Browse Topic: Coatings, colorants, and finishes

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Biomanufacturing uses microorganisms to produce chemicals or materials of interest, much like a brewery uses fermentation by yeast to produce the alcohol in beer. Biomanufacturing relies upon synthetic biology to reprogram yeast or other microorganisms to produce something of greater value, such as fuel, food, or pharmaceuticals. Industrial biomanufacturing has made significant advances and the products it can deliver include reactive coatings and textiles, sensors, optical materials that can bend light, and new therapeutics such as antimicrobials and vaccines. The convergence of synthetic biology, robotics, and artificial intelligence is opening the way to produce materials never before possible in the commercial market. These same technologies create the opportunity for the miniaturization of this technology to fit into ever more compact spaces, bringing forward deployment of these mini-factories closer and closer to the point of need.
Ahern, Brooke, Crumbley, Annie, Walker, Anne, Grodecki, Joseph
G-3, Aerospace Couplings, Fittings, Hose, Tubing Assemblies
Coating the surface of pipelines is one of the most crucial and effective methods for inhibiting corrosion and prolonging the operational lifespan of pipelines. The coating acts as a protective shield that isolates the pipeline metal from external corrosive environments. However, once the coating begins to peel off or deteriorate due to aging, mechanical damage, or environmental factors, the exposed metal surface becomes highly susceptible to corrosion. Statistics indicate that over 50% of external corrosion failures in pipelines are directly associated with coating defects. Despite the critical importance of coating integrity, research on the interaction between surface coatings and nondestructive testing methods—particularly ultrasonic guided wave techniques—has remained relatively limited in recent years. In this study, the impact of surface coatings on the propagation behaviors of ultrasonic guided waves in pipeline systems was systematically investigated. Coal tar pitch, a commonly used and cost-effective coating material, was applied to steel pipeline specimens with varying coating lengths. The attenuation rate of the guided wave signal amplitude was measured under different coating conditions to analyze the relationship between coating parameters and acoustic energy loss. The experimental results reveal that the coating significantly affects guided wave propagation, especially in terms of signal attenuation and boundary reflection. Furthermore, the study reveals that ultrasonical guided waves possess strong sensitivity to coating discontinuities and can accurately locate coating boundaries. These findings confirm the potential of guided wave technology for early detection of coating defects and quantitative evaluation of coating adhesion. Moreover, the outcomes provide useful insight for other transportation and aerospace structures that employ multilayer coatings or protective films, such as aircraft pipelines and composite fuselage components, where similar material interfaces and inspection challenges exist. This research provides theoretical and experimental references for improving the reliability of pipeline health status detection.
Xiao, Tianyi, Li, Bing
P2-type layered oxides are good cathode materials in high-performance sodium-ion batteries since they have desirable two-dimensional ion migration pathways. However, their instability at interfaces and their attenuation as cycles persist also remain a significant challenge. To increase their electrochemical stability, surface coating is also a good plan, but the balance between the coating and ionic conductivity is one of the key challenges. This study constructed an immensely thin layer of alumina (Al2O3) coating, and the influence of the amount of the coating (0.3-1.2 wt percent) on the working of the material was methodically examined. Electrochemical analysis showed that the lowest levels of Al2O3 (0.3 wt) provide the greatest improvement in performance. The optimized sample showed a retention capacity of 96.35 after 100 cycles of operation at 1C, significantly higher compared with samples that had increased coating contents. An analysis of cyclic voltammetry and impedance spectroscopy was subsequently done to corroborate the presence of a 0.3 wt% coating, which infected the electrode-electrolyte interface by inhibiting side reactions but minimally obstructing sodium-ion transport and thus promoting reaction reversibility and improved interfacial kinetics. These results highlight the importance of a less-is-more rule when it comes to surface coating and provide a novel understanding of how long-life sodium-ion battery cathodes can be designed by carefully engineered interfaces.
Hu, Chao, Peng, Rui, Zhou, Yu, Zhou, Dengmei, Tian, Liangliang
Copper red glazes have received considerable attention due to their perfect decorative effects and vivid coloration. This paper selected four different formula copper red glazes with different colors of bright red, violet blue, dark red, and gray blue as the samples. Based on the analysis of the colorimeter, X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), and scanning electron microscope (SEM), a possible coloration mechanism was proposed to explain the variation of glaze colors. The results indicated that the glaze layers were mainly composed of amorphous phases with few quartz diffraction peaks and mainly presented a granulous structure and phase separation. Increasing the content of CaO could cause color changes of the glaze due to the high ionic potential of calcium ions, which could form a unique feature in the glaze melt. In addition, a small amount of calcium phosphate could greatly change the color of the glaze. The phase separation structure of the blue samples was more obvious than that of the red samples, with a phase separation size of less than 100 nm. The formation of droplet phase separation structure in the glaze could lead to Rayleigh scattering and Mie scattering, which made the color of copper red glazes blue and opacified. Increasing the content of Cu0 and decreasing Cu+ could weaken the structural color, which contributes to a* value of the glaze changing from 26.93 to 22.93. At the same content of Cu0, the higher the ratio of Cu+ /Cu2+ is, the less a* value of the glaze is. Finally, the existence of CuSiO3 in the glaze could also make the blue color.
Ding, Erbao, Yang, Mengli, Liu, Nannan, Li, Yabo, Zheng, Ruimiao, Xu, Yan
This study investigates the characterization and dry machining performance of advanced physical vapor deposition (PVD) aluminum titanium nitride (AlTiN) and aluminum chromium titanium nitride (AlCrTiN) coatings deposited using three techniques: cathodic arc evaporation (CAE), high-power impulse magnetron sputtering (HiPIMS), and scalable pulse power plasma (S3p). The coatings were evaluated for thickness, microstructure, surface roughness, coefficient of friction (CoF), adhesion strength, and microhardness. Among the tested coatings, the S3p-deposited AlCrTiN showed the best performance, exhibiting the highest microhardness (40 GPa), the strongest adhesion (108 N), and the lowest CoF (0.25), along with a defect-free microstructure. Under the selected dry turning condition of 150 m/min cutting speed, 0.15 mm/rev feed rate, and 0.7 mm depth of cut, the S3p-deposited AlCrTiN coating achieved a maximum tool life of 10,800 mm, nearly three times higher than the CAE-deposited AlTiN coating. In contrast, CAE coatings showed comparatively lower hardness and weaker adhesion, with minimum values of 25 GPa and 68 N for C1, along with higher CoF values of 0.58–0.60. Furthermore, AlCrTiN coatings produced by HiPIMS and S3p provided 20–30% longer tool life than AlTiN coatings under identical cutting conditions, highlighting the importance of deposition technique.
Sonawane, Gaurav Dinkar
In order to improve the polar adaptability of the submarine, a protective coating was applied to a large surface injection-molded part. The anti-icing characteristics of the protective coating under a low-temperature environment were studied using the protective coating as the research object. The contact angle test, freezing time test, and hydrophobic face ice adhesion test between liquid droplets and coating surfaces at low temperatures were completed by controlling variables.The results showed that temperature had a significant impact on the contact angle, with a decrease of 8% to 11% from 25 °C to 0°C, while the droplet salinity only gave a small effect on the contact angle. The inherent properties of coatings and droplet salinity had a huge impact on the ice adhesion on droplets and freezing time.Under the same droplet salinity, there are significant differences in the time of freezing and ice adhesion of droplets on distinct coating surfaces. However, as the droplet salinity increases from 0‰ to 35‰, the droplets on the protective coating surface freeze more slowly, the time increases by 64.7 seconds, and the ice adhesion decreases by 43.9%.
Feng, Shengyao, Zou, Debo, Guo, Chao, Jiang, Yong, You, Chuang, Lu, Bingju
A team of researchers at the Max Planck Institute for Intelligent Systems (MPI-IS) in Stuttgart developed a biohybrid micro swimmer covered with magnetic material, whose swimming ability is largely unaffected by the coating. The team from the Physical Intelligence Department at MPI-IS published their work in the journal Matter, which covers a wide range of materials science research.
In military and aerospace systems, thin film patterned substrates literally serve as the foundation of some of the most critical electronic assemblies, including radio frequency (RF), microwave, millimeter wave, and high-speed digital circuits. These substrates are typically made by depositing extremely thin layers of conductive and dielectric materials on bases built from materials like alumina, aluminum nitride, quartz, or certain high-performance titanates with various dielectric constants up to a k of 4,000.
Additive manufacturing (AM) processes facilitate the production of components with high geometrical complexity, presenting substantial opportunities for innovation in demanding sectors such as aerospace and biomedical engineering. A significant challenge impeding their broader application is the characteristic surface roughness of as-fabricated parts, which results from the layer-wise construction and the presence of partially melted powder particles. While electrochemical polishing (EP) represents a viable post-processing technique for achieving a smooth surface finish, a comprehensive understanding of how the non-equilibrium microstructures characteristic of AM materials interact with the EP process remains incomplete. This investigation centers on the electrochemical polishing behavior of Ti-6Al-4V alloy fabricated by direct energy deposition (DED), utilizing a sodium chloride-ethylene glycol electrolyte. The findings reveal that the material's distinct engenders anisotropic anodic dissolution. This behavior is attributed to the differential electrochemical potentials among the constituent phases and their crystallographic orientations, which consequently narrows the operational process window for effective, uniform polishing. This preferential dissolution of certain phases results in the formation of a subtle, micro-scale topographical variation that mirrors the orientation of the original columnar grain structure. Notwithstanding this microstructural influence, the EP treatment proved highly successful in refining the surface finish, substantially decreasing the average surface roughness from 0.350 μm to 0.042 μm. Concurrently, the treatment led to a significant enhancement in the alloy's corrosion resistance, attributed to an oxide layer. These findings underscore the critical necessity of accounting for microstructural characteristics when developing optimized electrochemical polishing protocols for additively manufactured components.
He, Hongxi, Wu, Chenxi, Li, Yongjun, Kang, Chengwei
Desulfurization equipment in electric power industry is in a multi-field coupled corrosion environment with high temperature, high humidity, strong acid and solid-containing slurry. The annual direct economic loss of corrosion exceeds 5 billion yuan, and the equipment replacement cycle is only 1.5-2 years. Traditional protective coatings are difficult to meet the needs. The concept of “bionic barrier-intelligent response-in-situ purification” is proposed to construct multifunctional protective coatings: The Langmuir-Blodgett technique was used to alternately assemble MXene nanosheets and polysilazane. Ti-O-Si covalent bonds enhanced the interface bonding, resulting in a coating hardness of 4H and an elongation of 200%. After 1500 hours of extreme environment test, the coating has low weight loss rate, high self-repair and antibacterial rate, and its service life is extended by 8 times. The engineering application makes the maintenance period of desulfurization tower of a 660MW unit extended from 8 months to 6 years, saving 1.2 million yuan annually, and increasing 200,000 yuan annually by recovering H ˇ SO 2. It provides a cross-scale scheme for electric power corrosion protection.
Nie, Pengfei, Gao, Jiangyu, Chen, Wei
The malfunction of the aircraft windshield electric heating system, particularly arc discharge, poses a serious threat to flight safety by causing glass breakage. A systematic study was conducted on the causes and effects of arc faults on windshield structural integrity, employing macroscopic observation, microscopic analysis, and energy dispersive spectroscopy (EDS) following a windshield fracture incident. The results indicate that arc discharge typically occurs at the interface between the heating film busbar and adjacent structures. Localized high temperatures cause the outer glass to fracture, generating radial cracks. The ablation of the busbar silver coating and the carbonization of the PVB interlayer are direct evidence of arc action, whereas the heating wire remains a passive component affected by the high-temperature environment. The fault is primarily attributed to local disbonding at the busbar interface and moisture ingress. Based on the findings, recommendations are proposed for process optimization and inspection method improvement, providing a basis for the safe design and maintenance of windshield structures.
Chen, Li, Feng, Yanpeng, Ding, Keqin
This paper designs and synthesizes a series of high-performance waterborne polyurethane (WPU) laminating adhesives using polyester, polyether polyols and isophorone diisocyanate as the main raw materials. It focuses on exploring the effects of polyol types and R value (the ratio of polyol to isocyanate) on the properties of the adhesives, including emulsion viscosity, solid content, water absorption rate of the adhesive film, mechanical properties, and bonding performance on different substrates. The results show that WPU2 with polycarbonate diol (PCDL) as the polyol has the best water resistance and the highest tensile strength; WPU1 with polytetrahydrofuran (PTMG) as the polyol has the optimal elongation at break and exhibits outstanding bonding performance on the polar substrate PET; the regulation of R value can optimize the bonding performance of the adhesive on the non-polar substrate BOPP. This type of WPU laminating adhesive features low VOC emissions, no benzene-based solvents, excellent flexibility, and good resistance to high and low temperatures. It not only meets the environmental protection and safety requirements in packaging fields such as food and medicine, but also shows potential application value in high-end fields like aerospace interior compounding and lightweight transportation structure bonding. Its performance is highly compatible with the strict requirements for materials in the modern aerospace and transportation industries. The adjustable strong adhesiveness, compliance with strict emission standards, and adaptability to various substrates make it an ideal choice for a new generation of composite manufacturing, especially suitable for industrial fields pursuing reliability, sustainability and high performance.
Wang, Chengming, Yu, Jiacheng, Wang, Huixia, Huang, Yiqiang, Ren, Xiue
Phase angle light scattering (PALS) was chosen to study the charging behaviors of metal oxide SiO2 distributed in nonpolar solvents, including nonionic surfactant, often known as “charge control agents”. Zeta potential was examined systematically in relation to the concentration of Span80 (Sorbitan monooleate) and particle size and concentration. The findings showed that Zeta potential was unaffected by the surfactant concentration of Span80 over the critical micelle concentration (CMC) at various particle concentrations (volume percentages ranging from 10^–4 to 10^–2). Over a considerable range, the charging of the particles was not significantly affected by the particle concentration. Additionally, the particles showed a size-independent zeta potential. A straightforward model based on meanfield Poisson-Boltzmann theory and preferential adsorption was offered to predict SiO2 particles’ charging procedure in Span80-dodecane solution. The experimental data and the simulated findings agreed well. It was shown that the preferential adsorption of micelles that carry a charge is the cause of the charging of the SiO2 particle in Span80-dodecane solution.
Jiang, Liyuan, Chen, Jiayi, Lv, Qunsong, Cao, Huiying
This research demonstrates a facile method for fabricating an anti-icing coating through spray deposition on a metallic substrate. A dual-layer structure was designed to enhance icephobic properties: a primer layer incorporating fluorocarbon resin, butyl acetate, and rod-shaped micrometer-sized metal oxides to establish a secondary roughness morphology, followed by a topcoat composed of butyl acetate and nano-scaled superhydrophobic particles. Evaluation of the coating performance revealed a maximum water contact angle of 171.9°, indicating exceptional hydrophobicity. Furthermore, the coating exhibited notable abrasion resistance and anti-icing capabilities against overlaying ice.
Li, Dongyang, Xu, Zelong, Wu, Jiang, Tong, Wei, Wang, Weiqing, Cong, Rimei, Qian, Jiawei, Qu, Shaohui
Driven by increasing engineering demands, the need for high-performance flexible electronics has surged, accelerating the development of stretchable devices within mechanics. Among multilayer structures, the film/substrate architecture serves as a typical example, and its buckling behavior remains a longstanding focus of mechanical investigation. This work examines how an elastic film bonded to a soft tri-layer substrate loses stability, producing wrinkled surface patterns under compression. We first construct a mechanical model, then derive an analytical expression for the wrinkle amplitude using a force-balance approach, and finally employ finite-element simulations and theoretical comparisons, we systematically explore how the middle layer’s stiffness and thickness jointly govern the onset, wavelength and amplitude of surface buckling, revealing quantitative selection rules that have not previously been reported for tri-layer structures. The results show that the tri-layer film/substrate structure exhibits two instability modes: film-intermediate co-buckling and film-only wrinkling. By simply varying the middle layer’s elastic modulus or its thickness, one can move the structure across the boundary that separates the film-only and bi-layer buckling regimes, providing a direct mechanical selection for on-demand mode. In addition, the wrinkle amplitude increases monotonically with the applied initial strain. Those findings offer a theoretical reference for designing flexible electronics based on film/substrate structures.
Chen, Hao, Zhang, Wulin, Song, Yahui
For the large drive mechanisms of the survey platform, aiming to achieve long-life in-orbit rotation lubrication, a study was conducted on the tribological characteristics of a lubrication solution combining molybdenum disulfide (MoS2) coating with the application of perfluoropolyether (PFPE) greases. Validation tests were carried out under vacuum and high-low temperature environments to evaluate the equivalent in-orbit service life of solid lubrication coatings when used in conjunction with vacuum greases. Additionally, the physical properties of the friction pairs under solid-liquid hybrid lubrication conditions were investigated. Using life components equivalent to the actual product state, vacuum high-low temperature life tests under solid-liquid lubrication conditions have been completed to validate long-life lubrication technology. This holds significant guiding and reference value for the design of subsequent long-life spacecraft.
Fu, Zhibin, Zhang, Kai, Yang, Siqi, Zhu, Jiahao, Qian, Zhiyuan, Ji, Ming, Zhang, Lei, Wang, Zhiyi, Ma, Zhifei
This specification covers a corrosion- and heat-resistant cobalt alloy in the form of bars, forgings, flash-welded rings, and stock for forging or flash-welded rings.
AMS F Corrosion and Heat Resistant Alloys Committee
The impact of a titanium nitride (TiN) coating by the cathodic arc deposition (CAD) technique on a 316L stainless steel (SS) 316L substrate is examined in this experimental work. The X-ray diffraction study showed that TiN made the osbornite phase grow in the coated specimen. The SS 316L sample had a hardness of 217.66 HV, and the samples with CAD coatings were five times harder than the uncoated disc. The wear test was conducted using a pin-on-disc tribometer under dry and wet conditions at loading conditions of 2 N, 4 N, and 6 N with the counterpart of grade 5 titanium alloy (Ti6Al4V). Wear resistance improved significantly, with the wear rate decreasing markedly after coating compared to the uncoated sample. The wear morphology of the wear on the contact surfaces was identified by SEM analysis of the images. The biocompatibility of the ceramic-coated SS 316L sample with the normal cell line was proved by a cell viability test. The demand for SS 316L and the use of CAD coatings to reduce friction and wear in bio-implant applications were the main topics of the current study.
Gopi, R., Devaraju, A., Sivasamy, P., Raju, M.
The development of remote tower systems in aviation and the resurgence of multi-display interfaces and virtual environments have dramatically influenced ATC, increasing both controllers’ visual demands and their ergonomic needs. This study uses the Visual Ergonomics to study the impact of screen luminance level, along with color temperature, on trainees’ visual performance, fatigue, and physical discomfort in the control rooms of the Remote Tower. By combining a simulated remote control system with spectrometer measurements, PVT alertness tests, VMT (Visual Memory Test) measurements, and subjective evaluations, COST B21 can build up a multi-dimensional ergonomic assessment framework. Eight levels of display luminance (and color temperature) were tested, including two illuminance levels (300 lx and 400 lx) and four color temperature ranges (6000 K–9000 K). Using the Analytic Hierarchy Process (AHP), these parameters were assigned weights to derive a Visual Ergonomics (VE) scoring model, and the ideal visual performance was observed at 400 lx illuminance and 8000 K CCT. The results clearly illustrate the significant impact of display parameters on operational performance in remote tower systems and provide both practical data and a theoretical basis for the human factors design and fatigue reduction research on RTSs.
Zhong, Linfeng, Hu, Ruohui, Luo, Peilin, Zuo, Qinghai, Zhong, Qingwei, Ai, Yi
The numerical simulation of the transformation process of multiple droplets into liquid films is a complex problem involving multiphase flow, interface dynamics, and heat and mass transfer. It usually requires the combination of fluid mechanics, interface science, and numerical calculation methods. Based on the smooth particle fluid dynamics method, this paper establishes a multiphase fluid-solid coupling interaction model among droplets, surrounding air and solid walls, and studies the dynamic change process of multiple raindrops dispersed in different grooves. The results show that when the contact Angle is small, the boundaries of multiple raindrops do not come into contact. The multiple raindrops evolve in their respective grooves and eventually form multiple raindrops that approach the steady-state contact Angle. The second situation is that the boundaries of multiple raindrops do not come into contact, the raindrops start to fuse, and multiple raindrops form a larger one. At this point, the contact point of the gas-solid-liquid phase disappears, that is, the "regulating force" of the contact Angle is 0. This paper provides important numerical simulation references for flight safety, aerodynamic performance and anti-icing/de-icing technologies during the flight of aviation aircraft.
Huo, Ye, Chen, Yongheng, Sun, Cunxiang
This specification establishes the procedures used to produce a hard anodic coating on magnesium alloys and the properties of the coating.
AMS B Finishes Processes and Fluids Committee
In this study, high-speed back-illuminated imaging and laser-induced fluorescence (LIF) methods were employed to investigate the impingement behavior of millimeter-sized single isooctane drops on a dry solid wall and various liquid films, including isooctane and glycerol solution films of different concentrations. Various fuel spray impingement scenarios in gasoline direct injection engines were examined. High-speed back-illuminated imaging was primarily used to examine the impact of fuel drops on a dry wall and a fuel film of the same composition as the drops. The LIF method was used to examine the impact of fuel drops on the glycerol solution film, allowing for the distinction between fuel drops and the glycerol solution film. The impingement behavior varied depending on the Weber number of the incident drop and the wall condition. When fuel drops impacted the solid dry wall vertically, they spread into a circular liquid film. The outer edge of the liquid film folded and bulged, and upon reaching the maximum spreading diameter, it maintained equilibrium and did not retract. When isooctane fuel drops impacted the isooctane film, they broke and splashed, with thinner films producing stronger splashes. Additionally, the Weber number of the fuel drops significantly influenced the crown shape and splashing after impact. The impingement behavior of fuel drops on the glycerol solution film was also investigated, focusing on the liquid film morphology after impact. Based on the experimental data, empirical correlations were established between the critical Weber numbers for transitions among different crown morphologies and the dimensionless film thickness under varying film viscosities.
Yang, Tian, Lu, Lili, Guo, Zongwei, Song, Enzhe, Yao, Chong, Ning, Yilin, Ke, Yun
As a contribution to the reduction of greenhouse gas emissions in the transportation sector, the indicated efficiency of SI engines can be increased via thermal swing coatings. Thereby, a decrease in greenhouse gas emissions can be achieved, although not at all operating conditions. Here, the often-observed increased hydrocarbon emission partially overcompensates the reduced wall heat losses. The main root cause is always attributed to the increased surface roughness and porosity, leading to an increased crevice volume. Further investigations were performed at a single-cylinder engine equipped with a FTIR for species analysis of hydrocarbon emissions. A comparison of direct injection and port fuel injection were performed for RON95 E10 and methanol to assess the influence of mixture preparation. 3D CFD was used to additionally investigate the in-cylinder processes. The comparison of port fuel injection and direct injection showed a significant influence on the fuel hydrocarbon emissions for the direct injection when the thermal swing coating was applied. The effect is more pronounced for methanol. For port fuel injection nearly the same or reduced fuel hydrocarbon emissions can be observed. This is mainly attributed to an increased wall film agglomeration at the piston for the thermal swing coating in case of direct injection, which can be observed in 3D CFD. Due to the low thermal effusivity of the coating, the droplet impingement leads to a notable decrease in the surface temperature. This results in lower evaporation of the fuel and a longer droplet lifetime. Consequently, a fuel wall film is still present at top dead center after ignition leading to additional hydrocarbon emissions.
Fischer, Marcus, Pischinger, Stefan
AMS6885/1 gives information about the technical requirements and qualification procedure for unidirectional carbon fiber tape epoxy repair prepreg capable of curing under vacuum for repair of carbon fiber reinforced epoxy structures. The repair system includes an epoxy film adhesive to be applied in a co-bonding process with the prepreg for solid laminate and sandwich bonding.
AMS CACRC Commercial Aircraft Composite Repair Committee
This SAE Aerospace Information Report (AIR) provides descriptions of test methods for determining if an aircraft surface coating of any thickness has adverse effects on aircraft deicing/anti-icing fluids with respect to fluid holdover time performance and aerodynamic performance. Although not the primary mandate of the G-12 Aircraft Ground Deicing Committee, this document also provides descriptions of suggested test methods for evaluating aircraft surface coatings with respect to durability, hardness, weathering, aerodynamic drag, ice adhesion, ice accumulation, contact angle, and thermal conductivity. These additional tests can provide informational data for characterizing the coatings and may be useful to operators when evaluating the coatings.
G-12ADF Aircraft Deicing Fluids
AMS6885/2 gives specific information about the qualification program for unidirectional carbon fiber tape epoxy repair prepreg capable of curing under vacuum for repair of carbon fiber reinforced epoxy structures. The prepreg system shall include an epoxy film adhesive to be applied in a co-bonding process with the prepreg for solid laminate and sandwich bonding.
AMS CACRC Commercial Aircraft Composite Repair Committee
It is known fact that Thermal management systems are essential to the safety, operational efficiency, and structural integrity of present-day commercial aircraft. Very critical insulation and thermal protection materials are utilized across various aircraft zones to mitigate extreme temperature challenges, ranging from cryogenic conditions at high altitude to pyrotechnic conditions at low altitude/ sea level. Some of the examples where specific materials at their functional role are, In engine pylons and nacelles, high temperature alloys such as Titanium and Inconel, along with ceramic Matrix composites (CMCs) serve as firewalls and heat shields, which are designed to contain fires and protect primary structures. In bleed air ducting, fiberglass or silica insulations blankets are employed to prevent thermal degradation of surrounding aluminum and composite components, when air at temperatures above 200 degree C flows. This paper focuses on the critical insulation and thermal protection materials on passenger Egress system utilized to mitigate pyrotechnic events. The focused case study on passenger egress system highlights a unique application of thermal protection. As these system, as mandated by FAA TSO-C69c, must ensure the system remains deployable and structurally stable for at least 90 seconds under intense heat exposure, preserving a workable egress path for passengers. The passenger egress system surface functions as a heat resistance barrier, resisting thermal energy from potential post-crash jet fuel fire. The heat barrier materials are polymer coated with woven nylon, impregnated with a metallic/ Ceramic layer. This study will emphasize how tailored material coating solutions are fundamental to addressing the diverse and extreme thermal demands in aerospace design, directly contributing to passenger’s safety and aircraft survivability.
Govindaraju, Parthasarathy, Nanjundegowda, Harshavardhana
This study systematically evaluated the wear resilient performance of AZ61 magnesium alloy reinforced with 15 wt.% SiC and diverse amounts of multi-walled carbon nanotubes (MWCNTs) under dry sliding circumstances adopting pin-on-disc apparatus (ASTM G99). To identify the influence of factors like sliding speed (SS) (1-3 m/s), axial load (AL) (10-30 N), and MWCNT concentration (0-3 wt.%) that affect tribological performance, experiments were developed using a Central Composite Design (CCD) under Response Surface Methodology (RSM). SEM micrographs revealed a dispersion optimum near 2 wt.% MWCNT, where CNTs anchor to SiC and bridge the α-Mg matrix, while 3 wt.% shows agglomerates and micro-voids. Findings showed that wear loss (WL) and friction coefficient (CoF) was greatly amplified by increasing AL owing to localized heating and contact stresses. A compacted tribolayer was formed by increasing SS, which decreased WL but marginally raised the CoF. At low AL (10 N), SS (2.09 m/s), and 2.12 wt.% MWCNT, the wear resistance was significantly improved by improving load transfer and creating a lubricating carbon-rich coating, resulting in a decreased WL of 0.006 g. The CoF persisted within the range of 0.19 to 0.28. Agglomeration of MWCNTs caused increased WL and CoF when the MWCNT content is increased above 2 wt.%. Worn-surface microscopy at the optimum showed fine wear tracks and a continuous carbon/oxide glaze, evidencing a lubricious CNT-rich third-body film, whereas high AL/low MWCNT produced deep grooves and delamination.
Senthilkumar, N.
Acoustic-induced vibrations pose a significant risk to launch vehicle hardware and payload reliability during critical phases such as lift-off and transonic phase. Reducing such vibrations is especially challenging when the hardware has already been fabricated, limiting the possibility of structural redesign. This study demonstrates a practical post-fabrication solution using a thin viscoelastic polymer coating applied externally to fully assembled hardware. Comprehensive evaluations were conducted using both acoustic testing and Experimental Modal Analysis (EMA) before and after coating application. During acoustic test, a substantial decrease in structure response from 150Hz to 2000Hz, with a reduction of approximately 50% in the grms values was observed for the coated structure demonstrating significant vibration mitigation over a wide frequency range. In contrast, EMA measurements using impact excitation revealed that the response transfer functions did not show a significant reduction within the band considered and modal properties remained largely unchanged upto 200 Hz, indicating that the coating did not significantly alter the structural properties. The apparent enigma calls for a detailed study. A brief overview on the results and the plausible reasons are detailed in the paper. Out of the probable causes, the observed vibration reduction can be primarily attributed to the operational damping and mass addition effects of the PC10 coating. These findings highlight an effective and practical approach for mitigating acoustic-induced vibrations in aerospace structures, with direct application to launch vehicle stages and other aerospace hardware where post-fabrication solutions are critically needed.
Avirah, Nohin K, Panda, Ajay Kumar, Shaikh, Altafhusen
Aerospace and defense systems demand materials capable of maintaining performance under extreme environmental and operational stressors, including wide thermal cycling ranges, exposure to hydrocarbon fuels, vacuum conditions, and repeated mechanical strain. Silicone-based materials have become essential in these environments because they can retain elasticity, stability, and functionality where many traditional materials fail. Silicones are widely used as coatings, adhesives, sealants, and elastomers in aircraft and spacecraft applications. Their chemical structure enables resistance to both high and low temperatures, while also providing durability against solvents and fuels such as jet fuel. In contrast, many conventional elastomers degrade under prolonged thermal exposure or become brittle at cryogenic temperatures.
Using an inexpensive electrode coated with DNA, MIT researchers have designed disposable diagnostics that could be adapted to detect a variety of diseases, including cancer or infectious diseases such as influenza and HIV.
Polyimides are a class of polymers with imide rings in their main chains. They are renowned for their exceptional mechanical properties, high-temperature resistance, low-temperature endurance, and resistance to chemical solvents, which allow for long-term use under harsh medical operating conditions. Consequently, research on polyimide films has garnered widespread attention. In this study, a two-step method was employed to simplify and optimize the preparation process of polyimide. Initially, a polyamic acid (PAA) solution was prepared, and PAA films were fabricated using a spin coater. Subsequently, the films were imidized to obtain polyimide (PI) films. The impact of various parameters, such as spinning speed, layer number, and temperature, on the film-forming properties of polyimide was investigated using the method of controlling variables. The findings indicate that by setting the spin coater parameters to 700 revolutions per minute (r/min) for 90 seconds, followed by a transition to a high speed of 2200 r/min for 210 seconds for spinning the PAA solution, and then subjecting the film to a temperature gradient of 100°C for 1 hour, 150°C for 1 hour, 200°C for 2 hours, and 300°C for 2 hours for imidization, a complete and mechanically robust polyimide film can be produced. The average light transmittance of the film across a wavelength range of 400-2500 nm is 90.46%.
Huang, Jiehao, Xu, Zihui, Zhao, Kaihong, Lin, Qiting, Hu, Wenzhong, Wang, Liying
Live-line operation is a critical technique for maintaining the reliability and continuity of power supply in modern distribution networks. Insulating mats serve as essential protective equipment during such operations by providing both electrical insulation and mechanical shielding. In practical service conditions, insulating mats are subjected to repeated mechanical contact and friction against conductors, metallic fittings, and ground surfaces, which progressively deteriorates their surface integrity and compromises operational safety. Current performance standards for insulating mats emphasize dielectric and tensile properties, while tribological durability remains unaddressed. In this study, an EVA – PA6 composite film fabricated via the tape casting method was selected as the representative outer insulating layer of insulating mats. Reciprocating friction tests were conducted using an SDR339 abrasion tester to evaluate the effects of normal load and sliding speed on wear behavior. The results indicate that wear mass increased monotonically with friction cycles at a given speed, whereas the incremental wear rate gradually decreased due to contact area evolution. A pronounced transition from mild surface abrasion to severe material removal was observed when the applied load reached 5 N, accompanied by surface scratching and exposure of the internal fibrous layer. These findings demonstrate that the wear resistance of the EVA – PA6 composite film is insufficient for long-term service under realistic frictional conditions. The results provide experimental evidence supporting the necessity of incorporating standardized wear resistance evaluation into performance criteria for insulating mats used in live-line operations.
Sun, Xin, Wen, Libin, Kou, Hanpeng
AMS6885/5 is the Material Specification (MS) which defines the requirements of a unidirectional carbon fiber tape epoxy repair prepreg capable of curing under vacuum for repair of carbon fiber reinforced epoxy structures. It also defines the requirements of an epoxy film adhesive to be applied in a co-bonding process with the prepreg for solid laminate and sandwich bonding.
AMS CACRC Commercial Aircraft Composite Repair Committee
This Purchasing Specification, AMS6885/4, specifies the batch release and delivery requirements for film adhesive used for repair. This specification is applicable only when the film adhesive is used as part of the repair system defined in AMS6885 and AMS6885/1. This specification also defines the procedure and requirements for storage life extension of materials purchased against this specification. It is only applicable for materials qualified against AMS6885 (refer to PRI-QPL-AMS6885), and shall be carried out within the responsibility of the purchaser and under control of its Quality organisation.
AMS CACRC Commercial Aircraft Composite Repair Committee
This specification establishes requirements for chrome-free surface pretreatment materials used for surface preparation of metallic surfaces prior to applying organic coatings.
AMS G8 Aerospace Organic Coatings Committee
This test method covers procedures to qualitatively determine the visual and physical condition of a liquid organic coating component (pigmented base, base without pigment, curing solution, or thinner) in a container. Also covered is evaluation of the component container to determine any degradation.
AMS G8 Aerospace Organic Coatings Committee
This standard defines a color index system used by, but not limited to, Government activities in a format suitable for color identification, color selection, color matching, and quality control inspection. It also describes the designation and use of color media that is available to conduct these activities. Use of the color index referenced in this standard is intended to promote standardization and consistency in the color of items produced for Government use. Color media is described as follows: Color Chip Representation, Fan Deck: Suitable for color identification and selection. Color Chip Representation, Color Book: Suitable for color identification and selection. Precise Color Matching, Individual Color Chips: Suitable for color matching and quality control inspection purposes. Precise Color Matching, Set of Color Chips: Suitable for color matching and quality control inspection purposes.
AMS G8 Aerospace Organic Coatings Committee
Cold spray deposition is a kinetic-based deposition method that uses an inert gas flow to accelerate particles, where kinetic energy causes plastic deformation upon impact with a substrate, as discussed in Reference 1. Cold spray has been investigated as a method to deposit metal coatings on polymer-based composites, such as aerospace carbon-fiber-reinforced plastics (CFRP's), as discussed in Reference 2. These methods also exhibit low deposition efficiency (15-45%) as shown in Reference 3. In this work, to achieve high deposition efficiency and create an erosion-resistant coating, we use metal-polymer composite powders for cold spray, to make polymer-on-polymer bonding the dominant and effective bonding mechanism; this method lowers impact velocities relative to pure metal deposition to avoid substrate damage. The polymer can also lower the effect of material mismatch, while the nickel can help enhance the erosion performance of the final coating above that of pure polymer. This paper discusses the development of the cold spray deposition process, sample post-processing, erosion testing, and characterization of the samples. The results validate that this method successfully creates a method of depositing a coating with erosion resistance approaching that of bulk titanium without substrate damage on PEEK substrates. Further work is needed to address the issues with depositing on CF-PEEK substrates.
Fischer, Brandon, Wolfe, Douglas, Ryan, Caillin, DeSalle, Chris, Yamamoto, Namiko
Robust perception systems for autonomous vehicles rely heavily on high-quality, labeled data, particularly in off-road and unstructured environments. However, the performance of the perception model is often degraded by data chaos resulting from limitations in automated segmentation. Foundation models, such as SAM2, while powerful, typically generate masks based on low-level visual cues, including color and texture gradients. In complex off-road scenes, this leads to semantic fragmentation. A single object, like a moss-covered log, can be split into not only dozens of segments for its bark and moss but also hundreds of smaller, meaningless patches based on minor color variations. This paper introduces a context-aware annotation agent to resolve this issue. Our workflow integrates a vision-language model (Florence-2) for scene understanding with a segmentation model (SAM2) for mask generation. Instead of segmenting indiscriminately, our agent leverages Florence-2 to comprehend the image holistically, localizing complete objects. For example, after Florence-2 identifies a ”moss-covered log,” its semantic context guides the generation of masks for the entire entity or meaningful sub-components, such as moss patches and bark, not just fragmented color variations. This initial mask, generated in seconds, provides annotators with an excellent starting point, significantly reducing the manual effort required for vertex-by-vertex outlining. Annotators retain complete editing control, with the ability to adjust polygon vertices for a pixel-perfect mask and features such as drawing a bounding box or sketch to automatically segment an object. This agent provides a framework that utilizes the complementary strengths of scene understanding and segmentation models. Deploying each model for its own specialized task makes it possible to make more consistent, high-quality automotive datasets faster, which speeds up the creation of safer perception systems.
Patil, Ashish, Mikulski, Dariusz, Mwakalonge, Judith, Jia, Yunyi
In the design of Rechargeable Energy Storage System (RESS) structures, including battery trays, module side plates, and end plates, there are multiple conflating factors, including: Mechanical requirements necessitating the use of electrically conductive materials (steel and aluminum); proximity between battery module structure and battery cells, necessitating the use of electrical isolation coatings; and, module and pack designs that retain cells via the use of Structural Adhesive Material (SAM). Inherently, with this design approach, organic coatings are placed in a new and perilous position. In a sense, the coating becomes a supplement to an adhesive. As Computer-Aided Engineering (CAE) virtual analysis tools become more sophisticated, there is increasing reliance on these tools to predict the occurrence of structural failures in various load cases. Factors in test method, paint pretreatment, and topcoat affecting adhesion of organic coatings in structural adhesive joints are discussed, including: Adhesive sample preparation; adhesive selection, coating film pretreatment; age of pretreatment bath; acid cleaning; substrate material type (steel vs. aluminum); substrate product form effects within aluminum, and coating thickness. This information is useful for organic coating process development on metallic substrates. It is especially useful for material constructions requiring paint in contact with structural adhesives, as in these joints, paint adhesion is often a limiting factor on the performance of the structural adhesive. The characterization and optimization of this interface is especially important for EV battery modules & packs.
Moceri, Charles, Harper, Jared
Embedded vision systems are essential for contemporary applications, including robotics, advanced driver assistance systems (ADAS), and intelligent surveillance; yet they frequently experience diminished image quality due to resource constraints, environmental variability, and inconsistent illumination conditions. Such degradations impact multiple visual attributes—sharpness, contrast, color accuracy, noise levels, and structural similarity—that are critical for reliable perception in safety- and performance-driven domains. This study introduces a comprehensive system-level calibration architecture that integrates three coordinated layers: sensor-level adjustment, firmware optimization, and adaptive software enhancements. At the sensor level, exposure control, gain tuning, and white balance adjustments mitigate luminance imbalance and color shifts under changing light conditions. Firmware optimization leverages image signal processor (ISP) parameters to reduce temporal and spatial noise, refine tone mapping, and correct color reproduction through calibrated color correction matrices. Software-level improvements apply adaptive sharpening, contrast enhancement, and gamma correction to maintain visual fidelity across diverse scenes. The proposed pipeline was evaluated on three representative embedded platforms—NVIDIA Jetson Nano, Raspberry Pi 4B, and STM32F7 MCU—covering a range of computational capabilities and power budgets. Experimental results demonstrate substantial improvements in image quality: Peak Signal-to-Noise Ratio (PSNR) increased from 24.2 dB to 31.6 dB in indoor low-light conditions, Structural Similarity Index (SSIM) improved from 0.73 to 0.88 in dynamic scenarios, and color accuracy (ΔE) was reduced to 3.1 in bright outdoor conditions. The complete calibration pipeline sustained real-time responsiveness (< 40 ms/frame) with acceptable power consumption (maximum 172 mW) and memory utilization (peak 35.7 MB). These results validate the modularity, efficiency, and robustness of the proposed method, making it well-suited for deployment in practical embedded vision applications where image quality, latency, and resource constraints must be balanced.
Indrakanti, Rama Kiran Kumar, Vishnoi, Nitin, Kamadi, Venkata
This specification covers the requirements for an inorganic black coating applied at ambient temperature to steel to touch up black oxide coating in areas where the black oxide has been removed. This coating is intended only to visually change the surface to a black color, not to meet the requirements of any black oxide specification.
AMS B Finishes Processes and Fluids Committee
Spectral imaging tools — cameras that capture colors beyond the RGB spectrum visible to our eyes — are vital for gleaning information about an object’s material and structural properties. Marrying them with machine learning has provided a powerful pipeline for identifying features in real-world applications including semiconductor fabrication, pollutant tracking, and crop monitoring.
Five-Axis CNC machines have become essential for creating the complex geometries demanded by industries such as aerospace and defense. These advanced machines offer superior part accessibility and minimize the need for repositioning, enabling shops to eliminate secondary set-ups and post-processing. However, for many machine shops, unlocking the full performance potential of five-axis equipment requires more than sophisticated motion control: it also demands higher spindle speeds. Traditional five-axis machines often top out at spindle speeds between 6,000 and 15,000 RPM. While this is sufficient for heavy roughing operations using large diameter tools, when it comes to finishing intricate features or micro-drilling, small tools require consistent spindle speeds of 40,000 to 90,000 RPM on the toolpath to function effectively. Without that capability, shops risk poor surface finishes, broken tools and unacceptably long cycle times. This is where governed high-speed air-driven spindles offer a transformative upgrade.
Master Bond EP40 is a two-part, room temperature curing epoxy for bonding, sealing, coating, and encapsulating. EP40 bonds well to a variety of substrates, including naval steel, the primary structural metal used in the shipbuilding industry. Master Bond Inc., Hackensack, NJ To reduce its environmental impact and pollution, the shipping industry is investigating methods to construct more lightweight ships. One potential method is using adhesive bonding techniques to replace traditional welding and riveted joints on ships to fabricate lighter ships with smaller carbon footprints. However, adhesives age and deteriorate when exposed to moisture, high temperatures, and ultraviolet light. This makes it necessary to understand how they age in maritime environments to determine whether they can truly replace traditional welding techniques. To this end, researchers at Centro de Investigación en Tecnologías Navales e Industriales (CITENI) and Centro de Investigación TIC (CITIC) developed a new method for studying adhesive aging on naval steel substrates. Master Bond EP40 was selected as the test adhesive for this method due to its strong performance and suitability for marine conditions. By using EP40, the team ensured that the observed adhesive bonding behavior would reflect a high-quality epoxy's potential in ship structures. The goal was to evaluate how EP40 bonds to naval steel and how the bulk epoxy material would behave in seawater to provide insights into the construction of lighter ships using this approach.
Using waste to purify water may sound counterintuitive. But at TU Wien, this is exactly what has now been achieved: a special nanostructure has been developed to filter a widespread class of harmful dyes from water. A crucial component is a material that is considered waste: used cellulose, for example, in the form of cleaning cloths or paper cups. The cellulose is utilized to coat a fine nanofabric to create an efficient filter for polluted water.
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