Browse Topic: Resins

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Carbon nanotube (CNT) reinforced epoxy nanocomposites were prepared using a solvent-assisted dispersion method and characterized to evaluate their structural, mechanical, and thermal behaviour. X-ray diffraction (XRD) confirmed the presence of CNTs in the polymer matrix through the characteristic (002) reflection, while scanning electron microscopy (SEM) revealed that CNTs were found to be uniformly embedded within the epoxy matrix, showing limited agglomeration and strong interfacial bonding. Fourier-transform infrared spectroscopy (FTIR) supported these observations by revealing absorption bands associated with C=C stretching, C–O–C ether linkages, and O–H vibrations, indicating chemical interactions between CNTs and the epoxy network. Mechanical testing showed that CNT concentrations of 0.25–0.50 wt.% provided the most effective reinforcement, with notable and measurable improvements in tensile and compressive strength as well as modulus. At higher CNT loadings, however, agglomeration led to reduced tensile performance, despite compressive strength remaining comparatively stable. Thermal conductivity increased steadily with CNT addition, from 0.2143 W/m.K for neat epoxy to 0.2435 W/m.K at 0.75–1.00 wt.%, with the most pronounced improvements observed above 0.25 wt.% due to the formation of more efficient conductive pathways. Overall, these findings suggest that low-to-intermediate CNT loadings achieve a practical and useful balance between strength and thermal conductivity while avoiding the drawbacks of excessive filler content. Effective dispersion of nanotubes is a critical factor that governs the mechanical and thermal behaviour of the composites. These results indicate that CNT/epoxy nanocomposites produced under optimized conditions can serve as lightweight, mechanically reliable, and thermally stable materials, making them attractive candidates for advanced applications in aerospace, automotive, and energy-related sectors where both structural performance and efficient thermal management are required.
Gul, AysenurKamali, Ali Reza
This research demonstrates a facile method for fabricating an anti-icing coating through spray deposition on a metallic substrate. A dual-layer structure was designed to enhance icephobic properties: a primer layer incorporating fluorocarbon resin, butyl acetate, and rod-shaped micrometer-sized metal oxides to establish a secondary roughness morphology, followed by a topcoat composed of butyl acetate and nano-scaled superhydrophobic particles. Evaluation of the coating performance revealed a maximum water contact angle of 171.9°, indicating exceptional hydrophobicity. Furthermore, the coating exhibited notable abrasion resistance and anti-icing capabilities against overlaying ice.
Li, DongyangXu, ZelongWu, JiangTong, WeiWang, WeiqingCong, RimeiQian, JiaweiQu, Shaohui
In this study, five resin-based brake pad samples with modified fly ash contents of 0%, 4%, 8%, 12%, and 16% were prepared to investigate the influence of fly ash content on the comprehensive performance of the friction materials. The tribological properties of all samples were evaluated under temperature conditions ranging from 100 °C to 350 °C, and their overall performance was assessed using five evaluation indices. Based on the AHP-MOORA algorithm, sample F12 exhibited the highest comprehensive weighted score of 0.11, followed by samples F0 and F8 with scores of 0.10 and 0.09, respectively, indicating a slight decline. In contrast, the comprehensive weighted scores of F4 and F16 were relatively low, at 0.05 and −0.01, respectively. Among the five composites, F12 demonstrated the best overall performance, with F0 and F8 ranking next, while F4 and F16 performed poorly. These results suggest that, within a certain range, increasing the fly ash content can enhance the comprehensive properties of the material. However, excessive addition of fly ash may lead to the detachment of harder particles during wear, thereby increasing wear thickness and wear rate.
Li, XiaobiaoHe, KangZhao, ZhuanzheWu, BoSun, Fei
This study investigates the structural improvement of recycled carbon fibre composites through hybridisation with continuous flax fibres to address sustainability concerns and performance limitations. Recycled carbon fibres, while environmentally beneficial, suffer from short, randomized orientations and lower mechanical properties limiting their application beyond decorative uses. This research explores whether incorporating unidirectional flax fibres can enhance rCF behaviour for structural applications. Six hybrid composite layup variants and two plain composites were manufactured using cold compression moulding with Ampro Bio Resin. Each hybrid configuration comprised eight layers, divided into four layers of recycled carbon and four layers of flax fibres oriented at 0°. Complete mechanical characterization was performed following ISO standards for tensile (ISO 527), flexural (ISO 178), and impact (ISO 179) testing. Results demonstrated significant performance improvements in hybrid composites. Among hybrids, layup 2 achieved 212.5 MPa tensile strength whilst layup 3 managed to achieve 20.5 GPa in stiffness. Flexural testing revealed layup 6 achieved the highest flexural modulus of 19.6 GPa among hybrids. Impact resistance improved dramatically with layup 3 demonstrating 186% improvement in energy absorption over recycled carbon fibre. The study confirms that hybridisation creates a positive effect, producing more predictable and durable materials. The complementary behaviour between brittle and ductile materials enhances damage tolerance and structural integrity, establishing a foundation for sustainable engineering materials suitable for automotive applications without compromising reliability.
Hnatyk, DawidChrysanthou, AndreasDe Vuyst, TomIsmail, Sikiru
This SAE Aerospace Recommended Practice (ARP) describes and gives general guidelines on use and applicability of standard methods for impregnating dry fabric and lay-up of the impregnated plies. The methods of impregnating dry fabric and ply lay-up described in this document have specific application and are not interchangeable. The methods should only be used when specified in an approved repair procedure or with the agreement of the Original Equipment Manufacturer (OEM) or regulatory authority.
AMS CACRC Commercial Aircraft Composite Repair Committee
This SAE Aerospace Recommended Practice (ARP) describes standard methods of heat application to cure thermosetting resins for commercial aircraft composite repairs. The methods described in this document shall only be used when specified in an approved repair document or with the agreement of the Original Equipment Manufacturer (OEM) or regulatory authority.
AMS CACRC Commercial Aircraft Composite Repair Committee
This paper investigates the feasibility of using flax fiber-reinforced composites in combination with additively manufactured polymer cores for helicopter rotor blades. A new rotor blade with flax composite spar and skin laminates and a 3D-printed ASA Aero core was designed to be geometrically equivalent to an existing carbon fiber/foam reference blade of the MERIT rotor test rig and manufactured using identical tooling. Material characterization included compression testing of the printed core at ambient and elevated temperatures, single-lap shear adhesion testing with epoxy laminates, and hygroscopic conditioning of core and laminate specimens. Structural testing comprised static beam bending, experimental modal analysis with axial pre-loading to approximate centrifugal stiffening, and sustained-load creep and recovery testing of the flax blade. The results show that the 3D-printed core provides sufficient compressive stiffness at curing temperature and adhesion to epoxy laminates, enabling its use as an internal consolidation tool during blade manufacturing. Compared to the carbon reference blade, the flax/3D blade exhibits reduced flapwise and lead–lag bending stiffness, altered modal behavior, and pronounced viscoelastic effects, including creep, incomplete recovery, and strong hygroscopic swelling. Component-level hygroscopic tests reveal that moisture-induced mass and thickness changes can generate sufficient internal stresses to locally initiate structural damage. Overall, the study identifies key limitations and design considerations for applying flax fiber composites in primary rotor blade structures.
Gaugelhofer, LukasYavrucuk, Ilkay
Is there a way to stick hard and soft materials together without any tape, glue, or epoxy? A new study published in ACS Central Science shows that applying a small voltage to certain objects forms chemical bonds that securely link the objects together. Reversing the direction of electron flow easily separates the two materials. This electroadhesion effect could help create biohybrid robots, improve biomedical implants, and enable new battery technologies.
Materials can exhibit significantly different mechanical behaviors compared to quasi-static conditions at high strain rates (> 100 s-1). High strain rate tests using setups such as SHPB (Split-Hopkinson Pressure Bar) can provide, in a practicable manner, the stress-strain relations for a material at high strain rates. Such properties are vitally needed for activities such as simulation-driven impact safety design of composite structures deployed in the form of automotive body parts and assembly, and other sub-systems. Although the behaviors of isotropic and ductile materials such as various metallic alloys appear to have been extensively studied and reported in literature, dependence of mechanical properties of fiber-reinforced composites especially in different off-axis directions are extremely difficult to come across. To fill up this void, a detailed experimental study has been carried out on high strain rate mechanical characterization of a laminated orthotropic glass/epoxy composite using an in-house SHPB powered by a compressed gas gun and equipped with a high speed DAQ (data acquisition) system. A unique feature of the current study is the reporting of stress-strain curves at high strain rates when specimens are loaded in off-axis directions i.e. at angles to the principal direction (viz. 0°, 15°, 30°, etc.). The results highlight the substantive effect of strain rate on properties such as failure strength of the considered composite, and its visibly distinct behaviors in various off-axis loading directions.
Bawa, PrashantDeb, AnindyaBarui, AnanyaZhu, Feng
This paper presents a simplified approach to model thermal runaway propagation in a multi-cell battery pack, with the goal of designing a safe and lightweight pack for mass-sensitive applications. The key parameters which characterize single-cell thermal runaway, including heat release profile, apparent cell emissivity and mass loss, were extracted from empirical nail penetration tests. This characterization was used to drive a three-dimensional thermal model of a 19-cell hexagonal sub-pack with a center trigger cell. To enable rapid design exploration, a symmetry-based computationally simplified domain was used for a full-factorial Design of Experiments (DOE) varying cell spacing, epoxy thickness, heat spreader thickness, and cup geometry. The DOE results were used to identify dominant heat-transfer mechanisms, capture main and interaction effects, and determine mass-efficient design levers governing peak-neighbor cell temperature during propagation. Insights from the DOE study informed the design of a physical prototype and the placement of thermocouples for model validation. Measured temperature data showed good agreement with model predictions across multiple initiator locations, with 4–7 °C error in peak temperature and 3–5 s error in time to reach peak temperature. However, accurate reproduction of the observed trends required increasing epoxy thermal conductivity on the initiator cell to represent epoxy carbonization observed during post-test teardown. This simplified modeling approach, paired with targeted testing, can provide practical design guidance, reduce overall testing cost, and enable fast development of mass-optimized, propagation-resistant battery packs.
Kalyankar, ApoorvOwen, ElliotStrohmaier, KyleMardall, Joseph
Demand for cost-effective automotive traction inverters requires improved power module packaging. This paper presents a packaging method using an epoxy composite insulator applied directly to the cold plate surface, replacing Direct Bonded Copper (DBC) and Active Metal Brazed (AMB) substrates. This integration removes the substrate-to-cold plate solder interface and eliminates two material layers from the thermal path. The epoxy composite demonstrates a dielectric strength greater than 60 kV/mm. Thermal resistance (junction-to-coolant) measured approximately 0.17 K∙cm2/W. Electrical characterization showed a relative permittivity of 3.9, which is lower than standard ceramics and results in reduced parasitic capacitance. Initial thermal cycling tests indicated no significant degradation in thermal or electrical performance. These results suggest the epoxy composite insulator could be a promising alternative for traction power modules.
Chen, YuMena-Garcia, JavierChen, HaoXiao, KeweiGupta, Man PrakashDegner, Michael
To reduce its environmental impact and pollution, the shipping industry is investigating methods to construct more lightweight ships. One potential method is using adhesive bonding techniques to replace traditional welding and riveted joints on ships to fabricate lighter ships with smaller carbon footprints. However, adhesives age and deteriorate when exposed to moisture, high temperatures, and ultraviolet light. This makes it necessary to understand how they age in maritime environments to determine whether they can truly replace traditional welding techniques.
Master Bond EP40 is a two-part, room temperature curing epoxy for bonding, sealing, coating, and encapsulating. EP40 bonds well to a variety of substrates, including naval steel, the primary structural metal used in the shipbuilding industry. Master Bond Inc., Hackensack, NJ To reduce its environmental impact and pollution, the shipping industry is investigating methods to construct more lightweight ships. One potential method is using adhesive bonding techniques to replace traditional welding and riveted joints on ships to fabricate lighter ships with smaller carbon footprints. However, adhesives age and deteriorate when exposed to moisture, high temperatures, and ultraviolet light. This makes it necessary to understand how they age in maritime environments to determine whether they can truly replace traditional welding techniques. To this end, researchers at Centro de Investigación en Tecnologías Navales e Industriales (CITENI) and Centro de Investigación TIC (CITIC) developed a new method for studying adhesive aging on naval steel substrates. Master Bond EP40 was selected as the test adhesive for this method due to its strong performance and suitability for marine conditions. By using EP40, the team ensured that the observed adhesive bonding behavior would reflect a high-quality epoxy's potential in ship structures. The goal was to evaluate how EP40 bonds to naval steel and how the bulk epoxy material would behave in seawater to provide insights into the construction of lighter ships using this approach.
This study focuses on the vibration analysis of hybrid composite laminated plates fabricated from E-glass Fiber and areca Fiber reinforced with epoxy resin. The hybrid laminates were prepared using the Vacuum Assisted Resin Transfer Moulding (VARTM) process with different stacking sequences and Fiber ratios, where brake lining powder was also incorporated as a filler in selected configurations to enhance mechanical and damping properties. The fabricated plates (280 × 280 mm) were subjected to experimental modal analysis using an impact hammer and accelerometer setup, with data acquisition carried out through DEWESoft software. Natural frequencies and damping ratios were determined under three boundary conditions (C- C-C-C, C-F-C-F, and C-F-F-F). The results revealed that Plate 1, with E-glass outer layers, areca reinforcement, and filler addition, exhibited the best vibration performance, achieving a maximum natural frequency of 332.8 Hz under C-C-C-C condition, while Plate 2 showed a balanced response and Plate 3 demonstrated higher stiffness but lower damping capability. These findings suggest that incorporating areca Fiber in combination with E-glass not only reduces weight but also improves damping without significantly compromising structural integrity. The developed hybrid composites hold strong potential for lightweight, vibration-sensitive applications such as automotive interiors, marine structures, construction panels, and sports equipment, where both sustainability and performance are critical.
D R, RajkumarO, Vivin LeninR, SaktheevelR G, Ajay KrishnaNg, Bhavan
Polymer composites with the addition of natural fibers have gained prominence as a sustainable and technically viable alternative to conventional synthetic materials, especially in applications that require a balance between mechanical performance and environmental responsibility. This study evaluated the mechanical behavior of composites produced with plant fibers from banana (Musa sapientum) and sugarcane (Saccharum officinarum L.), both sourced from the northern region of Brazil. The fibers, used in their natural state without chemical treatment, were cut to a uniform length of 5 mm for standardization. The polymer matrix used was unsaturated terephthalic polyester resin, pre-accelerated and catalyzed with methyl ethyl ketone peroxide (MEKP). The molding of test samples was performed manually in silicone molds, according to ASTM D638 specifications, to ensure repeatability and comparability of results. The mechanical tests revealed that the composites made with sugarcane fibers had an average tensile strength of 17.05 (±1.41) MPa, while those with banana fibers reached 28.85 (±0.94) MPa, compared to 26.94 (±4.60) MPa for the pure polymer matrix. These values indicate that the addition of sugarcane fibers resulted in an approximate 36.7% reduction in tensile strength, whereas the use of banana fibers led to an increase of about 7.1% in this property. The results demonstrate the potential of natural fibers added to polymer composites, especially banana fibers, which acted as reinforcement of the matrix, proving to be a technically efficient and environmentally promising alternative for applications in engineering materials.
Santos Borges, LarissaDias, Roberto Yuri CostaBrandao, Leonardo William MacedoMendonca Maia, Pedro VictorSilva de Mendonça, Alian GomesFujiyama, Roberto Tetsuo
Brazil is recognized for its vast biodiversity and abundance of natural resources, many of which are still underutilized. In an effort to promote sustainability and innovation, there is a growing movement to replace non-recyclable materials with ecological alternatives. Within this context, acai leaves (Euterpe oleracea Mart.) and coconut leaves (Cocos nucifera L.) appear as potential natural reinforcements in polymer composites. This study aims to evaluate the mechanical properties of composites formed by these sheets, using polyester resin as the matrix phase. Tensile strength tests were conducted on specimens, following the ASTM D 638M standard, to determine the mechanical properties of the composites. The results obtained were compared with data from the existing literature in order to validate the effectiveness of the composites produced. Additionally, fractures in the specimens were visually analyzed for a better understanding of the failure mechanisms.
Dias, Roberto Yuri CostaSantos Borges, LarissaBrandao, Leonardo William MacedoMendonca Maia, Pedro VictorSilva de Mendonça, Alian GomesFujiyama, Roberto Tetsuo
There is a growing demand for new materials that meet mechanical and structural performance requirements, with specific properties, especially in the automotive industry. From a context of innovation and global needs to be met, there is the appreciation of composite materials, specifically applied in the automotive sector, since these can be obtained from the combination of two or more different materials, obtaining certain properties from the individual characteristics of its phases, expanding the availability of materials to be used in this sector. In recent years the use of natural fibers in composite materials for automotive applications has gained relevance due to factors such as sustainability, low weight and good mechanical properties. The attempt to combine innovation and environmental preservation make such applications promising, aiming to obtain ecological solutions, considering that natural fibers of vegetable origin such as sisal, jute and flax are biodegradable and renewable, being an environmentally friendly alternative compared to synthetic fibers such as glass and carbon. Sisal fiber, for example, is already used in coatings, interior panels and car sound insulation. Therefore, the present work aims to present a review about the general panorama of the use of natural fibers and composites reinforced by such fibers at national level in the automotive sector. For this, will be cataloged articles, dissertations, course completion work etc. for the interval of 2014 to 2025, which are related to this theme, from university libraries, academic platforms or directly in journals dedicated to engineering among other sources of information, being presented the main thermoplastic and thermofix matrices used, such as polypropylene, polyester and epoxy, in addition, the presentation of natural fibers found in Brazil, such as jute, sisal, coconut and curaua. In addition, attending conferences and symposia in the area can provide updated and relevant information to present the main applications, research and trends on the subject. Thus, research on the use of natural fibers in the automotive industry is growing, reflecting the increased demand for more sustainable solutions.
Dias, Roberto Yuri CostaSantos Borges, Larissa dosBrandao, Leonardo William MacedoMendonca Maia, Pedro Victor deSilva de Mendonça, Alian Gomes daFujiyama, Roberto Tetsuo
This specification and part standard specifies polytetrafluoroethylene (PTFE) resin material and the dimensional requirements for scarf-cut retainers (backup rings) previously specified by MIL-R-8791 and MIL-R-8791/1. The retainers are intended for use in hydraulic and pneumatic system components as anti-extrusion devices in conjunction with seals and O-rings.
A-6C2 Seals Committee
This specification establishes the requirements for a waterborne, corrosion-inhibiting, chemical- and solvent-resistant, anodic electrodeposition epoxy primer capable of curing at 200 to 210 °F (93 to 99 °C).
AMS G8 Aerospace Organic Coatings Committee
Stretch broken carbon fiber (SBCF) offers enhanced formability as compared to continuous carbon fiber (CCF). However, robust, quantitative evaluation of forming defects remains a challenge. This study introduces a unified formability index (UFI) that integrates multiple defect types, including texture anomalies, bridging, wrinkling, thickness variation, spring-back, and resin distribution variation (RDV), into a single weighted score. Each defect is ranked on a scale of 0-5 using normalized metrics with a tunable parameter, α, allowing users to balance defect magnitude and frequency as desired. The full scoring pipeline is demonstrated for texture defects using measured data, while normalized legacy scores from previous work are used for non-texture defects to enable complete formability index computation. Case studies on three laminates illustrate how variations in α affect both texture scoring and the overall formability index and demonstrate the geometry-agnostic nature of the updated ranking and UFI systems. This framework maintains compatibility with existing evaluations while offering improved resolution, consistency, and scalability for assessing laminate quality across complex geometries.
Williams, CooperRyan, CecilyCairns, DouglasRidgard, ChristopherNelson, Jared
Plastic waste, in the past few years, has risen to be one of the most concerning and endangering pollutants to environment and life, making its effective management and reduction a major domain of focus among researchers and industrialists. This comparative study is an attempt to utilize recycled Polyethylene Terephthalate (rPET) fibres combined with Epoxy Resin in various combinations, to provide effective and low-cost insulation in moderate to low requirements. The above-mentioned components serve as viable insulators. Moisture resistance of both materials and temperature resistance of Epoxy resins ranging from 120°C to 150°C (depending upon the grade of Epoxy used) indicate a good stability in harsh external operating environment. While Epoxy resins are not inherently flame retardants, additives are introduced for this purpose in order to render the composite safer to use. Owing to the excellent adhesive properties of the Epoxy resin, the rPET fibres are allowed to bond together firmly and also exhibit good overall strength of the composite and also making sure that the composite will not delaminate or weaken over time. Controlled environmental experiments and mathematical modelling of the real-life conditions have been performed. As a part of this study, multiple configurations of the mentioned composite have been tested experimentally and simulatively with varying overall thickness ranging from 3mm to 15mm. Results show temperature difference of about 12°C, indicating that the composites developed can be used as effective thermal insulators.
Purihella, Sri Sai KrishnaPali, Harveer SinghKumar, PiyushSharma, Ved Prakash
3D-printed microscopic particles, so small that to the naked eye they look like dust, have applications in drug and vaccine delivery, microelectronics, microfluidics, and abrasives for intricate manufacturing. However, the need for precise coordination between light delivery, stage movement, and resin properties makes scalable fabrication of such custom microscale particles challenging. Now, researchers at Stanford University have introduced a more efficient processing technique that can print up to 1 million highly detailed and customizable microscale particles a day.
The research project focused on investigating the mechanical, thermal, and chemical properties of composite plates made from bamboo leaves and coconut leaves reinforced with epoxy resin that has received limited attention in previous studies. The bamboo and coconut leaves underwent alkaline treatment, were thoroughly washed with distilled water, and dried in sunlight for 24 hours. For the fabrication of three composite plates, Hand lay up method was employed according to the American Society for Testing and Materials (ASTM) standards. The compositions of the composite plates were varied as first Composition has 25 wt% bamboo leaves, 25 wt% coconut leaves and 50 wt% resin, the Second Composition has 30 wt% bamboo leaves, 30 wt% coconut leaves, and 40 wt% resin and the third composition has 35 wt% bamboo leaves, 35 wt% coconut leaves, and 30 wt% resin. Tensile test, shear and flexural tests helped determine the tensile strength, shear strength, and flexural strength of the composite materials. Additionally, Thermo- gravimetric analysis (TGA) was performed according to ASTM E- 1131 to assess the degradation temperature of the composite plates. Additionally, Fourier-transform infrared spectroscopy (FTIR) tests were also conducted to identify the functional groups of the organic materials present with in the composite plates. The outcomes of this research are anticipated to contribute to a more sustainable utilization of waste bamboo and coconut leaves.
D R, RajkumarO, Vivin LeninR, SaktheevelS, Edwin Roshan
Natural fiber composites (NFC’s) have considerable promise for a wide range of technological applications due to their exceptional features, which include notable weight reduction, high strength, and affordability. The aforementioned materials are also biodegradable and sustainable, which makes them appealing for use in sustainable engineering methods. This research focuses on evaluating the mechanical features of jute fiber and Al₂O₃ particle fortified polymer composites, exploring their potential for advanced engineering uses. The Taguchi technique is used with a L9 orthogonal array, integrating three-level, three-parameter approach, to systematically examine potential combinations of process variables in the manufacturing of these polymer composites. The primary goal is to optimize the mechanical attributes of the composites, which include tensile modulus, tensile stress, and weight percentage increase. Detailed investigations are conducted to interpret the effects of these process factors on the performance metrics. The research employs ANOVA and regression evaluation to assess the pertinence of process factors on the individual output variables. Furthermore, interaction assessment is carried out to discover the implications of the impact of interactions among the process factors on the intended performance measures. To examine the multi-performance index, Grey analysis is used to establish the Grey Relational Coefficient (GRC) values, which provide a comprehensive performance assessment. The resulting composite materials demonstrate considerable potential for application in interior automotive components, such as dashboards and luggage compartments, due to their enhanced mechanical properties and environmental benefits.
Somsole, Lakshmi NarayanaNatarajan, ManikandanPasupuleti, ThejasreeKatta, Lakshmi NarasimhamuVivekananda, Soma
Polypropylene has been the plastic traditionally used in the manufacture of bumpers. Composite materials have been presented as an alternative due to lightness and sustainability. This article presents a composite of polyester resin and jute fiber fabric as an innovative alternative to be studied for the manufacture of automotive bumpers. Composite material was manufactured for characterization. It was used as matrix the terephthalic polyester resin, unsaturated and pre-accelerated, and the catalyst MEK V388 for curing the composite. The chosen reinforcement was the jute fiber fabric. Silicone molds with dimensions according to ASTM 3039 were used to manufacture specimens, and subsequent tensile strength test to determine properties and compare with literature data. The composite with jute fiber reinforcement with alignment 0°/0°/0° was evaluated as viable for the application in car bumpers, having its value of tensile strength surpassed that of the composite reinforced by jute fiber with alignment 45°/45°/45° and the results presented in the literature.
Dias, Roberto Yuri CostaSoares, Rafael Vilhenade Mendonca Maia, Pedro Victordos Santos, Jose Emilio MedeirosMiranda, Igor Ramon SinimbúJunior, Waldomiro Gomes PaschoalFujiyama, Roberto Tetsuo
This study describes the Taguchi optimization process applied to optimize drilling parameters for glass fiber reinforced composite (GFRC) material. The machining process is analyzed in relation to process parameters using analysis of variance (ANOVA). The characteristics assessed for both the drilling and the specimen include speed, feed rate, drill size, and specimen thickness. The commercial software program MINITAB14 was used to collect and analyze the measured results. Cutting force and torque during drilling are examined in relation to these parameters using an orthogonal array and a signal-to-noise ratio. The primary goal is to identify the critical elements and combinations of elements that impact the machining process to achieve minimal cutting thrust and torque, based on the evaluation of the Taguchi technique.
Raja, RosariJannet, SabithaKandavalli, Sumanth Ratna
Electric vehicles (EVs) represent a pivotal shift in the automotive industry, offering a sustainable alternative to traditional gasoline-powered vehicles. Central to their operation are lithium-ion batteries, which are favoured for their high energy density and long lifespan. Ensuring thermal stability during battery pack operation is crucial for both safety and efficiency. To enhance heat transfer within the battery pack, various encapsulants are employed. This study utilizes simulation to investigate the thermal performance of a 3.072kWh, 51.2V, 60Ah battery pack composed of 6Ah 32700 LFP cells, encapsulated with commercially available materials such as polyurethane (PU) foam, silicone, and silicone-modified epoxy under 1C and 2C discharge conditions. The findings show that, at 1C and 2C discharge rates, respectively, the battery pack potted with silicone attains a maximum temperature that is 2.57°C and 3.84°C lower than the pack simulated with air. Additionally, silicone-modified epoxy facilitates 1.92 times greater heat transfer in the battery pack compared to the pack without encapsulant at 1C, at 2C the heat transfer is 2.07 times higher. While encapsulants with higher thermal conductivities result in lower peak temperatures, they also exhibit a higher temperature gradient across the battery. The findings indicate that as the thermal conductivity of the encapsulant increases, the rate of improvement in the battery pack's heat transfer capabilities tends to decrease.
Somarajupalli, ShanmukhadevVedantam, SrikanthGupta, ShubhamJha, Kaushal Kumar
Eight arguments for these resins, compounds and composites. Weight reduction in EV battery components is an important factor in optimizing battery energy density, which in turn is critical to extending vehicle range and boosting power and performance. Although traditional metals such as steel and aluminum are widely used in EV batteries, the ongoing push for higher energy density is opening new opportunities for thermoplastic resins, compounds, and composites. The main advantage of these materials vs. metals is their inherent lighter weight - particularly in the case of lower-density polymers. Thermoplastics can be 30-50 percent lighter than metals. They also increase design freedom, which permits further weight-out through part consolidation and thin walls.
Bobba, Somasekhar
Smaller than a coin, this optical device could enable rapid prototyping on the go. Massachusetts Institute of Technology, Cambridge, MA Imagine a portable 3D printer you could hold in the palm of your hand. The tiny device could enable a user to rapidly create customized, low-cost objects on the go, like a fastener to repair a wobbly bicycle wheel or a component for a critical medical operation. Researchers from MIT and the University of Texas at Austin took a major step toward making this idea a reality by demonstrating the first chip-based 3D printer. Their proof-of-concept device consists of a single, millimeter-scale photonic chip that emits reconfigurable beams of light into a well of resin that cures into a solid shape when light strikes it.
Thermoplastic composites are serious competitor for classic epoxy composites. They have comparable properties to epoxy composites, but characterize much lower processing costs. There are several methods of manufacturing the components from thermoplastic composites. One of the most interesting method in terms of efficiency is thermoforming on a press. This technology allows to product of the aircraft parts such as: ribs, brackets, covers, stiffeners. Thermoplastic composites are resistant to most solvents such as grease, oil and aviation fuel. They are also non-flammable and heat-resistant. This all makes them suitable for use in aircraft as upholstery, casing or elements around the tank. PZL Mielec has been developing press thermoforming technologies since 2016 and is the owner of the several patents in this area.
Głodzik, MarcinWojtuszewski, RadosławFarbaniec, KonradSienicki, JarosławBanaś, AleksanderGałaczyński, Tomasz
Carbon fiber reinforced epoxy composite stiffened panels are increasingly being used for structural components in large transport rotorcraft. However, problems are arising with high levels of vibration and interior noise due to the increased stiffness-to-density ratio of composites. The current investigation explores the potential of reducing vibrations in carbon/epoxy stiffened panels with the integration of acoustic black holes (ABH), namely features that incorporate a power law thickness taper. The proposed approach involves designing a taper into the thickness of the blade stiffeners as well as the thin plate. Integration of ABHs into the fuselage structure has the potential to reduce broadband vibrations. Multiple parametric studies with either an ABH integrated into the blade stiffener or a grid of ABHs integrated into the plate were conducted, and the tradeoffs between vibration amplitudes, panel mass, and compressive buckling load were examined. Carbon/epoxy panels were fabricated using vacuum-bag-oven processing with out-of-autoclave prepreg and verified to be of good quality. The integrated velocity response, a proxy for the radiated noise from a panel, and compressive buckling were simulated using finite elements. Comparisons were made to experimentally measured data from modal testing and compression buckling testing. Experimental results indicated that when an ABH is integrated into the blade stiffener and 15 ABHs are integrated into the plate in a grid configuration, the panel mass was unchanged, the integrated velocity response decreased by 2.82 dB, and the buckling load increased by 2.9% compared to a baseline non-tapered design.
Brown, AveryVlajic, NicholasShepherd, MicahBeck, BenSmith, EdwardBakis, CharlesRobertson, NoahPatel, Bhavya
This work proposes an experimental and numerical activity aimed at developing methods to evaluate the strength and toughness of Kevlar/Epoxy composite fastened joints used in aeronautical structures and exposed to high energy impacts. Experiments were conducted using an Arcan rig that allowed applying various loading conditions, ranging from pull-through to bearing. A non-linear model of the material based on a bi-phasic decomposition and hybrid meshing technique was built and calibrated. The material model was used to develop a high-fidelity model of the junction to simulate the pull-through test with the Abaqus/Explicit finite element solver. The results of the analysis point out that the implemented progressive damage laws are capable of achieving an appreciable experimental-numerical correlation, both from the qualitative and the quantitative standpoint. Therefore, the combined experimental-numerical approach is promising for developing a validated numerical tool capable of predicting the overall response of different junctions with minimal experimental effort, so to provide data for simulating impact scenarios at the rotorcraft structural scale and designing critical joints.
Novembre, EdoardoCacchione, BenedettaJanszen, GerardusBrunori, FilippoAiroldi, Alessandro
Recycling of advanced composites made from carbon fibers in epoxy resins is required for two primary reasons. First, the energy necessary to produce carbon fibers is very high and therefore reusing these fibers could greatly reduce the lifecycle energy of components which use them. Second, if the material is allowed to break down in the environment, it will contribute to the growing presence of microplastics and other synthetic pollutants. Currently, recycling and safe methods of disposal typically do not aim for full circularity, but rather separate fibers for successive downcycling while combusting the matrix in a clean burning process. Breakdown of the matrix, without damaging the carbon fibers, can be achieved by pyrolysis, fluidized bed processes, or chemical solvolysis. The major challenge is to align fibers into unidirectional tows of real value in high-performance composites.
Muelaner, JodyRoye, Thorsten
Introducing a groundbreaking exploration into the mechanical properties of epoxy hybrid biocomposites, this study unveils a comprehensive analysis encompassing tensile strength, flexural properties, impact resistance, and hardness characteristics. The materials under scrutiny include hemp fiber (H), kenaf fiber (K), and coconut powder (CP), both in their untreated state and after undergoing alkaline processing. This research marks a significant milestone in understanding these sustainable materials and their potential for enhancing composite materials. In this endeavour, hemp is the basis material, while kenaf and coconut are filler elements. The total weight proportion of hemp was kept constant while the other two fibre fillers were changed. The unprocessed laminate sample significantly improves tensile, flexural, and impact strength with increasing coconut fiber loading. The improved interlinking capacity of the natural fibre composites (NFC) and an epoxy matrix is also to blame for the composite’s efficient resistance competency. Furthermore, the creation of powerful hydrogen bonds due to the increased polarisation of the epoxy matrix improved the bending characteristics of the hybrid natural composites. Untreated specimens’ impact strength was enhanced by up to 20% wt. of CP and K. The addition of more CP and K had a detrimental effect. Furthermore, as coconut fibre loading increased, the hardness value of unprocessed samples declined steadily. The mechanical properties of unprocessed material and chemically modified hybrid samples were evaluated. Compared to unprocessed composite samples, the results of alkali-treated composite samples demonstrate more excellent tensile, flexural, compression, impact strength, and hardness. SEM examinations on the fractured surface of hybrids revealed that surface alteration of the fibre occurred, which increased fibre-matrix interaction.
Kaliappan, S.Natrayan, L.
The automobile industry is searching for materials that offer superior mechanical and thermal properties. With this objective, the current study delves into the potential advantages of integrating nanofillers into hybrid composite structures tailored for vehicle applications. The investigation employed Kevlar fiber, a renowned material in vehicular composites, and reinforced it with an epoxy matrix, crafting a nanocomposite surface. This method was paralleled by incorporating nanoparticle-infused resin into the Kevlar fiber. The concentration of nano clay within the epoxy resin was adjusted across different weight percentages: 2.5%, 5%, 7.5%, and 10%. Both composite and nanomaterial panels were meticulously crafted using the hand layup method post-curing. The outcome was enlightening: the tensile strength of the clay/epoxy/Kevlar composite surged by 10.54% at the 7.5 wt% clay concentration. This enhancement, however, saw a decline in higher clay incorporations. The study also unveiled that the elastic modulus of these hybrid composites resonated better performance at reduced clay levels, peaking impressively at 381.47 MPa and 9.14 GPa for the 7.5 wt% variant. The same clay concentration bore witness to a zenith in flexural strength and modulus, registering 421.58 MPa and 15.01 GPa remarkable 13.15% upsurge when juxtaposed against the baseline Kevlar mix. Notably, the Interlaminar shear strength for this composition reached 96.21 MPa, overshooting the baseline Kevlar by 23%. However, shifting to a 10% clay mix reduced the interlaminar shear strength to 61.94 MPa, marking a 9% decrease from the baseline. Thermally, the composite showcased optimal stability at the lower clay concentrations from 0°C to 180°C. SEM imaging further buttressed these findings, highlighting that a 7.5% clay-enriched hybrid composite possessed distinct and advantageous surface features, making it a promising candidate for next-generation vehicle applications.
Natrayan, L.Seeniappan, KaliappanSree, G. Vanya
Due to the increasing demand for lightweight and eco-friendly materials in the automotive sector, alternative fibers like kenaf are gaining attention as potential materials for car components. This study aims to evaluate the impact of fly ash and Al2O3 nanomaterials on the mechanical and thermomechanical properties of kenaf fiber-reinforced composites, particularly for automotive applications. Various composites were produced and tested using standard manual fabrication methods for key mechanical properties such as tensile strength, flexural strength, inter-laminar shear strength, hardness, and impact resistance. Adding kenaf fibers, fly ash, and Al2O3 nanofillers to epoxy composites demonstrated a noticeable improvement in the thermomechanical properties of the resulting material. This enhancement is attributed to improved interfacial bonding and uniform distribution of the nanofillers within the polymer matrix. In our analysis, Al2O3 nanofillers had a more significant impact on the composite's performance than fly ash. A comparative study of different composite formulations revealed that the C-type composite had superior tensile properties, exhibiting a tensile strength of 86.74 MPa and a modulus of 5120.78 MPa. The A-type composite excelled in flexural tests, showing a bending strength of 101.54 MPa and a modulus of 8690.75 MPa. Meanwhile, the B-type composite showcased the highest impact resistance, hardness, and ILSS values, recording 7.51 KJ/m2 for impact, 69.47 D for hardness, and 29.14 MPa for ILSS. This research indicates that kenaf fiber composites reinforced with fly ash and Al2O3 nanofillers are promising for automotive applications by offering enhanced mechanical and thermomechanical performance.
Kaliappan, S.Natrayan, L.
With the evolving demand in the automobile industry for lightweight and sustainable components, the study of natural fiber composites has gained significance. Such fibers are economically efficient and offer advantageous weight-specific properties. Additionally, they are non-abrasive and environmentally degradable, marking them as viable alternatives to conventional automobile materials. This research emphasizes the flax-based composite, developed using the hand lay-up method and augmented with three distinct graphene nanofillers. The graphene fillers are categorized as large nanorods (dimensions 3-5 nm, lengths 150-300 nm), small nano threads (dimensions 6-12 nm, lengths under 50 nm), and spherical particulates (dimensions 29-39 nm). Reinforcement was consistently maintained at 2%, 4%, and 6% by weight. The results indicate that a 4 wt.% inclusion of spherical graphene nanoparticles is particularly effective in enhancing the ultimate tensile strength and fracture elongation of the epoxy matrix, registering improvements of 10% and 29% respectively. Reinforcements with all graphene variants noted an augmentation in the quasi-static toughness of the composites. Interestingly, a 6 wt.% infusion of the large graphene rod boosted the conductivity of the epoxy matrix by 52%. Thermal conductivity evaluations of the composite, integrated with different graphene configurations, recorded enhancements ranging from 0.22 W/mK to 0.286 W/mK at a 2 wt.% graphene concentration. At an elevated 4 wt.% graphene addition, the small rod-shaped fillers demonstrated an impressive 59.6% enhancement over the flax/epoxy baseline, while the larger rod and spherical graphene nanoparticles showcased a 22.14% enhancement. This study underscores the potential of graphene-augmented flax/epoxy composites as promising materials for automobile parts.
Kaliappan, S.Natrayan, L.
Automobile parts often require materials that offer high strength and durability. With the continuous push for environmentally friendly solutions, natural fibers such as jute have emerged as a potential alternative for synthetic fibers in automobile components. In this study, we aim to enhance the properties of jute fibers by coating them with different polymers and assessing their suitability for automotive applications. We treated jute fibers with various polymers—low-density polyethylene, polyester, and araldite epoxy. The performance of these treated fibers was compared using fiber tensile experimentation, differential calorimetry, and dynamic mechanical evaluation. Our findings reveal that the treated jute fibers exhibit a tensile strength of 598 MPa. However, when coated with polymers, there’s a variance in strength: polyethylene (263 MPa), polyester (191 MPa), and epoxy (281 MPa). Among these, epoxy-coated fibers displayed the least tensile strength, while polyethylene-coated jute fibers recorded the highest. A noteworthy observation is the lower dispersion value for the polyethylene-coated jute fiber, attributed to the penetration of polyethylene liquid into the jute fiber pores. In conclusion, modifying jute fibers using different polymers can enhance their mechanical properties, making them a viable option for automobile components.
Natrayan, L.Kaliappan, SeeniappanBalaji, N.Mahesh, V.
Bamboo fibers were used as reinforcement in hardened epoxy mixes altered with ethoxylated soybean oil (ESO) to enhance the mechanical and thermal qualities. Compared to a bio-based epoxy mix, the tensile strength and modulus of the laminate with 20% bamboo fiber were higher. During thermogravity analysis (TGA) evaluation, it was discovered that the rate of deterioration peak had been moved to a warmer temperature, indicating improved thermal durability of the aggregate over the base material. The dynamic mechanical evaluation of the bio-based composite anticipated increased storage modulus and greater glass transition temperatures. High fiber–matrix adherence was visible in scanning electron morphology (SEM). Measurements of the interfacial adhesion demonstrate the hydrophilicity of the bio-based reinforced composites. The binding and effective insemination of fibers is responsible for the fiber-reinforced composite’s durability. Higher rigidity and durability were generated because the lignocellulosic biomass adhered well to the low-viscosity resin. Moreover, research on adherence in composite materials reveals that the interfaces of composite materials with bamboo fibers are becoming more hydrophilic. Sufficient mechanical hardness, stiffness, and durability are realized for automobile and industrial purposes.
Meshram, Pawan DevidasNatrayan, L.Balaji, N.Reddy, Vinay
Steel represents more than 50% of weight in vehicles, being more susceptible to corrosion processes. Corrosion studies in these components are of great industrial and economic interest, and anticorrosive coatings with efficiency of superior protection is still a relevant area in materials research. Paintings from inorganic and organic hybrid compounds have been used to produce more effective and efficient coatings. Among polymeric coatings, epoxy resin is considered one of the most used anticorrosion coatings, mainly due its excellent protective properties. High barrier level is reached by reinforcing the coatings with inorganic fillers such heavy metal, nanoparticles, silica, and now more recently, carbon-based materials, like graphene and its derivatives. Graphene combined with additives presented in the paint composition can act as a passive physical barrier between the corrosive environment and the metal surface, restricting the diffusion of corrosive agents across the metal surface. In this work we provided a general view about the potential use of anticorrosive protective coatings based on graphene composites in epoxy resins in the automotive industry. We evaluated the state-of-the-art of some recent advances in the scientific and patent research databases in the last 10 years, as well as the existing commercial products available in the market. Finally, positive and negative points of view were observed in the use of graphene composites in coatings, such as the possibility of producing waterborne paint, which causes a reduction of potential polluting materials present in paint compositions. On the other hand, the dispersion and interactions of graphene structures along the resins are still the main challenges in processing of these composites. Despite facing major challenges, its versatility and noticeable studies results reveal the capability of graphene composite coatings to attend demand protection standards of the new car’s generation.
de Oliveira, Elisa M. N.Sormani, Mariana B.Hurtado, Luiz P.Polkowski, Rodrigo D. O.
Thermoplastic resins, composites, and copolymers can help the healthcare industry address multiple sustainability challenges. Specifically, thermoplastic materials can help manufacturers develop medical devices that:
Epoxy polymers are widely used in various industries, e.g., as coatings, adhesives, and for lightweight construction due to their unique properties such as high strength, chemical resistance, and adhesion to various surfaces. Therefore, one of the most prominent applications is their use as matrix material in fiber-reinforced composites, which are heavily employed in the aerospace sector. However, the disposal of epoxy polymers and composites thereof has become a significant concern due to their recalcitrant nature and the adverse environmental effects caused by traditional recycling methods.
Composites are especially important for the development and implementation of sustainable technologies such as wind power, energy-efficient aircrafts, and electric cars. Despite their advantages, their non-biodegradability raises challenges for the recycling of polymer and composites in particular. University of Hamburg, Hamburg, Germany Epoxy polymers are widely used in various industries, e.g., as coatings, adhesives, and for lightweight construction due to their unique properties such as high strength, chemical resistance, and adhesion to various surfaces. Therefore, one of the most prominent applications is their use as matrix material in fiber-reinforced composites, which are heavily employed in the aerospace sector. However, the disposal of epoxy polymers and composites thereof has become a significant concern due to their recalcitrant nature and the adverse environmental effects caused by traditional recycling methods. In this context, the overall production of plastic waste is projected to double within the next 20 years, with only 18 percent currently being recycled, leading to the deposition of around 12,000 Mt of plastic waste in landfills and the environment by 2050 (see figure 1). Even though epoxy polymers only accounted for a rather small share of the global plastic production volume of around 7.1 percent in 2021, the demand for fiber-reinforced polymers is steadily increasing. This is closely linked to emerging sustainable technologies such as off and on-shore wind power plants or electric vehicles that rely on lightweight construction materials for increased efficiency. To cover the resource demand of the composite industry and to reduce the environmental impact of accumulated epoxy waste, there is an urgent need for the development of sustainable recycling methods.
The requirement of the current scenario is to identify the sustainable material and process it into acceptable properties for current applications. The natural fiber is a prime sustainable material having the properties of biodegradability, plenty of availability, economical and adequate physical-mechanical property. Sesbania rostrata fiber is extracted from the stem of Sesbania rostrata plant which is cultivated along with Turmeric plants on 1000 acres annually as a nitrogen fixation plant. The fiber-reinforced composite is a tailor made material by altering the fiber and polymer weight proportion to achieve desired properties for applications. The natural fiber is a promising material to replace synthetic fiber to transform the composite into biodegradable. The making of holes in the biocomposite by the secondary process is essential for the assembly operation. The biocomposite was developed by reinforced Sesbania rostrata fiber in Polycaprolactone (PCL) biopolymer at the weight ratio of 20:80 and the mechanical properties and drilling parameters were investigated. The tensile, flexural and impact strength of the biocomposite was increased by 68%, 28% and 20.6% respectively compared with PCL biopolymer. The biocomposite was drilled by 4 mm at spindle speeds of 300, 750, and 1800 rpm with feed rates of 0.05, 0.12, and 0.25 mm/rev to evaluate the thrust force and delamination properties. The results showed that increasing spindle speed and feed rate resulted in higher thrust force and increased delamination in the composites. This study provides valuable insights into the mechanical properties and drilling behaviour of Sesbania rostrata fiber reinforced Polycaprolactone biodegradable composite and their potential use in various applications.
Raja, KA, KarthikSenthil Kumar, MSP S, Sampath
In order to determine if carbon–luffa hybrid composites are appropriate for automotive applications, this study gives a thorough mechanical evaluation of such materials. A potential path to improving the performance of automotive components is provided by combining the remarkable strength and stiffness of carbon fibers with the lightweight and environmentally friendly qualities of luffa fibers. The mechanical characteristics of the hybrid composites were characterized using a variety of experimental examinations, including tensile, flexural, and impact testing, and contrasted to those of traditional materials often used in the automobile sector. The composite containing 85% epoxy and 15% carbon fibers displayed the best tensile strength among the examined samples, reaching 168.58 MPa. However, 85% epoxy, 7.5% luffa, and 7.5% carbon fibers had a remarkable bending strength of 110.25 MPa. Notably, the B-type specimens distinguished themselves from the others with their low void content of 0.72% and low moisture absorption. The study’s findings offer important information on the viability of using carbon–luffa hybrid composites as lightweight, high-performance substitutes in various automotive applications, advancing the development of environmentally friendly automobile design and production.
Natrayan, L.Kaliappan, S.
Recycling of advanced composites made from carbon fibers in epoxy resins is essential for two primary reasons. First, the energy necessary to produce carbon fibers is very high and therefore reusing these fibers could greatly reduce the lifecycle energy of components which use them. Second, if the material is allowed to break down in the environment, it will contribute to the growing presence of microplastics and other synthetic pollutants. Recyclability and Embodied Energy of Advanced Polymer Matrix Composites discusses current recycling and disposal methods—which typically do not aim for full circularity, but rather successive downcycling—and addresses the major challenge of aligning fibers into unidirectional tows of real value in high-performance composites. Click here to access the full SAE EDGETM Research Report portfolio.
Muelaner, Jody Emlyn
To grow the application space of polymer additive manufacturing (AM), the industry must provide an offering with improved mechanical properties. Several entities are working towards introducing continuous fibers embedded into either a thermoplastic or thermoset resin system. This approach can enable significant improvement in mechanical properties and could be what is needed to open new and exciting applications within the aerospace industry. Introduction of Continuous Fiber Reinforced Polymer: A New Additive Manufacturing Path for Aerospace examines a couple of unsettled issues that are beginning to come to light regarding these materials and focuses on the ability to design and provide robust structural analysis for continuous fiber reinforced polymer AM—unsung aspects that can make or break this new technology as it finds its way into the aerospace market. Without solutions to them, adoption by the aerospace industry will be limited to point design applications, thus constraining the technology to being nothing more than a specialized tool. Click here to access The Mobility Frontier: Metals, Polymers, or Composites Click here to access the full SAE EDGETM Research Report portfolio.
Hayes, Michael
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