Browse Topic: Ceramics

Items (1,206)
High-performance composite materials are widely used in the main structural components of satellites. Various cylindrical components will hit the satellite at the time. The cartridge is fixed and unchanging. Honeycomb structure and ceramic honeycomb structure are the same, the cylindrical component is lighter and can attack satellites at a greater speed under the same conditions as the propellant. In terms of mass quality, the speed can reach over 1.6 times, and ceramic honeycomb structure can have minimal kinetic energy loss and can face enemies in combat with thicker steel plates, allowing for continuous destruction. Cylindrical component remaining kinetic energy (∆E) is 3.2968e3 J, but ceramic cylindrical component ∆E is 2.082e3 J, and ceramic cylindrical component have more advantages, and there are fewer arbitrary steel balls flying.
Xu, JianYang, ZhenChang, XuefangLi, QiangZhang, KunQu, Dandan
SiC-based power devices are favored for high-voltage and high-power applications due to their superior material properties. However, the demand for higher breakdown voltages and improved channel mobility presents significant challenges to the etching process, especially the micro-trenching effect. In this study, etching results from inductively coupled plasma (ICP) have been presents, which focused on using various SF6/O2/Ar gas ratios to eliminate micro-trenching effect. The profile analysis of micro-trench was taken by cross-sectional scanning electron microscopy (SEM). The results demonstrate that micro-trenches primarily originate from the coupling effect between ion multi-reflection from sidewalls and redeposition of etch byproducts. Based on this mechanism, we propose a quasi-Bosch process: a combined polymerization and etching step in oxygen-fluorine-rich plasma deposits polymer on exposed SiC and the mask, while removing it from the structure bottom via ion bombardment to enable etching and passivation; then alternates with a short fluorine-plasma step, which consumes sidewall polymer through ion incidence and prevents SiFxOy charge accumulation, cycle etching gradually deepens the structure without micro-trenches. Different gas ratios and etching time not only change the plasma energy distribution but also affect the temporal synchronization between etching and passivation steps. This approach reduces the special demands on ICP equipment capabilities while achieving superior trench profiles. The optimal etching conditions produced a micro-trench-free SiC structure with a vertical sidewall angle and a surface roughness of less than 1 nm. This methodology and resulting structures significantly advance the manufacturability of high-performance SiC power devices, enabling next-generation applications in electric vehicles and grid infrastructure where device yield and reliability are paramount.
Zhao, YingfanDong, ShuangSun, XiaoxuChang, XiangpengLiang, YiweiTong, Weiping
The impact of a titanium nitride (TiN) coating by the cathodic arc deposition (CAD) technique on a 316L stainless steel (SS) 316L substrate is examined in this experimental work. The X-ray diffraction study showed that TiN made the osbornite phase grow in the coated specimen. The SS 316L sample had a hardness of 217.66 HV, and the samples with CAD coatings were five times harder than the uncoated disc. The wear test was conducted using a pin-on-disc tribometer under dry and wet conditions at loading conditions of 2 N, 4 N, and 6 N with the counterpart of grade 5 titanium alloy (Ti6Al4V). Wear resistance improved significantly, with the wear rate decreasing markedly after coating compared to the uncoated sample. The wear morphology of the wear on the contact surfaces was identified by SEM analysis of the images. The biocompatibility of the ceramic-coated SS 316L sample with the normal cell line was proved by a cell viability test. The demand for SS 316L and the use of CAD coatings to reduce friction and wear in bio-implant applications were the main topics of the current study.
Gopi, R.Devaraju, A.Sivasamy, P.Raju, M.
It is known fact that Thermal management systems are essential to the safety, operational efficiency, and structural integrity of present-day commercial aircraft. Very critical insulation and thermal protection materials are utilized across various aircraft zones to mitigate extreme temperature challenges, ranging from cryogenic conditions at high altitude to pyrotechnic conditions at low altitude/ sea level. Some of the examples where specific materials at their functional role are, In engine pylons and nacelles, high temperature alloys such as Titanium and Inconel, along with ceramic Matrix composites (CMCs) serve as firewalls and heat shields, which are designed to contain fires and protect primary structures. In bleed air ducting, fiberglass or silica insulations blankets are employed to prevent thermal degradation of surrounding aluminum and composite components, when air at temperatures above 200 degree C flows. This paper focuses on the critical insulation and thermal protection materials on passenger Egress system utilized to mitigate pyrotechnic events. The focused case study on passenger egress system highlights a unique application of thermal protection. As these system, as mandated by FAA TSO-C69c, must ensure the system remains deployable and structurally stable for at least 90 seconds under intense heat exposure, preserving a workable egress path for passengers. The passenger egress system surface functions as a heat resistance barrier, resisting thermal energy from potential post-crash jet fuel fire. The heat barrier materials are polymer coated with woven nylon, impregnated with a metallic/ Ceramic layer. This study will emphasize how tailored material coating solutions are fundamental to addressing the diverse and extreme thermal demands in aerospace design, directly contributing to passenger’s safety and aircraft survivability.
Govindaraju, ParthasarathyNanjundegowda, Harshavardhana
For brake and clutch components of aircraft vehicles which require higher mechanical strength and wear resilient, light-weight aluminium composites were developed infusing solid lubricant. In this study, hybrid composites were developed using powder metallurgy route with aluminum alloy AA356 and various amounts of zirconium oxide (ZrO2) (0, 5, 10, 15, and 20 wt.%) as reinforcements. A solid lubricant hexagonal boron nitride (hBN) at a fixed 5 wt.% is considered. Following the appropriate ASTM guidelines, the specimens were mechanically characterized by measuring their density, porosity, micro-hardness, compression strength, impact strength, and flexural strength, among other properties. The findings showed that the composites' mechanical and physical behaviour were greatly affected by the inclusion of ZrO2. Porosity increased as a result of particle clustering and interfacial voids, while density increased gradually as ceramic content increased. Consistently increasing ZrO2 addition led to micro-hardness improvements; at 20 wt.% reinforcement, values reached their maximum, indicating that the hard ceramic phase contributed to better surface resistance. The best balance between particle reinforcement and matrix continuity was suggested by the compression and flexural strengths peaking at 15 wt.% ZrO2. However, when the addition was raised to 20 wt.%, brittleness and porosity began to marginally deteriorate. Unreinforced and lower ZrO2 composites had superior toughness in impact, whereas materials with a higher content had a poorer energy absorption capacity. The 5 wt.% hBN improved fracture arresting capabilities and helped load transmission over the interface. Inclusion of hBN provides solid-lubricating tribofilm formation that enhances the tribological performance. This study reveals that AA356/ZrO2-hBN hybrid composites have good hardness and compressive strength improvements, with 15 wt.% ZrO2 being the best composition with good strength, toughness, and wear resistance.
Senthilkumar, N.
To develop magnesium matrix composites, ceramic silicon nitride (Si3N4) particles are added to the magnesium (AZ31) matrix at 2 wt.%. The composite is produced via disintegrated melt deposition vacuum-stir-casting procedure. Microstructural studies reveal the presence of Si3N4 particles and their uniform spreading. An L9 orthogonal array, planned using Taguchi’s experimental design, is selected for three wear parameters; axial load (AL), rotational speed (RS), and time duration (TD) with trials as per the G99 standard in the pin-on-disc apparatus to assess the wear resilient of the composite. Experimental results show an increase in axial stress, and wear loss (WL) increases dramatically. Because the area of contact shrinks as RS increases, WL diminishes dramatically. When the AL is low, the friction coefficient (CoF) increases, and when the AL is large, CoF drops. When the RS is increased, CoF decreases. To optimize multiple responses effectively, the TOPSIS (Technique for Order Preference by Similarity to Ideal Solution) approach was adopted. According to the analysis, the ideal combination turned out to be a 10 N A, an RS of 275 rpm, and a TD of 1000 seconds. ANOVA results show that AL (56.99%) and RS (27.2%) contribute more, with a regression coefficient of 92.99%. Abrasive and adhesive wear mechanisms are observed from the worn-out surface micrographs.
Senthilkumar, N.Dhinakar Raj, C K
Hybrid bearings, which pair traditional bearing-steel raceways with ceramic rolling elements, can offer improved performance over full-metal bearings, particularly in aerospace applications. Because rolling-element bearings are critical components, effective condition monitoring is essential to prevent in-flight failures and support proactive maintenance strategies. Wear-debris monitoring is widely used in these applications to detect and diagnose bearing fault modes. To compare degradation behavior and monitoring signatures, bearing life tests were conducted on hybrid and full-metal bearings under matched Hertzian stress conditions. The results showed that differences in degradation curves between the two bearing types were small relative to the overall variability in bearing life. Additionally, hybrid bearings that develop rolling-element pitting were observed to progress toward raceway spall formation. This paper was presented at ERF Forum 51 but has been updated with new findings addressing questions over the effect of impact energy on the degradation rate between hybrid and full-metal bearings.
Mahmoud, HassanOszmian, Adam
Certain materials — such as quartz, some ceramics, and even bone — produce an electrical charge when they are squeezed, pressed, or vibrated. This is piezoelectricity, which comes from the Greek “piezein” meaning to press. Modern vehicles rely on piezo components in fuel injectors, parking sensors, airbag systems, and other functions.
Demand for cost-effective automotive traction inverters requires improved power module packaging. This paper presents a packaging method using an epoxy composite insulator applied directly to the cold plate surface, replacing Direct Bonded Copper (DBC) and Active Metal Brazed (AMB) substrates. This integration removes the substrate-to-cold plate solder interface and eliminates two material layers from the thermal path. The epoxy composite demonstrates a dielectric strength greater than 60 kV/mm. Thermal resistance (junction-to-coolant) measured approximately 0.17 K∙cm2/W. Electrical characterization showed a relative permittivity of 3.9, which is lower than standard ceramics and results in reduced parasitic capacitance. Initial thermal cycling tests indicated no significant degradation in thermal or electrical performance. These results suggest the epoxy composite insulator could be a promising alternative for traction power modules.
Chen, YuMena-Garcia, JavierChen, HaoXiao, KeweiGupta, Man PrakashDegner, Michael
Researchers have pioneered a 3D printing method that grows metals and ceramics inside a water-based gel, resulting in exceptionally dense, yet intricate constructions for next-generation biomedical technologies.
The application of Thermal Barrier Coatings (TBC) has been widely utilized in aerospace turbines to enhance the operational temperature and thermal efficiency of titanium alloys, while preserving their properties such as low density, creep resistance, and corrosion resistance. TBC systems typically consist of a metallic substrate, a metallic coating (Bond Coat), a thermally grown oxide (TGO), and a ceramic topcoat (TC). This study investigated the fracture surface characteristics of Ti-6Al-4V with TBC after a creep test at a constant temperature of 600 °C, under stress levels of 125, 222, and 319 MPa, in order to understand the mechanisms involved. The TBC was composed of a NiCrAlY (BC) and a zirconia co-doped with yttria and nióbia (TC). The fracture characterization of the alloy after the creep test was conducted through stereoscopy and scanning electron microscopy. The fracture mechanism at 600 °C and 222 MPa was predominantly ductile, as evidenced by the presence of dimples and shear zones at the edges of the specimens, indicating necking. In contrast, at 600 °C and stress levels of 125 and 319 MPa, brittle fracture was the dominant mechanism, with cleavage facets and a low percentage of area reduction. Thus, it can be predicted that the titanium alloy with TBC at 600 °C will exhibit better mechanical strength under stress conditions around 222 MPa.
Takahashi, Renata Jesuinade Assis, João Marcos KruszynskiRodrigues, Bianca Costade Andrade Acevedo Jimenez, Laila RibeiroReis, Danieli Aparecida Pereira
Composite Materials Handbook Volume 3 - Revision HR-64010/16/2025
The third volume of this six-volume compendium provides methodologies and lessons learned for the design, analysis, manufacture, and field support of fiber-reinforced, polymeric-matrix composite structures. It also provides guidance on material and process specifications and procedures for using the data that is presented in Volume 2. The information provided is consistent with the guidance provided in Volume 1, and is an extensive compilation of the current knowledge and experiences of engineers and scientists from industry, government, and academia who are active in composites. The Composite Materials Handbook, referred to by industry groups as CMH-17, is a six-volume engineering reference tool that contains over 1,000 records of the latest test data for polymer matrix, metal matrix, ceramic matrix, and structural sandwich composites. CMH-17 provides information and guidance necessary to design and fabricate end items from composite materials. It includes properties of composite materials that meet specific data requirements as well as guidelines for design, analysis, material selection, manufacturing, quality control, and repair. The primary purpose of the handbook is to standardize engineering methodologies related to testing, data reduction, and reporting of property data for current and emerging composite materials. It is used by engineers worldwide in designing and fabricating products made from composite materials.
CMH-17
Researchers have demonstrated a new technique that uses lasers to create ceramics that can withstand ultra-high temperatures, with applications ranging from nuclear power technologies to spacecraft and jet exhaust systems. North Carolina State University, Raleigh, NC A new technique that leverages the concept of sintering, can be used to create ceramic coatings, tiles or complex three-dimensional structures, which allows for increased versatility when engineering new devices and technologies. “Sintering is the process by which raw materials - either powders or liquids - are converted into a ceramic material,” says Cheryl Xu, co-corresponding author of a paper on this research and a Professor of Mechanical and Aerospace Engineering at North Carolina State University (NCSU). “For this work, we focused on an ultrahigh temperature ceramic called hafnium carbide (HfC). Traditionally, sintering HfC requires placing the raw materials in a furnace that can reach temperatures of at least 2,200 degrees Celsius - a process that is time-consuming and energy intensive.
A new technique that leverages the concept of sintering, can be used to create ceramic coatings, tiles or complex three-dimensional structures, which allows for increased versatility when engineering new devices and technologies.
This specification, in conjunction with the general requirements for peening media covered in AMS2431, establishes the requirements for the procurement of ceria-zirconia ceramic shot.
AMS B Finishes Processes and Fluids Committee
Abrasive water jet (AWJ) machining is the most effective technology for processing various engineering materials particularly difficult-to-cut materials such as aluminum alloys, steels, brass, ceramics, composites, and the like. The present study focuses on the experimental study on surface roughness and kerf taper is carried out during AWJ machining of Al 6061-T6 alloy with 40 mm thickness, and the influence of process parameters includes water jet pressure, standoff distance, and abrasive flow rate on the kerf taper and surface roughness is analyzed. The number of experiments is designed using Taguchi’s L9 orthogonal array. Experimental results are statistically analyzed using ANOVA. Also gray relational analysis (GRA) coupled with principal component analysis (PCA) hybrid approach was implemented to optimize the performance parameters. From the results it is found that standoff distance and hydraulic jet pressure are the most influencing parameters on surface roughness and kerf taper.
Kolluri, Siva PrasadSrikanth, V.Ismail, Sk.Bhanu, C.H.
Researchers are developing soft sensor materials based on ceramics. Such sensors can feel temperature, strain, pressure, or humidity, for instance, which makes them interesting for use in medicine, but also in the field of soft robotics.
This study investigates the thermal buckling behavior of axially layered functionally graded material (FGM) thin beams with potential applications in automotive structures. The FGM beam is constructed from four axially stratified sections, with the proportional amount of metal and ceramic fluctuating through the thickness. The buckling analysis is carried out for three different support configurations: clamped-clamped, simply supported-simply supported, and clamped-simply supported. The primary objective is to identify the optimal thermal buckling temperature of the FGM thin beam using the Taguchi optimization method. Beam arrangements are established using a Taguchi L9 orthogonal array and analyzed using finite element software (ANSYS). Layers 1-4 of the axially layered beam are considered process parameters, while the thermal buckling temperature is the response parameter. Minitab software performs an Analysis of Variance (ANOVA) with a 95% confidence level to identify the most influential layer and its relative contribution to the buckling temperature. The results, confirmed by a separate test, indicate that Layer 2 substantially affects the critical buckling temperature within the beam. Ultimately, the optimal critical buckling temperature is forecasted based on the 95% confidence interval of the confirmation analysis and population data. This research provides valuable insights into optimizing the thermal performance of FGM thin beams for automotive applications, where lightweight structures with high thermal stability are crucial. Engine Hood A non-uniformly heated engine hood can buckle and warp, affecting aesthetics and potentially causing fitment issues with fenders or compromising safety features like hood latches. The findings can guide the design and development of vehicle heat-resistant components, potentially leading to improved fuel efficiency and safety.
Pawale, DeepakBhaskara Rao, Lokavarapu
This research examines the thermal instability of slender beams composed of functionally graded materials (FGMs), with a specific focus on their suitability for engine hood components. The FGM combines the durability of aluminum with the heat tolerance of silicon nitride. The study aims to determine the maximum temperature the beam can withstand without buckling under various support conditions, simulating the uneven heat distribution experienced by engine hoods in actual use. The FGM structure comprises four longitudinally arranged layers, where the ceramic and metallic components gradually shift across the thickness. Finite element modeling software (ANSYS) is utilized to examine the buckling response under diverse temperature conditions. To enhance the thermal performance of the engine hood panel, the Taguchi L9 orthogonal array methodology is employed utilizing Minitab 19 software. The first four layers of the FGM beam are defined as process variables, while the critical buckling temperature is designated as the output variable. The material composition of each layer is adjusted across three levels to assess its impact on the hood panel's resistance to thermal strain. The Signal-to-Noise (S/N) ratio is employed to determine the ideal configuration for achieving the highest possible critical buckling temperature. This investigation also uncovers the influence of ceramic and metallic composition on the behavior of each layer, enabling the creation of an FGM hood panel that offers superior heat resistance and structural robustness. Additionally, an Analysis of Variance (ANOVA) is performed with a 95% confidence interval to identify the layer with the most substantial impact on the critical buckling temperature and quantify its relative influence. This information is essential for customizing the FGM composition to target areas of the hood panel exposed to the highest thermal loads, like the region directly above the engine. Finally, utilizing the 95% confidence interval derived from the confirmatory analysis and population statistics, the ideal maximum temperature before buckling for the FGM engine hood component is projected. This investigation yields significant knowledge for the development of lightweight, thermally resilient FGM engine hood structures. By refining the material composition of each layer, designers can produce engine hoods with superior resistance to heat-induced warping, potentially resulting in improved vehicle safety and functionality.
Pawale, DeepakBhaskara Rao, Lokavarapu
Aluminum Matrix Composites (AMCs) are gaining traction in aerospace, automotive, and marine industries due to their superior mechanical properties. By integrating hard ceramic particles such as silicon carbide (SiC) and aluminum oxide (Al₂O₃) into aluminum matrices, these composites exhibit enhanced wear resistance and strength-to-weight ratios. This study explores the fabrication and characterization of 6061-T6 aluminum alloy matrix composites, reinforced individually with SiC and Al₂O₃ particles through the squeeze casting technique. The research includes a comprehensive analysis of microstructures and mechanical properties, focusing on compressive strength, Brinell hardness, and tribological behavior. Findings reveal that SiC and Al₂O₃ reinforcements boost compressive strength by up to 27% and 47%, respectively, and increase hardness by up to 29% and 20%, respectively, compared to unreinforced aluminum.
Thirumavalavan, R.Santhosh, V.Sugunarani, S.Regupathi, S.Sundaravignesh, S.
This research was conducted with the aim of exploring the usage of advanced lightweight materials such as aluminum matrix composite and aramid fiber reinforcement polymer for increased structural integrity of the hood of an automotive vehicle. The automotive sector is moving toward lightweight materials because of the need to enhance fuel efficiency, the importance of reducing environmental impact, and the need to ensure safety of new-generation automobiles. While traditional materials such as steel and aluminum might be very rigid and durable, they also add huge weight to the overall vehicle design. Consequently, these vehicles become more fuel inefficient, which could lead to higher emissions and pollution. The two materials chosen for this research are very promising, considering that both are characterized by high specific strength and impact resistance capabilities. The low weight of the materials is also an added bonus. While AMC is manufactured by consolidating aluminum with ceramic or metallic components, AFRP employs aramid fibers in a polymer matrix. The test performed in this research to evaluate the suitability of the two materials for the said purpose include tests on impact resistance, tensile strength, and hardness. The materials were tested concerning the standards of the Charpy test, the universal testing machines, and the Vickers scale. The findings of the test produced differing results concerning the two materials. AMC demonstrated an average impact resistance of 76 kJ/m2, a tensile strength of 402 MPa, and a hardness of 122 HV. AFRP, on the other hand, registered superior values for the said test: an average impact resistance of 153 kJ/m2, a tensile strength of 556 MPa, and a hardness of 122 HV. Consequently, the research concludes that AFRP is the most suitable material for hood design in the automotive industry.
Arvinda Pandian, C.K.Balaji, N.Seeniappan, KaliappanNatrayan, L.Maranan, RamyaRavi, D.
The modern-day development in the field of mobility demands the development of advanced engineering materials for various engineering applications. Composite materials play a pivotal role in the advancement of mobility by achieving overall weight reduction and thereby contributing to the sustainability of the environment. Metal matrix composites has played a crucial role over the last few decades in the automotive industry replacing the conventional metal in achieving a better strength to weight ratio. Metal matrix composites can be a combination of a metal and a ceramic combined at a macroscopic level to achieve better mechanical and tribological properties at a reduced weight to strength ratio. Aluminium being one of the largest metals widely used in automobiles, are gradually being replaced with Aluminium metal matrix composites. Aluminium – silicon carbide composite is a key interest among the researchers due to the attractive mechanical and tribological properties that enhance the performance of automobiles. The most common applications of aluminium silicon carbide composites in automobiles are pistons, cardan shaft, connecting rods etc. This study is focused on the chemical interfacial reaction between silicon carbide and aluminium matrix which occurs during the elevated temperature of casting process and thereby creating stress localization due to the formation of aluminium carbide in the matrix. The chemical reaction also results in the degradation of silicon carbide which can lead to poor performance of the composite. Hence it is very important to keep this chemical reaction to a minimum level. This research is centered on finding out an effective solution for hindering this chemical reaction by adding a material which is cheap, easily available and existing as an industrial waste material. Utilizing it for the composites can contribute to the sustainability of nature as well. Various mechanical properties are evaluated for this hybrid composites to evaluate the performances.
Valsan, Ashray
Residual thermal energy, a by-product of automobiles, contributes notably to climate change and global warming. This energy is produced as exhaust gases in vehicles with internal combustion engines and as heat from batteries and fuel cells in eco-friendly vehicles. A thermo-electric generator (TEG) can transform this waste heat into useful electrical energy. The efficiency of the TEG is influenced by several factors, including the properties of the materials used, the geometrical design (form factor), and the conditions under which it operates. In this study, we examine how the choice of materials for the semiconductors, electrodes, ceramics, and joining components influences the overall performance of the TEG. We evaluate the TEG’s performance based on output power, and efficiency. The findings from these measurements allow us to determine which material and its properties significantly impact the TEG’s performance. For optimal TEG performance, seek materials with high Seebeck coefficients, low thermal conductivities, and low specific resistivities. For all other components (electrodes, ceramic plates, and thermal interface materials), using higher thermal conductivity materials results in higher TEG performance.
Ponangi, Babu RaoMutagi, MeghaBali, Gaurav
This specification, in conjunction with the general requirements for peening media covered in AMS2431, establishes the requirements for the procurement of yttria-zirconia ceramic shot.
AMS B Finishes Processes and Fluids Committee
The phenomenon of drop-wall interaction plays a crucial role in a wide range of industrial applications. When liquid droplets come into contact with a high-temperature surface, it can lead to thermal shock due to rapid temperature fluctuations. This abrupt temperature change can generate thermal stress within the solid wall material. If the thermal stress exceeds the material's strength in that specific stress mode, it can result in material failure. Therefore, it is imperative to delve into the evolving temperature patterns on high-temperature surfaces to optimize material durability. This study focuses on investigating drop-wall interactions within the context of engine environments. To achieve this, the Smoothed Particle Hydrodynamics (SPH) method is employed to simulate the impact of fuel droplets on a silicon nitride wall. The goal is to understand the heat transfer mechanisms, thermal penetration depths, and temperature distributions within the heated wall. Furthermore, this research explores the performance of ceramic materials, specifically silicon nitride, in terms of thermal stress. Thermal stress calculations are derived from temperature gradients and material properties. Results show that the silicon nitride glow plug can operate for infinite engine cycles if it is run under the relevant engine conditions.
Ahamed, SheikhKong, Song-Charng
FMVSS No. 205, “Glazing Materials,” uses impact test methods specified in ANSI/SAE Z26.1-1996. NHTSA’s Vehicle Research and Test Center initiated research to evaluate a subset of test methods from ANSI Z26.1-1996 including the 227 gram ball and shot bag impact tests, and the fracture test. Additional research was completed to learn about potential changes to tempered glass strength due to the ceramic paint area (CPA), and to compare the performance of twelve by twelve inch flat samples and full-size production parts. Glass evaluated included tempered rear quarter, sunroof, and backlight glazing. Samples with a paint edge were compared to samples without paint, and to production parts with and without paint in equivalent impact tests. A modified shot bag with stiffened sidewalls was compared to the ANSI standard shot bag. The fracture test comparison included evaluating the ANSI Z26.1 impact location and ECE R43 impact location. Over 900 tests covering the various test conditions outlined above were completed. High-speed video was recorded for each test to capture break initiation and propagation. Overall trends showed a decrease in glazing strength due to the CPA when impacted with the 227 gm ball. The modified shot bag concentrated the impact force, resulting in more glass breakages than with the ANSI bag. ECE R43 fracture test location produced larger pieces than the ANSI fracture location. Results of this study may be used to help determine if the tests in ECE R43 and ANSI/SAE Z26.1-1996 can be harmonized to reduce testing burden, and also if the effect of the ceramic paint on glazing performance could be considered in evaluating glazing performance.
Rains, Corinn
Additive manufacturing enables unrivaled design freedom and flexible fabrication of components from a wide range of materials including metals, composites, polymers, and ceramics. The near net shape parts are made by processes like sequential melting or layer-by-layer material deposition with a complex set of processing variables. The sequential nature of the process means that every step can impact the next and thus, tools to evaluate that risk before and during manufacturing are necessary.
Magnesium and its alloys are promising engineering materials with broad potential applications in the automotive, aerospace, and biomedical fields. These materials are prized for their lightweight properties, impressive specific strength, and biocompatibility. However, their practical use is often hindered by their low wear and corrosion resistance. Despite their excellent mechanical properties, the high strength-to-weight ratio of magnesium alloys necessitates surface protection for many applications. In this particular study, we employed the plasma spraying technique to enhance the low corrosion resistance of the AZ91D magnesium alloy. We conducted a wear analysis on nine coated samples, each with a thickness of 6mm, to assess their tribological performance. To evaluate the surface morphology and microstructure of the dual-phase treated samples, we employed scanning electron microscopy (SEM) and X-ray diffraction (XRD). The bare AZ91D magnesium alloy exhibited a microhardness value of 403 HV. However, the coatings substantially improved these values, resulting in hardness measurements of 715 HV and 850 HV, respectively.
Kishore Kanna, K.Mohamed Thariq, R.Marimuthu, S.Daniel Das, A.Suresh Balaji, R.Manivannan, S.
The requirement for lightweight, high-performance materials with higher wear resistance, which is critical in industries such as aerospace, automotive, and consumer-related sectors, has fueled the development of particle reinforced metal matrix composites (PRMCs). These materials are an appealing alternative for a broad variety of scientific and technological applications due to their remarkable mechanical qualities and low cost. The primary goal of developing metal matrix composite materials is to combine the favorable properties of metals and ceramics. This study included several experimental experiments to explore the behavior of stir-cast composites made of aluminum grade 6063 with varying amounts of SiC, Al2O3, and TiO2 reinforcements. The specimens obtained through the use of stir casting methodologies are subjected to a wide range of mechanical tests, including tensile tests, impact analyses, hardness measurements, and tribological investigations such as sliding wear tests and erosive wear tests. The existence of phases inside the reinforced material was determined using X-ray diffraction. The testing findings showed that the integration of silicon carbide particles resulted in improved mechanical properties owing to the particles' uniform distribution. Many variables impact the properties of metal matrix composites (MMCs), including the interface characteristics, the volume fraction of reinforcement, and the material selection. The Al MMC's tribological metrics show a decrease in both the coefficient of friction and the wear rate. The experimental findings show that semi-ductile behavior exists in composites with a high erosion rate. The aforementioned composite materials may find use in the aerospace and automotive industries, where increased properties like as toughness, wear rate, density, and hardness are desired. Nonetheless, these findings may serve as a foundation for the creation of MMC components by both academics and industry designers. The ductility test results show that the incorporation of reinforcement particles (SiC-Al2O3-TiO2) in the matrix material of Al 6063-(SiC-Al2O3-TiO2) composites reduces ductility significantly.
Chaudhary, Amit S.Waghulde, Kishor B.Javanjal, Vijaykumar KisanSubhash, Gadhave
Aluminium composites are remarkably used in automotive, aerospace, and agricultural sectors because of their lightweight with definable mechanical properties. The stir casting route was followed to fabricate cylindrical samples with base aluminium alloy LM4, LM4/SiC, LM4/Al2O3, and LM4/SiC/Al2O3. The tensile strength, compressive strength, hardness, and micro-structural analysis were performed on samples and Finite element analysis (FEA) was adopted to predict the failure modes of composites. The composites experimental results were found to be in line with the FEA results, however, the LM4/SiC/Al2O3 revealed better results on the mechanical properties when compared with other composite configurations. The mechanical properties improvement like hardness 5%-11%, tensile strength 10.26%-20.67%, compressive strength 15.19% - 32.58% and 71.52 - 82.1% reduction in dimension have been achieved in LM4/SiC/Al2O3 composite comparing to base metal.
Rajeswari, B.Manikandan, C.Rajeshkumar, L.Aravind, R.M.
In this study, we have investigated the microstructural characteristics, the mechanical properties, and the dry sliding wear behavior of a ceramic coating consisting of zirconia (ZrO2) and alumina (Al2O3) deposited by flame spraying. A series of wear tests were carried out under a variety of loads and at two different sliding speeds. The evaluation included an examination of the coating microstructure, microhardness, coefficient of friction (COF), and wear resistance of the flame-sprayed coating. The results showed that the coatings had a perfectly structured micro-architecture and were metallurgically bonded to the substrate. The Al2O3 coating exhibited a fine granular structure with pores and oxides. The microstructure of Al2O3-10 wt.% ZrO2, on the other hand, showed a blocky structure with a uniform distribution of ZrO2 inclusions in the composite coating. X-ray diffraction (XDR) results showed that the phases in both coatings were predominantly α-Al2O3 with a minor presence of γ-Al2O3. However, in addition to residual ZrO2 in the tetragonal phase, the ZrO2-Al2O3 coating showed a predominance of ZrO2 in the monoclinic structure. To elucidate the intricacies of the wear mechanism and the characteristics of the wear debris, a comprehensive analysis of the wear performance of flame-sprayed ceramic coatings was carried out.
Younes, RassimBaiamonte, LidiaIdir, AbdelhekDalibon, EugeniaSadeddine, AbdelhamidBradai, Mohand Amokrane
In pursuing enhanced bio-composite properties, filler materials play a pivotal role. This study delves into the impact of ceramic additives on the chemical resistance and moisture durability of flax fiber-reinforced polymers. Utilizing the hand lay-up technique, we developed polyester composites reinforced with flax fibers. Silicon carbide (SiC) and aluminum oxide (Al2O3) were chosen as filler components. One batch of flax fibers underwent an alkaline treatment to enhance their properties further using a 5% NaOH solution. The resistance of composite samples to acetic acid and sodium hydroxide was then assessed. Additionally, the moisture absorption patterns of all models were investigated. A thorough comparative analysis was conducted among multiple composite batches. The results highlighted that integrating additives significantly bolstered the chemical and moisture resistance of the composites. Notably, the alkali-treated samples exhibited superior moisture and chemical agent resistance compared to their untreated counterparts.
Pandian, ArvindaKaliappan, SeeniappanNatrayan, L.Reddy, Vinay
Composite ceramic brake discs are made of ceramic material reinforced with carbon fibers and offer exceptional advantages that translate directly into higher vehicle performance. In the case of an electric vehicle, it could increase the range of the vehicle, and in the case of conventional internal combustion engine vehicles, it means lower fuel consumption (and consequently lower CO2 emissions). These discs are typically characterized by complex internal geometries, further complicated by the presence of drilling holes on both friction surfaces. To estimate the aerothermal performance of these discs, and for the thermal management of the vehicle, a reliable model for predicting the air flowing across the disc channels is needed. In this study, a real carbon-ceramic brake disc with drilling holes was investigated in a dedicated test rig simulating the wheel corner flow conditions experimentally using the particle image velocimetry technique and numerically. The simulation was performed using the moving reference frame (MRF) approach and the experimental data were used to validate the numerical model. The results show that drilling holes contribute to about 13% of the inlet mass flow and more than 86% of the air driven into the brake disc comes from the main inlet of the disc. Moreover, the numerical results are in an agreement with experimental data, supporting MRF approach as a suitable model for the analysis of complex flows in complicated geometries.
Rouina, SamanehBarigozzi, GiovannaAbdeh, HamedPalomino Solis, Daniel A.Iavarone, Paolo
Billions of people around the world lack access to clean, drinkable water. A research team led by engineers at The University of Texas at Austin has developed a new water filtration system using locally sourced materials for members of the Navajo Nation in the Southwest.
Magnesium alloy nanocomposite prepared with hard ceramic particles via conventional technique is a promising future material for automotive applications due to its unique characteristics like low density, high strength, castability, and good wear resistance. The present study is to enhance the tribo-mechanical properties of alumina nanoparticle (10wt %) reinforced magnesium alloy (Mg/Al) composite by incorporating 1wt%, 3wt%, and 5wt% zirconium dioxide (ZrO2) nanoparticles through stir casting method. The tensile strength, impact toughness, hardness, and wear rate of developed composites were compared with (10wt %) alumina nanoparticles reinforced magnesium alloy composite. The nanocomposite containing 3wt% ZrO2 shows maximum impact strength of 22.8 J/mm2. The maximum tensile strength (88.9MPa), hardness (124.5BHN), and wear resistance (9.802mm3/m at 20N) are obtained for 5wt% ZrO2 magnesium alloy nanocomposite.
J, ChandradassT, ThirugnanasambandhamRajendran, RMurugadoss, Palanivendhan
This specification covers characteristics for chemistry, microstructure, density, hardness, size, shape, and appearance of zirconium oxide-based ceramic shot, suitable for peening surfaces of parts by impingement.
Surface Enhancement Committee
ABSTRACT High performance fiber reinforced ceramic rotors have the potential to greatly improve metrics in heavy vehicles such as braking distance, acceleration time, maximum speed, fuel consumption, improved handling, and increased vehicle maximum loads. Three types of carbon ceramic composite brake rotor materials were created using polymer infiltration pyrolysis (PIP) for carbon fiber reinforced silicon oxicarbide, reactive melt infiltration (RMI) for carbon fiber reinforced silicon carbide, and electric field assisted sintering (EFAS) for carbon fiber reinforced silicon carbide-zirconium diboride to investigate the manufacturing of 396mm diameter heavy vehicle brake rotors. The microstructure of parts created by each manufacturing method were discussed and contrasted. The EFAS manufactured rotor created the highest quality part due to extremely fast processing times, uniform material microstructure, and fusing of adjacent fibers in the carbon fiber network. Thermal conductivity was measured to be greater than that of a traditional steel rotor. Citation: Jorgen Rufner, Clifford Leonard, Steven Nutt, Kevin Hyuyen, “Manufacturing of Carbon Fiber Reinforced Silicon Carbide – Zirconium Diboride Composite Brake Rotors using Electric Field Assisted Sintering,” In Proceedings of the Ground Vehicle Systems Engineering and Technology Symposium (GVSETS), NDIA, Novi, MI, Aug. 16-18, 2023.
Rufner, JorgenLeonard, CliffordNutt, StevenNguyen, Kevin
Many of today’s high-performance technologies — nuclear reactors, spacecraft, concentrated solar plants, and hydrogen cells — require advanced materials. Advanced means they are made of metals and ceramics that can withstand extreme conditions or meet exacting specifications.
Photonics, the science and technology of light, relies on optical components that affect light transmission in very specialized ways. To achieve the precision required, the optical components must be precisely ground from standard forms of glass, ceramics, or other materials to exceedingly tight tolerances, in many cases with extreme levels of flatness and parallelism.
Cooling loss reduction is essential to enable further increases in thermal efficiency of reciprocating internal combustion engines. Many in-cylinder cooling loss reduction studies have been carried out by applying various thermal barrier coatings to the piston and/or other in-cylinder surfaces, taking advantage of the lower thermal effusivity of ceramic materials. However, the end result was mostly minimal or in some cases, negative. In our previous study, significant cooling loss reduction was experimentally confirmed by utilizing a mirror-like polished stainless-steel thermal sprayed surface (HVOF: high velocity oxy-fuel) on a forged steel piston. This study firstly investigated an alternative insulating layer material to stainless-steel, along with effects of its thickness on heat transfer by a one-dimensional unsteady numerical model. Results showed that lower thermal effusivity doesn’t always reduce heat transfer, but increases nonuniformity of surface temperature. Next, a modified insulation structure composed of a thin aluminum coating overlayed by physical vapor deposition (PVD: physical vapor deposition) on a stainless-steel layer of both the piston and cylinder head, was tested in a heavy-duty single cylinder engine. Aluminum was initially selected due to its high reflectance, to reduce absorption of flame radiation, but selectively absorb it at soot deposits, where the flame interacts with the wall, and reduce local convection. Experimental results suggested that higher surface temperatures of exposed areas are caused by better heat conduction outward from hot spots during and after the combustion period, through the aluminum coating. Such surface temperature equalization could also result in further reduction of cycle-integrated heat transfer.
Kawaharazuka, FumihiroUchida, Noboru
This paper will illustrate the surface treatment coating that forms a strong metallurgical bond between the titanium alloy matrix regarding the high friction properties and challenging lubricating of titanium alloys. In this research, TC4 has been selected as a base material instead of TiC. Then Ni-composite coating was employed as the surface treatment of TC4 by laser cladding (LC) process. The Ni-based alloy coating material powder is good self-fluxing, has high-temperature resistance, and is analytically pure with 200 mesh. The chemical properties of Ni composite coating include 31.2 % Chromium, 8%Titenium, and 3.6% Carbon. Overall characterization and microstructure analysis of the prepared coating utilizing OM, XRD, SEM, EDS, and EPMA with different laser-specific energies (LSP) performance impact. It is evident that an excellent coating can be employed at the LSP of about 12.5kJ/cm2. The TiC ceramic particle reinforced phase is dispersed into a two-phase solid solution of β-Ti and γ-Ni. The micro-hardness of the employed coating is greater than the base alloy. This research also optimized that laser power is proportional to the coating structure. This research has practical value in the modern aerospace and automobile industry to increase the application of titanium alloy.
Miah, Md HelalChand, Dharmahinder SinghMalhi, Gurmail SinghKhan, Shahrukhal Muin, Abdullah
Brazilian Emissions Regulations are getting tighter in the coming years. With PROCONVE L7 in Jan-2023 and PROCONVE L8 in 2025, regulated emissions limits will significantly decrease, such as, the NMOG + NOx standard from 130 mg/km (PL6) to 50 mg/km (PL8). This challenge will necessitate better aftertreatment performance, with expected increases the catalytic converter PGM content, and consequently higher system cost. It is understood that approximately 75% of an engine’s gaseous pollutants occur during the first few seconds after a cold start, thus it is crucial to promote the emissions conversion performance during that period. One approach is to decrease the heat capacity of the catalytic system, which can be done by utilizing cordierite substrates with thinner walls or an increased material porosity. CORNING has developed an innovative technology to substantially raise the porosity of conventional ultra-thin wall substrates from 35% to 55%, while maintaining their strength. This advanced low mass design allows for a reduction of the substrate volumetric heat capacity, enabling a faster thermal response for improved catalytic function and lower tailpipe emissions. With an aim to understand the performance of the advanced low mass substrate technology within Brazil’s traditional ethanol-fuel environment, an emissions test program was performed using a modern 1.0L turbo-charged E100 engine on a transient dynamometer. The aftertreatment system consisted of 2 catalytic converters; a 1.26L converter in the closed-coupled position, and a 1.0L converter in the underfloor position. The focus of the study was to evaluate the substrate impact in the close-coupled catalyst, while the maintaining the underfloor catalyst. The baseline reference was a standard 750/2 substrate with a conventional TWC formulation in the close-coupled position. To explore the emission and cost reduction potential, samples of the low mass, high porosity substrates were coated and tested with the same TWC formulation, as well as, with reduced precious metal content. Prior to testing, all samples were oven-aged at 900°C to represent an end-of-life condition. Emission testing procedures followed the USEPA FTP75 protocols. Results from this study confirmed that the advanced low mass substrate can significantly reduce emissions (THC emissions by roughly 13%) or allow for lower PGM loadings without emissions penalty.
Petrini Fogaça, RômuloUrbani Amadei, GabrielL. Warkins, JasonA. Craig, Angus
Aerospace & Defense Technology: December 202222AERP1212/1/2022
Why are Aerospace & Defense Companies Embracing Additive Manufacturing? Simplifying Power Design with Modular Architectures The Role of DevSecOps in Modern Edge Systems Making Machines Curious Designing Multi-Channel Microwave Radio Systems Using Optical Interconnects Solving Military Satellite, Radar and 5G Communications Challenges with GaN-on-SiC MMIC Power Amplifiers Advanced Airborne Defensive Laser for Incorporation on Strike Fighter Aircraft A technical and operational analysis of an airborne "hard-kill" Ytterbium fiber laser-based anti-missile system for use on strike fighters. Additive Manufacturing Utilizing a Novel In-Line Mixing System for Design of Functionally Graded Ceramic Composites Exploring the development of a direct ink writing system with multimaterial and in-line mixing capabilities for printing inks composed of high solids-loaded ceramic particulate suspensions. Hierarchical Diamond-Based Ceramic Composites An innovative combination of experimental synthesis and testing and multiscale simulation techniques explored the effects of hierarchical microstructure (mesoscale diamond packing and nanoscale interfaces) on the mechanical and ballistic performance of diamond-silicon carbide (SiC) composite ceramics. Biobased Carbon Fibers and Thermosetting Resins for Use in DOD Composites Applications Using biological resources to make advanced fibers and high-performance thermosetting resins will help reduce the dependence of military composites on the volatile cost of petroleum, resulting in significant technological gains and reducing the toxicity of composite materials. MOVPE Growth of LWIR AlInAs/GaInAs/InP Quantum Cascade Lasers: Impact of Growth and Material Quality on Laser Performance The quality of epitaxial layers in quantum cascade lasers (QCLs) has a primary impact on QCL opera-tion, and establishing correlations between epitaxial growth and materials properties is of critical im-portance for continuing improvements in QCL performance.
The impetus for advancing brittle ceramic materials used for armor applications has been identified as both an increased mass efficiency for greater weight reduction and enhanced performance against ballistic threats through manipulating the physics of failure.
This research developed and utilized advanced processing, modeling, and micromechanical tools to discover and demonstrate hierarchically structured diamond-based composites with exceptional mechanical and ballistic behavior. Understanding how nanoscale and mesoscale microstructural features in diamond–silicon carbide (SiC) composites influenced the physics of failure was critical in uncovering ways to improve performance for soldier protection and discover potential defeat mechanisms.
Hierarchical Diamond-Based Ceramic Composites22AERP12_0912/1/2022
An innovative combination of experimental synthesis and testing and multiscale simulation techniques explored the effects of hierarchical microstructure (mesoscale diamond packing and nanoscale interfaces) on the mechanical and ballistic performance of diamond-silicon carbide (SiC) composite ceramics. Army Research Laboratory, Aberdeen Proving Ground, Maryland This research developed and utilized advanced processing, modeling, and micromechanical tools to discover and demonstrate hierarchically structured diamond-based composites with exceptional mechanical and ballistic behavior. Understanding how nanoscale and mesoscale microstructural features in diamond-silicon carbide (SiC) composites influenced the physics of failure was critical in uncovering ways to improve performance for soldier protection and discover potential defeat mechanisms. Emphasis was placed on the fundamental understanding of the deformation and failure mechanisms, which enabled the design and development of robust materials to support Army core functions. Development of new materials was the focus with specific emphasis on fundamental knowledge of microstructural grain boundaries in diamond-SiC composites. Novel processing routes to selectively tailor the nano-mesoscale microstructure in heterogeneous ceramic armors were explored via conventional hot-pressing, reactive hot-pressing, and spark plasma sintering (SPS). Correlations between the nano-mesoscale hierarchical microstructure, deformation mechanisms, and mechanical response were explored using advanced characterization methods and small-scale mechanical testing. Higher fidelity mesoscale mechanics models were sought by using experimentally obtained microstructural information coupled with atomistic models of relevant grain boundary interfaces.
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