Browse Topic: Composite materials
g-C₃N₄, a metal-free semiconductor photocatalyst, demonstrates remarkable potential, but its practical application in pollutant degradation is significantly limited by the rapid recombination of photogenerated electron-hole pairs and low photocatalytic efficiency. To address this, a series of magnetic recyclable g-C₃N₄/CoFe₂O₄ composite photocatalysts with different CoFe₂O₄ doping ratios were innovatively designed and prepared via thermal polymerization, sol- gel, and combined with ultrasonic and heat treatment processes. The novelty of this composite design lies in the effective integration of magnetic CoFe₂O₄ with g-C₃N₄ through a heterojunction structure. It substantially boosts the absorption of visible light. Concurrently, it effectively fosters the separation and mobility of photo-induced charge carriers. The composite materials were systematically characterized by X-ray diffraction, thermogravimetric analysis, scanning electron microscopy with energy-dispersive X-ray spectroscopy, photoluminescence spectroscopy, and ultraviolet-visible diffuse reflectance spectroscopy. Using tetracycline hydrochloride as the target pollutant, the photocatalytic activity of the composites was evaluated under visible light irradiation, and the effects of initial concentration, catalyst dosage, and the influence of solution pH on degradation efficiency were also examined. The results indicated that the composite with a CoFe₂O₄ to g-C₃N₄ mass ratio of 1:3 (denoted as 3-CN/CFO) exhibited the optimal performance: a TCH degradation rate of 80.29 % within 105 minutes and a total organic carbon removal rate of 61.63 %. After five consecutive cycling experiments, the degradation efficiency remained above 70 %, demonstrating good reusability and stability. The performance improvement is attributed to the formation of heterojunctions in the composite, which effectively facilitates charge separation, inhibits carrier recombination, and enhances visible light absorption. Furthermore, the inherent magnetism of the composite permits efficient recovery, streamlining its integration into practical applications. Toward the purification of antibiotic-contaminated water, this research proposes a viable method for fabricating highly effective and recyclable photocatalysts.
With the increasing demand for material microimaging analysis, there is a growing need for advanced precision grinding and polishing equipment, especially for metals, ceramics, and composites. Existing automated systems struggle with handling complex material challenges. This paper presents a fully automated adaptive grinding and polishing machine based on an STM32 microcontroller that handles multi-material samples. The system includes modules for sample access, cleaning, pad replacement, human-computer interaction, and equipment communication. The STM32 microcontroller executes grinding and polishing tasks based on instructions from the host computer while dynamically adjusting PID control parameters using an improved weighted average optimization algorithm. This approach enhances control accuracy, stability, and overall surface treatment quality compared to traditional PID control methods.
Blended metal powders offer a compelling alternative to pre-alloyed powders in metal additive manufacturing by providing access to a wider range of alloy compositions and avoiding the high costs in producing pre-alloyed powders. In this work, a new and crack-free Ti-5AlMnScZrMgSiFe alloy (in wt.%) was manufactured by laser powder bed fusion (L-PBF) from mixed powders to investigate the microstructures, mechanical performance of printed parts. Ti-5 AlMnScZrMgSiFe alloy contains both alpha (α) and alpha prime (α′) phases. Further microstructural characterizations show that the L-PBF Ti-5 AlMnScZrMgSiFe contain dense dislocations and twins formed in additive manufacturing process. The as-printed Ti-5 AlMnScZrMgSiFe alloy exhibits a tensile fracture strength of ~950 MPa with a fracture elongation of ~12.5%. The eye-catching properties are attributed to the dense dislocations, nano-twins and solid-solution strengthening.
Due to their high specific modulus and specific strength, carbon fiber reinforced polymer (CFRP) composites have been widely adopted in the aviation field. However, CFRP components produced by conventional vacuum assisted resin transfer molding (VARTM) often exhibit defects such as Pores and dry spots. To address these limitations, this study develops a large-area, highly uniform vibration-assisted VARTM (UAVR) system and conducts ultrasound-assisted experiments. The results demonstrate that ultrasonic treatment at various frequencies consistently improves moulding uniformity. In particular, when the ultrasound frequency is 22 kHz, the tensile strength increases by up to 13.23%, and the compressive strength increases by up to 8.48%. This study has practical significance for improving the performance of CFRP.
This study prepares high-performance PI/VIP composite thermal insulation materials for buildings by integrating polyimide (PI) composite membranes and vacuum insulation panels (VIPs), and uses EnergyPlus to explore their impacts on building energy conservation, operating costs, and carbon emissions under different climates. Experimental results show the materials have low thermal conductivity, long service life, and excellent thermal insulation and flame-retardant properties due to their internal vacuum structure inhibiting heat transfer. Simulations in Jinan (tropical monsoon), Heilongjiang (cold temperate), and Shenzhen (subtropical humid) climates indicate that compared with traditional XPS and rock wool boards, buildings using PI/VIP composites achieve 21.3%, 34.7%, and 18.9% higher annual energy-saving efficiency respectively, with 27%-41% lower carbon emissions; the most significant effects in Heilongjiang highlight the material’s great promotion potential in severe cold areas.
Cu-Fe alloys exhibit excellent performance, and increasing Fe content reduces costs. However, high-Fe Cu-Fe alloys exhibit limited formability at room temperature, while warm rolling improves their processability. This research investigates the effect of rolling temperature on the microstructural transformations and texture development in the Cu-10Fe alloys. The experimental result is that during cold rolling, the morphology of Fe phases is mainly fibrous. With the rolling temperature rising, the microstructural morphology of Fe phases becomes globular / elliptical. The difference is that with the increase in rolling temperature, the average grain size of the Cu-10Fe alloy first decreases and then increases. The matrix microstructure remains dominated by deformed grains, with significant recovery observed at 500 °C. The Fe-phase microstructure primarily consists of substructured grains, and dynamic recovery intensifies with rising temperature. During cold rolling, high dislocation density and localized strain heterogeneity lead to dispersed texture orientations and low strength. In contrast, warm rolling promotes dislocation climb and dynamic recovery, triggering partial recrystallization. This reduces randomly oriented grains, enhances the strength and continuity of specific textures, and establishes a more concentrated texture distribution. This forms a structure with fine recrystallized grains embedded within deformed grains, exhibiting slightly lower strength than cold-rolled samples but better elongation. These findings reveal the crucial role of deformation temperature in controlling microstructure transformation and texture evolution, especially by regulating the recovery and recrystallization behaviors of Cu-10Fe alloys. The above results hope to provide some theoretical and experimental basis for a new approach to improve processing technologies for new Cu-Fe-based composites.
This Purchasing Specification (PS), AMS3970/3, specifies the batch release and delivery requirements for carbon fiber fabric epoxy prepreg used for repair. This specification is applicable only when the carbon fiber fabric epoxy prepreg is used as part of the repair system defined in AMS3970 and AMS3970/1. This specification also defines the procedure and requirements for storage life extension of materials purchased against this specification. It is only applicable for materials that are qualified against AMS3970 (refer to PRI QPL AMS3970) and shall be carried out within the responsibility of the purchaser and under control of its Quality organization.
This Purchase Specification (PS), AMS3970/5, specifies the batch release and delivery requirements for the companion non-structural glass fiber fabric prepreg. This specification also defines the procedure and requirements for storage life extension of materials purchased against this specification. It is only applicable for materials which are qualified and shall be carried out within the responsibility of the purchaser and under control of its Quality organization.
AMS6885/1 gives information about the technical requirements and qualification procedure for unidirectional carbon fiber tape epoxy repair prepreg capable of curing under vacuum for repair of carbon fiber reinforced epoxy structures. The repair system includes an epoxy film adhesive to be applied in a co-bonding process with the prepreg for solid laminate and sandwich bonding.
The increasing pressure to decarbonize manufacturing systems is pushing industry beyond conventional lightweighting strategies toward material and process paradigms, capable of delivering functional performance with radically lower environmental impact. In this context, polymer-based composite Additive Manufacturing (AM) offers an underexplored yet highly promising pathway for sustainable production of load-bearing components. This study presents a preliminary comparative cradle-to-gate Life Cycle Assessment (LCA) of a Formula SAE brake pedal, assessing the environmental transition from conventional sheet metal fabrication and finishing operations of Aluminum 7075-T6 to additive manufacturing solutions, with specific focus on Carbon-Fiber-Reinforced Polymer (CFRP) composites. Two topology-optimized designs, respectively for Powder Bed Fusion (PBF) in AlSi10Mg and Material Extrusion (MEX) in Polyethylene Terephthalate Glycol with Carbon Fiber (PETG-CF) are compared to conventional fabrication aluminum benchmark. The analysis is integrated in the product and process design following ISO 14040/14044 standards and is implemented using the Environmental Footprint 3.0 methodology within the 3DEXPERIENCE platform. Results outline that Material Extrusion (MEX) composite manufacturing achieves the lowest environmental impact across all evaluated categories. Compared to conventional manufacturing, the PETG-CF solution enables an approximate 50% reduction in Global Warming Potential and an almost complete elimination of mineral depletion. Unlike metal additive manufacturing, which remains constrained by high process energy demand, MEX benefits from low processing temperatures, minimal auxiliary systems, and highly efficient material deposition. Crucially, these sustainability gains are achieved while maintaining functional performance through design-driven topology optimization. AM composite solutions, by merging advanced material science with additive flexibility, may lead to design approaches which cease to be ‘potential’ enablers of sustainable manufacturing for the Industry 5.0 transition.
This research investigates the fabrication and evaluation of Delrin (polyoxymethylene, POM) composites reinforcing 5-20 wt.% chopped ramie fiber (RF). The polymer composites were fabricated via the injection moulding technique. Glass transition temperature (Tg), thermal conductivity, Vicat softening temperature (VST), heat deflection temperature (HDT), melt flow index (MFI), and coefficient of linear thermal expansion (CLTE) were the various thermal characteristics of the sustainable composites that were systematically evaluated as per the ASTM standards. The addition of RF drastically altered the Delrin matrix's performance. Among the formulations, the composite with 15 wt.% RF had the best combination of properties: higher VST and HDT values, which provide greater dimensional stability at high temperatures; lower CLTE, resulting in less thermal expansion; comparatively better thermal conductivity; and improved heat dissipation. Eventually, there was a moderate drop in the MFI, indicating more rigid polymer chains that restrict the flowability of the composite, thereby increasing its heat-withstanding capabilities. DSC analysis revealed a slight upward shift in Tg and increased crystallinity, suggesting restricted polymer chain mobility and enhanced load transfer at 20 wt.% RF loadings, agglomeration effects, and weaker interfacial bonding with the matrix led to deterioration in properties. Aircraft cabin components like interior panels, ducting supports, and lightweight non-structural fittings requires dimensional stability, thermal resistance, and mechanical reliability under fluctuating flight conditions.
For brake and clutch components of aircraft vehicles which require higher mechanical strength and wear resilient, light-weight aluminium composites were developed infusing solid lubricant. In this study, hybrid composites were developed using powder metallurgy route with aluminum alloy AA356 and various amounts of zirconium oxide (ZrO2) (0, 5, 10, 15, and 20 wt.%) as reinforcements. A solid lubricant hexagonal boron nitride (hBN) at a fixed 5 wt.% is considered. Following the appropriate ASTM guidelines, the specimens were mechanically characterized by measuring their density, porosity, micro-hardness, compression strength, impact strength, and flexural strength, among other properties. The findings showed that the composites' mechanical and physical behaviour were greatly affected by the inclusion of ZrO2. Porosity increased as a result of particle clustering and interfacial voids, while density increased gradually as ceramic content increased. Consistently increasing ZrO2 addition led to micro-hardness improvements; at 20 wt.% reinforcement, values reached their maximum, indicating that the hard ceramic phase contributed to better surface resistance. The best balance between particle reinforcement and matrix continuity was suggested by the compression and flexural strengths peaking at 15 wt.% ZrO2. However, when the addition was raised to 20 wt.%, brittleness and porosity began to marginally deteriorate. Unreinforced and lower ZrO2 composites had superior toughness in impact, whereas materials with a higher content had a poorer energy absorption capacity. The 5 wt.% hBN improved fracture arresting capabilities and helped load transmission over the interface. Inclusion of hBN provides solid-lubricating tribofilm formation that enhances the tribological performance. This study reveals that AA356/ZrO2-hBN hybrid composites have good hardness and compressive strength improvements, with 15 wt.% ZrO2 being the best composition with good strength, toughness, and wear resistance.
Porosity in carbon fibre reinforced polymers (CFRP) remains a critical concern for aerospace engineers, as even minor voids introduced during manufacturing can undermine the reliability of structural components. This work explores the influence of Interply porosity on composite panel behavior, employing a multiscale simulation approach that bridges material characterization and full-scale structural analysis. The study begins with virtual coupon testing using Digimat-VA and Digimat-MF, enabling the prediction of material allowable and the assessment of defect variability. Homogenized material properties derived from these simulations are then applied to detailed panel models constructed in MSC Apex, ensuring accurate representation of layup and orthotropic behavior. The workflow can support a range of structural load cases, allowing for the evaluation of stiffness, buckling, or other relevant scenarios as dictated by aerospace certification requirements. Nonlinear finite element analysis is performed in SOL400, comparing pristine panels with those containing a defined level of porosity. The results highlight a marked reduction in stiffness and strength for porosity-affected panels, underscoring the importance of defect control in both design and manufacturing. The approach demonstrates how advanced digital tools can accelerate the assessment of damage tolerance, reduce reliance on physical testing, and support the certification process. By integrating virtual materials laboratory capabilities with robust structural simulation, this methodology offers a practical framework for understanding and mitigating the risks associated with manufacturing defects in aerospace composites. The findings are directly relevant to engineers seeking to optimize composite structures for safety, performance, and regulatory compliance.
Carbon fiber has become indispensable in high-performance industries such as automotive engineering and aerospace. It’s lightweight, extremely durable, and can be shaped in almost any way. The start-up Blackwave, founded at the Technical University of Munich (TUM), specializes in this versatile composite material. What began with custom components for sports cars and aircraft has evolved into the development of high-pressure tanks for space applications.
Researchers from CompPair and the European Space Agency have developed a new composite material for spacecraft with an embedded healing agent. European Space Agency, Paris, France Healable spacecraft structures could soon be possible thanks to cutting-edge composite technology. Swiss companies CompPair and CSEM, and Belgian company Com&Sens have partnered with the European Space Agency (ESA) to modify their self-healing carbon fiber product for use in space transportation. Project Cassandra - an abbreviation for Composite Autonomous Sensing and Repair - includes sensors and a heating element within a composite carbon-fiber material, allowing spacecraft to autonomously repair initial stages of damage.
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