Browse Topic: Refractory materials

Items (615)
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Zhu, Mayuezhen, Li, Mei, Jiang, Jianwei, Men, Jianbing, Wang, Shuyou
This specification covers a columbium (niobium) alloy in the form of bars, rods, and extrusions.
AMS G Titanium and Refractory Metals Committee
This specification covers a columbium (niobium) alloy in the form of sheet, strip, and plate.
AMS G Titanium and Refractory Metals Committee
This specification covers columbium in the form of sheet, strip, plate, and foil.
AMS G Titanium and Refractory Metals Committee
AE-8C1 Connectors Committee
This specification covers tantalum in the form of sheet, strip, plate, and foil up through 0.1875 inch (4.75 mm), inclusive (see 8.7).
AMS G Titanium and Refractory Metals Committee
A new high-temperature resistant material exhibits great potential for applications such as energy-efficient aircraft turbines. Karlsruhe Institute of Technology, Karlsruhe, Germany A new material might contribute to a reduction of the fossil fuels consumed by aircraft engines and gas turbines in the future. A research team from Karlsruhe Institute of Technology (KIT) has developed a refractory metal-based alloy with properties unparalleled to date. The novel combination of chromium, molybdenum, and silicon is ductile at ambient temperature. With its melting temperature of about 2,000 degrees Celsius, it remains stable even at high temperatures and is at the same time oxidation resistant. The results are published in the journal Nature. High-temperature-resistant metallic materials are required for aircraft engines, gas turbines, X-ray units, and many other technical applications. Refractory metals such as tungsten, molybdenum, and chromium, whose melting points are around or higher than 2,000 degrees Celsius, can be most resistant to high temperatures. Their practical application, however, has limitations: They are brittle at room temperature and, in contact with oxygen, they start to oxidize causing failure within short time already at temperatures of 600 to 700 degrees Celsius. Therefore, they can only be used under technically complex vacuum conditions - for example as X-ray rotating anodes.
This specification covers a corrosion-resistant steel in the form of sheet and strip over 0.005 inch (0.13 mm) in nominal thickness.
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers a corrosion-resistant steel in the form of sheet and strip over 0.005 inch (0.13 mm) in nominal thickness.
AMS F Corrosion and Heat Resistant Alloys Committee
Recent advances in both alloy development and additive manufacturing have enabled the production of ultrahigh-strength steels in nearnet shape parts. Army Research Laboratory, Aberdeen Proving Ground, Maryland Ultrahigh-strength steels are traditionally defined as those steels with a minimum yield strength of approximately 1380 MPa. Notable examples of steels in this category include AISI 4130, AISI 4140, and AISI 4340. In many cases, maximizing the performance of these alloys requires a rather complex approach that involves a series of tempering, annealing, or stress-relieving treatments. As a result, they are produced using a variety of traditional processing methods such as casting, rolling, extrusion, or forging. These traditional methods - combined with the ultrahigh strength of the steels - often meant that the production of complex, near-net shape parts of high quality was quite difficult. In addition, these production methods often entailed repetitive treatments or long production cycles, both of which resulted in elevated production costs. Additive manufacturing (AM, also known as 3D printing) has recently been recognized as a manufacturing method that enables the production of near-net shape parts. In these methods, a complex part is iteratively built in a layer-by-layer process that involves powder deposition followed by selective melting/sintering of the powder to form the part. With the continued development of processing lasers, it is now possible to form fully dense components from a wide range of metals powders, including refractory alloys, steels, and other high-temperature alloys.
When it comes to quantum technology, niobium is making a comeback. For the past 15 years, niobium has been sitting on the bench after experiencing a few mediocre at-bats as a core qubit material. Qubits are the fundamental components of quantum devices. One qubit type relies on superconductivity to process information.
The machining process is employed to transform a workpiece into a predefined geometry with the assistance of a cutting tool. Throughout this process, the cutting tool undergoes various adverse effects, including deformation, stress, thermal gradient, and more, all of which impact tool sharpness, surface finish, and tool life. These outcomes are also influenced by cutting parameters, specifically cutting speed, feed rate, and depth of cut. The present investigation aims to demonstrate the application of ANSYS analysis software in predicting stress, deformation, thermal gradient, and other factors on the tool insert tip for various machining parameters. To achieve this, an experimental setup was arranged to collect cutting force and temperature data using a dynamometer and thermocouples during the machining process of maraging steel with a tungsten carbide tool insert. Experiments were conducted with different combinations of machining parameters using design of experiments (DoE). The measured cutting forces and temperatures for various machining parameters served as input for the analysis of stress, deformation, temperature gradient, and heat flux. The effects of these parameters are tabulated, and inferences are made for optimization.
Balasubramanian, K., Jeyakumar, R., Rajendran, C., Kandavalli, Sumanth Ratna
Super duplex stainless steel (SDSS) is a type of stainless steel made of chromium (Cr), nickel (Ni), and iron (Fe). In the present work, a 1.6 mm wide thin sheet of SDSS is joined using gas tungsten arc welding (GTAW). The ideal parameter for a bead-on-plate trial is found, and 0.216 kJ/mm of heat input is used for welding. As an outcome of the welding heating cycle and subsequent cooling, a microstructural study revealed coarse microstructure in the heat-affected zone and weld zone. The corrosion rate for welded joints is 9.3% higher than the base metal rate. Following the corrosion test, scanning electron microscope (SEM) analysis revealed that the welded joint’s oxide development generated a larger corrosive attack on the weld surface than the base metal surface. The percentages of chromium (12.5%) and molybdenum (24%) in the welded joints are less than those in the base metal of SDSS, as per energy dispersive X-ray (EDX) analysis. Corrosion modeling is done using the COMSOL Multiphysics software. Electrochemical corrosion modeling is used to determine the electrolyte potential (i.e., 0.09 V) and current density (i.e., 0.2 A/m2 to 1.8 A/m2). An entire mesh model contains 6240 elements. The largest and smallest element sizes are 4 mm and 0.1 mm, respectively. The maximum element rate of growth is 1.2.
Kumar, Sujeet, Kumar, Yogesh, E. K., Vimal K.
Solid rods of dissimilar metals are easily welded by friction welding. This process is a solid-state process where no fumes or gases are released which is friendly to the environment. In advanced engineering practice, joining Titanium (Ti) alloy and stainless steel (SS) is very important due to poor bonding strength in direct joining. These materials are easily joined by an interlayer technique using materials like nickel, silver, niobium, aluminum, and copper. Special surface geometry techniques hold the interlayer materials between dissimilar metals in different forms like coating, foils, and solid metals. In this investigation, the finite element method is used for modeling the process, and the Johnson-cook equation was used to find the analysis of output values with the defined material properties. The heat generated is calculated and numerically compared and analyzed with experimental results. Observations such as metallography, hardness, and tensile test were studied. The results are best suitable for the optimization of future design and improvement. It's important to note that while friction welding is a promising option, it's always recommended to perform feasibility studies and conduct tests on representative samples to ensure that the joint's mechanical properties meet the required standards for automobile applications like ball link joint, piston rod, air compressor piston, ball screw, butterfly valve, clutch hub, steering rack gear, trailer axles, etc. A maximum temperature of 11500C was observed at the interface and the highest tensile strength of 348MPa was obtained.
Balasubramanian, M., Prathap, P., Madhu, S.
The main objective of the work is to investigate the friction and wear behavior of sintered copper-based brake composite friction material with a change in the volume percentage of soft reinforcement particles namely MoS2 by pin-on-disc tribometer for medium-duty automotive applications. The composite brake friction material contains copper (Cu) as a matrix, tin (Sn) as an additive, silicon carbide (SiC) and molybdenum disulfide (MoS2) as hard and soft reinforcement particles and barium sulfate (BaSO4) as filler. These hybrids copper-based brake composite friction (pin) samples are successfully prepared by a change in compositions of MoS2 from 0 to 5 vol. % in the step of 1 vol. % and the characterizations of friction samples are studied to understand the physical and mechanical properties such as density, hardness, and compressive strength. Finally, the dry sliding friction and wear test is conducted against grey cast iron material (disc) at constant load and sliding speed of 50 N and 5 m/s respectively using pin-on-disc equipment under room atmosphere. Based on the analysis of the result, the developed copper-based brake composite friction sample with 2 vol. % of MoS2 has shown better mechanical and tribological properties among other compositions. Further, post-test analysis on the worn-out sample surfaces using a field emission scanning electron microscope (FESEM) with energy dispersive spectroscopy (EDS) revealed that change in wear mechanisms from abrasion to adhesion as an increase in the volume percentage of MoS2.
P, Raja, Ramkumar, Penchaliah
High-strength steel has several industrial applications such as automobile, tool and die, construction industries etc. However, it is challenging to achieve it. Various strengthening mechanisms, such as dispersion strengthening, alloying, grain boundary strengthening etc., plays a vital role in deciding the properties of the steel. At the industrial level, high-strength steel is produced by adding alloying elements such as Tungsten, Chromium, and Molybdenum in the steel matrix, increasing the high-strength steel cost. On the other hand, Wire Arc Additive manufacturing (WAAM) can produce dispersion strengthening in steel to mimic the properties of a high-strength steel matrix. The WAAM is a relatively low-cost additive manufacturing technology which uses a welding process to build up layers of material to fabricate the finished product. We have dispersed hard silicon carbide (SiC) particles in the mild steel matrix using the WAAM process in this work. SiC-dispersed steel's hardness is 28% higher than mild steel samples prepared by the WAAM process. The SEM micrograph shows the presence of dispersion of SiC in the steel matrix, which increases hardness compared to mild steel samples.
Natarajan, Harshavardhana, Vincent, Akash
Dissimilar metal welding (DMW) gives a distinctive and complex process because each zone in the different welding area has unique structures and characteristics. The customized weld zone has a unique structure and may have a heating effect on weld metal properties. DMW is used in aerospace, marine, oil refineries, petrochemical industries, power plants including nuclear and other engineering applications due to economic considerations and offered lightweight in design. This paper's main objective is to investigate the microstructure evolution and impact strength of a joint Austenitic AISI 321 plates and Duplex UNS32205 stainless steel welded using pulsed current GTAW (PCGTAW). The base plates were joined by ER2209 filler metal and the microstructure of base and weld metal zones was observed. The selected filler metal was a duplex in nature and contains equal ratio of austenite and ferrite phase in the different weld metal zones of UNS32205 and AISI 321 weldments. The fractography studies of dissimilar joints UNS32205 and AISI 321 were done and investigated through scanning electron microscopic (SEM). Pipe joints in oil and gas and petrochemical industries make use of bimetallic combinations of different stainless steels.
Kumar, S Praveen, Kilari, Naveen
This specification covers engineering requirements for the grinding of tungsten carbide high velocity oxygen/fuel (HVOF) thermal spray coatings applied to high strength steels (220 ksi and above).
AMS B Finishes Processes and Fluids Committee
Aluminum hybrid composites are driving a new trend in metal matrix composites for high strength-to-weight ratio applications such as the automotive industry (piston–cylinder, brakes, shafts), aircraft (engines, airframe), aerospace (space panels), and marine (body frame). Al 6061 is chosen as the matrix for its compatibility and excellent castability in the current work. The reinforcements were silicon carbide (SiC) of size 65μ and tungsten carbide (WC) of 3–5μ due to their enhancing mechanical and corrosion behavior with low density. Composites were prepared through stir casting using different quantities of SiC wt.% 10 and 15, while WC is 0–6% by weight in 2% increments. The results show that mechanical properties such as tensile strength and hardness enhanced due to the gradual strengthening of grains leads to high wear resistance. SEM images of tensile failure show that pits, voids, cracks, burrs, and grain fractures characterize composite failure. Corrosion tests show that the 15% SiC/6% WC composite has higher corrosion resistance than the 10% SiC composite. The corroded surface morphology indicates that the pit size of Al 6061/SiC 15%/WC 0–6% composites decreases with increasing WC weight %.
Pendhota, Vijay, Brahma Raju, K., Ramji, K., Kamaluddin, Syed
This specification covers two types of free-machining, corrosion- and heat-resistant steel in the form of bars, wire, forgings, and forging stock.
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers a corrosion- and heat-resistant nickel alloy in the form of bars and forgings, flash welded rings, and stock for forging or flash welded rings.
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers an aircraft-quality, low-alloy steel in the form of bars, forgings, and forging stock.
AMS E Carbon and Low Alloy Steels Committee
New research suggests that laser-based devices are poised to become a lot smaller. Researchers at Columbia University and Politecnico di Milano studied a 2D material called molybdenum disulfide (MoS2) and characterized how efficiently devices built from stacks of MoS2 less than one micron thick — 100 times thinner than a human hair — convert light frequencies at telecom wavelengths to produce different colors.
This specification covers an aircraft-quality, low-alloy steel in the form of sheet, strip, and plate.
AMS E Carbon and Low Alloy Steels Committee
This specification covers one type of aluminum silicon bronze in the form of rods and bars up to 3.00 inches (76.2 mm), inclusive, in nominal diameter or distance between parallel sides, and forgings and forging stock of any size (see 8.5).
AMS D Nonferrous Alloys Committee
This specification covers a corrosion- and heat-resistant steel in the form of wire 0.010 inch (0.25 mm), up to and including 0.25 inch (6.35 mm).
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers one type of bronze in the form of bars and rods of any size, and tubing over 1.00 inch (25.4 mm) in nominal outer diameter (see 8.5).
AMS D Nonferrous Alloys Committee
This specification covers an aircraft-quality, low-alloy steel in the form of bars, forgings, flash welded rings, and stock for forging or flash welded rings.
AMS E Carbon and Low Alloy Steels Committee
This specification covers established inch/pound manufacturing tolerances applicable to bars and rods of copper and copper alloys ordered to inch/pound dimensions. These tolerances apply to all conditions, unless otherwise noted. The term “exclusive” is used to apply only to the higher figure of a specified range.
AMS D Nonferrous Alloys Committee
This specification covers a silver alloy in the form of wire, rod, sheet, strip, foil, pig, powder, shot, and chips, and a viscous mixture (paste) of powder in a suitable binder.
AMS D Nonferrous Alloys Committee
This specification covers a silver alloy in the form of wire, rod, sheet, strip, foil, pig, powder, shot, and chips and a viscous mixture (paste) of powder in a suitable binder.
AMS D Nonferrous Alloys Committee
This specification covers a corrosion and heat-resistant steel in the form of bars, wire, forgings, mechanical tubing, flash welded rings, and stock for forging or flash welded rings.
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers a special aircraft-quality, low-alloy steel in the form of bars.
AMS E Carbon and Low Alloy Steels Committee
This specification covers a premium aircraft-quality alloy steel in the form of bars and forgings 199 square inches (1284 cm2) and under in cross section, and forging stock of any size.
AMS E Carbon and Low Alloy Steels Committee
"Physical Characterization of Niobium-Added Gray Irons for Brake Disc Applications "132969/14/2022
"High carbon equivalent (CE) gray iron brake rotors exhibit desirable thermal diffusivity and dampening properties. High CE rotors suffer, however, from reduced mechanical and wear properties in comparison to low CE rotors. Niobium (Nb) is shown to increase the strength and wear resistance of gray iron, but the interaction of niobium with other common alloying elements, namely chromium (Cr) and molybdenum (Mo), is not well understood. Thirteen gray cast iron alloys were produced with varying levels of CE, Cr, Mo, and Nb. Bars with four different diameters (8, 14, 22, and 30 mm) were cast from each alloy and microstructural and physical properties such as graphite flake morphology, pearlite spacing, electrical resistivity, and thermal diffusivity were measured. Mechanical characterization, including tensile testing from ambient temperature to 680?C, ambient temperature pearlite microhardness, macro Brinell hardness, and ASTM G65 sand abrasion wear testing, was conducted. Fluidity during casting was measured using a purpose-built finger mold. It was found that niobium refined the graphite morphology, reduced pearlite spacing, and precipitated eutectic NbC. When compared to Mo, Nb was found to be 2-3 times more potent at increasing strength and wear resistance while minimally reducing thermal diffusivity. One of the Nb containing alloys (0.22 wt% Nb) is compared to test data from a modern Chevy Silverado 1500 rotor (similar alloy chemistry excluding Nb addition) and exhibited a 7.8% increase in thermal diffusivity, a 5.8% increase in tensile strength, and a 8.4% increase in hardness while exhibiting similar wear resistance. "
Hasbrouck, Matthew
This specification covers a corrosion- and heat-resistant steel in the form of sheet and strip from 0.0005 to 0.1874 inch (0.013 to 4.760 mm) in thickness.
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers two types of carbon steel in the form of sheet, strip, and plate.
AMS E Carbon and Low Alloy Steels Committee
The element niobium (Nb), a transition metal, stands ready to improve the performance of one of the lithium-ion (Li-ion) battery’s confusing array of possible electrode chemistries — the LTO (lithium titanium oxide) anode, which after graphite is the second most-produced. During battery charging, lithium ions leave the positive cathode and move through the battery’s electrolyte to take up positions of higher energy in the anode. During discharge, this process reverses and drives electrons through an external circuit to power the load.
This specification covers an aircraft-quality, low-alloy steel in the form of heat treated bars and forgings 1.00 inches (25.4 mm) and under in nominal cross section or diameter and for hexagonal shapes, least distance between parallel sides.
AMS E Carbon and Low Alloy Steels Committee
This specification covers a copper-beryllium alloy in the form of mechanical tubing 2 inches (50.8 mm) and under in wall thickness (see 8.8).
AMS D Nonferrous Alloys Committee
This specification covers a corrosion and heat resistant work strengthened nickel alloy in the form of bars and wire, 1½ inches (38 mm) and under in nominal diameter (See 8.2).
AMS F Corrosion and Heat Resistant Alloys Committee
This specification covers a carbon steel in the form of sheet, strip, and plate.
AMS E Carbon and Low Alloy Steels Committee
This specification covers a premium aircraft-quality, low-alloy steel in the form of sheet, strip, and plate.
AMS E Carbon and Low Alloy Steels Committee
Performance evaluation of martensitic press-hardened steels by VDA 238-100 three-point bend testing has become commonplace. Significant influences on bending performance exist from both surface considerations related to both decarburization and substrate-coating interaction and base martensitic steel considerations such as structural heterogeneity, i.e., banding, prior austenite grain size, titanium nitride (TiN) dispersion, mobile hydrogen, and the extent of martensite tempering as result auto-tempering upon quenching or paint baking during vehicle manufacturing. Deconvolution of such effects is challenging in practice, but it is increasingly accepted that surface considerations play an outsized role in bending performance. For specified surface conditions, however, the base steel microstructure can greatly influence bending performance and associated crash ductility to meet safety and mass-efficiency targets. This study reports and elucidates the positive effect of niobium microalloying on bendability of the base PHS alloy through combined structural refinement, microalloy carbide precipitation, and modifications to tempered martensite morphology. Prior austenite grain size refinement due to microalloying results in both incremental strengthening and a reduced solute carbon (C) content in the austenite matrix prior to in-die quenching due to both enhanced segregation of C to austenite grain boundaries. Martensite-start temperature is thusly increased, and a greater degree of auto-tempering results in as-quenched steels. Additionally, the reduction of C content in the as-quenched martensite reduces driving force for oriented transition carbide precipitation during tempering. Measured bend angles are accordingly improved, and reduced strength of martensite, as a result of reduced matrix C, is compensated by the fine dispersion of microalloy carbonitrides. Alloy design and process recommendations are offered based on observed mechanisms.
Enloe, Charles M., Mohrbacher, Hardy
Alumina (Al2O3) thin film coatings are applied on Al alloys using Plasma Electrolytic Oxidation (PEO) method to reduce the wear and corrosion problems. Plasma Electrolytic Aluminating (PEA) is a technique which could generate Alumina coatings on cast iron, mild steel and copper alloys. In this study, the aim is to explore the anti-wear and anti-corrosion behaviours of PEA Alumina coatings on gray cast iron. The dry sliding tribology test data was obtained from Pin-on-Disk (POD) tests against SAE 52100 steel and Tungsten Carbide (WC) counterfaces. Comparing with the PEO Alumina coatings, the PEA Alumina coating has much lower Coefficient of Friction (COF) and less wear. The microstructure, chemical composition and phase composition of this coating were investigated with Scanning Electron Microscope (SEM), Energy-Dispersive X-Ray Spectroscopy (EDX) and X-Ray Diffraction (XRD), respectively. There was FeO (or FeAl2O4) found on the PEA Alumina coating. To figure out the relationship between FeO and the COF, 500 °C heat treatment was conducted on PEA Alumina coated samples, in which FeO could be fully oxidized into Fe2O3 by heat treatments. Differences between unheated and heated samples in chemical composition and wear behaviours were observed. The co-existence of FeO (or FeAl2O4) compounds in PEA Alumina coating is an important factor which introduce relative low COF. The corrosion resistance was evaluated by electrochemical tests. It could be observed and be calculated that the PEA Alumina coated gray cast iron has much better corrosion resistance than uncoated samples. Since the PEA coating can also be applied onto steel materials, the coating technology can be used to protect the hinges of doors and other joint parts from frequent wear and corrosion issues.
Sun, Jiayi, Cai, Ran, Tjong, Jimi, Nie, Xueyuan
In automotive body manufacturing the dies for blanking/trimming/piercing are under most severe loading condition involving high contact stress at high impact loading and large number of cycles. With continuous increase in sheet metal strength, the trim die service life becomes a great concern for industries. In this study, competing trim die manufacturing routes were compared, including die raw materials produced by hot-working (wrought) vs. casting, edge-welding (as repaired condition) vs. bulk base metals (representing new tools), and the heat treatment method by induction hardening vs. furnace through-heating. CaldieTM, a Uddeholm trademarked grade was used as trim die material. The mechanical tests are performed using a WSU developed trimming simulator, with fatigue loading applied at cubic die specimen’s cutting edges through a tungsten carbide rod to accelerate the trim edge damage. The tests are periodically interrupted at specified cycles for measurement of die edge damage. The microstructures from different routes are examined by laser 3D confocal microscopy. The evolution of edge damage projected areas and converted volumes are used, and the fatigue performances of manufacturing routes are compared and ranked. Microstructures from different routes are analyzed for providing metallurgical explanations of mechanical testing results. Directions of further study and trim die reconditioning method for fatigue property improvement are discussed.
Lu, Pengyan, Chen, Xingyu, Yang, Qingyu, Wu, Xin, Miller, Patricia
This specification covers a gold-nickel alloy in the form of wire, rod, sheet, strip, foil, pig, powder, shot, chips, preforms, and a viscous mixture (paste) of the powder in a suitable binder.
AMS F Corrosion and Heat Resistant Alloys Committee
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