooling loss reduction studies have been carried out by applying various thermal barrier coatings to the piston and/or other in-cylinder surfaces, taking advantage of the lower thermal effusivity of ceramic materials. However, the end result was mostly minimal or in some cases, negative. In our previous study, significant cooling loss reduction was experimentally confirmed by utilizing a mirror-like polished stainless-steel thermal sprayed surface (HVOF: high velocity oxy-fuel) on a forged steel piston. This study firstly investigated an alternative insulating layer material to stainless-steel, along with effects of its thickness on heat transfer by a one-dimensional unsteady numerical model. Results showed that lower thermal effusivity doesn’t always reduce heat transfer, but increases nonuniformity of surface temperature. Next, a modified insulation structure composed of a thin aluminum coating overlayed by physical vapor deposition (PVD: physical vapor deposition) on a stainless-steel layer of both the piston and cylinder head, was tested in a heavy-duty single cylinder engine. Aluminum was initially selected due to its high reflectance, to reduce absorption of flame radiation, but selectively absorb it at soot deposits, where the flame interacts with the wall, and reduce local convection. Experimental results suggested that higher surface temperatures of exposed areas are caused by better heat conduction outward from hot spots during and after the combustion period, through the aluminum coating. Such surface temperature equalization could also result in further reduction of cycle-integrated heat transfer.
Kawaharazuka, FumihiroUchida, Noboru
Cold spray (CS) is a rapidly developing solid-state repair and coating process, wherein metal deposition is produced without significant heating or melting of metal powder. Solid state bonding of powder particles is produced by impact of high-velocity powder particles on a substrate. In CS process, metal powder particles typically of Aluminum or Copper are suspended in light weight carrier gas medium. Here high pressure and high temperature carrier gas is expanded through a converging-diverging nozzle to generate supersonic gas velocity at nozzle exit. The CS process typically uses Helium as the carrier gas due to its low molecular weight, but Helium gas is quite expensive. This warrants a need to explore alternate carrier gases to make the CS repair process more economical. Researchers are exploring another viable option of using pure Nitrogen as a carrier gas due to its significant cost benefits over Helium. However, it shows challenges in achieving desired powder particle velocities and hence metal deposition efficiency. The work presented in this paper explores a carrier gas mixture of H2 and N2 as an alternate to Helium, to reduce the carrier gas cost. This paper describes a CFD methodology developed for predicting particle impact velocities in CS repair process at the exit of converging diverging nozzle. The key challenge in developing CFD methodology was about coupling gas & powder particle flow dynamics and application of appropriate drag laws. This modeling methodology was able to predict particle velocity at nozzle exit with more than 95% accuracy. Subsequently CFD methodology was deployed to recommend suitable process parameters such as carrier gas composition, pressure, and temperature. The process parameters have been studied using a design of experiments (DoE) study with the aim of arriving at a carrier gas composition that can help in achieving critical deposition velocity at a reduced cost.
Bhardwaj, DivyanshuBhise, Onkar PSalutagi, Shivayogi SRoberts, Kirstyn
This specification covers a mold release agent in the form of a liquid.
AMS P17 Polymer Matrix Composites Committee
This specification establishes requirements for pressure-sensitive adhesive tape designed for masking and color separation during aircraft painting operations.
AMS G8 Aerospace Organic Coatings Committee
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