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Cooperative Development of Analytical Methods for Diesel Emissions and Particulates — Solvent Extractables, Aldehydes and Sulfate Methods
ISSN: 0148-7191, e-ISSN: 2688-3627
Published February 1, 1984 by SAE International in United States
Annotation ability available
The Chemical Characterization Panel of the Coordinating Research Council Air Pollution Research Advisory Committee (CRC-APRAC) In house 1-64 Project Group (CAPI 1-64) conducted an extensive study of analytical methods for measuring diesel exhaust emissions. This report details the procedures developed for three of the non-regulated emissions. The first method, solvent extraction of particulate filters, recommends soxhlet extraction with either methylene chloride or toluene-ethanol, depending on the end use of the extract fraction. The second method involves collection of gas phase aldehydes in an acetonitrile-2, 4-dinitrophenylhydrazine solution followed by HPLC-UV analysis. The third method utilizes ion chromatography for analysis of particulate sulfate content.
Round-robin testing by 18 Chemical Characterization Panel participants established precision and accuracy data that define the engineering applicability of the test methods.
CitationPerez, J., Lipari, F., Seizinger, D., and , ., "Cooperative Development of Analytical Methods for Diesel Emissions and Particulates — Solvent Extractables, Aldehydes and Sulfate Methods," SAE Technical Paper 840413, 1984, https://doi.org/10.4271/840413.
Diesel Exhaust Emissions-Particulate Studies and Transient Cycle Testing
Number: SP-0578; Published: 1984-08-01
Number: SP-0578; Published: 1984-08-01
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