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Internal Diesel Injector Deposit Chemical Speciation and Quantification Using 3D OrbiSIMS and XPS Depth Profiling

Journal Article
2020-01-2098
ISSN: 2641-9645, e-ISSN: 2641-9645
DOI: https://doi.org/10.4271/2020-01-2098
Published September 15, 2020 by SAE International in United States
Internal Diesel Injector Deposit Chemical Speciation and Quantification Using 3D OrbiSIMS and XPS Depth Profiling
Sector:
Citation: Lamb, J., Barker, J., Wilmot, E., Scurr, D. et al., "Internal Diesel Injector Deposit Chemical Speciation and Quantification Using 3D OrbiSIMS and XPS Depth Profiling," SAE Int. J. Adv. & Curr. Prac. in Mobility 3(1):349-364, 2021, https://doi.org/10.4271/2020-01-2098. Erratum published in SAE Int. J. Adv. & Curr. Prac. in Mobility 3(1):2021, https://doi.org/10.4271/2020-01-2098.1. Erratum published in SAE Int. J. Adv. & Curr. Prac. in Mobility 3(1):2021, https://doi.org/10.4271/2020-01-2098.1.
Language: English

References

  1. Reid , J. , and Barker , J. Understanding Polyisobutylene Succinimides (PIBSI) and Internal Diesel Injector Deposits SAE Technical Paper 2013-01-2682 2013 https://doi.org/10.4271/2013-01-2682
  2. Barker , J. , Snape , C. , and Scurr , D. Information on the Aromatic Structure of Internal Diesel Injector Deposits from Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS) SAE Technical Paper 2014-01-1387 2014 https://doi.org/10.4271/2014-01-1387
  3. Ullmann , J. , Geduldig , M. , Stutzenberger , H. , Caprotti , R. et al. Investigation into the Formation and Prevention of Internal Diesel Injector Deposits SAE Technical Paper 2008-01-0926 2008 https://doi.org/10.4271/2008-01-0926
  4. Barker , J. , Richards , P. , Goodwin , M. , and Wooler , J. Influence of High Injection Pressure on Diesel Fuel Stability: A Study of Resultant Deposits SAE Int. J. Fuels Lubr. 877– 884 2009 https://doi.org/10.4271/2009-01-1877
  5. Banning , M. , Barker , J. , and Mulqueen , S.
  6. Hoang , A.T. , and Le , A.T. A Review on Deposit Formation in the Injector of Diesel Engines Running on Biodiesel Energy Sources, Part A 584– 599 2019 10.1080/15567036.2018.1520342
  7. Alves Fortunato , M. , Lenglet , F. , Ben Amara , A. , and Starck , L. Are Internal Diesel Injector Deposits (IDID) Mainly Linked to Biofuel Chemical Composition or/and Engine Operation Condition? SAE Technical Paper 2019-01-0061 2019 https://doi.org/10.4271/2019-01-0061
  8. de Goede , S. , Barbour , R. , Velaers , A. , Sword , B. , et al. The Effect of Near-Zero Aromatic Fuels on Internal Diesel Injector Deposit Test Methods SAE Int. J. Fuels Lubr. 163 183 2017 https://doi.org/10.4271/2017-01-0807
  9. Edney , M.K. , Barker , J. , Reid , J. , Scurr , D.J. et al. Recent Advances in the Analysis of GDI and Diesel Fuel Injector Deposits Fuel 2020 10.1016/j.fuel.2020.117682
  10. Dallanegra , R. , and Caprotti , R. Chemical Composition of Ashless Polymeric Internal Diesel Injector Deposits SAE Technical Paper 2014-01-2728 2014 https://doi.org/10.4271/2014-01-2728
  11. Cardenas Almena , M.D. , Lucio Esperilla , O. , Martin Manzanero , F. , Murillo Duarte , Y. et al. Internal Diesel Injector Deposits: Sodium Carboxylates of C12 Succinic Acids and C16 and C18 Fatty Acids SAE Technical Paper 2012-01-1689 2012 https://doi.org/10.4271/2012-01-1689
  12. Barker , J. , Reid , J. , Smith , S.A. , Snape , C. 2017
  13. Venkataraman , R. , and Eser , S. Characterization of Deposits Formed on Diesel Injectors in Field Test and from Thermal Oxidative Degradation of n-hexadecane in a Laboratory Reactor Chem. Cent. J. 2008 10.1186/1752-153x-2-25
  14. Trobaugh , C. , Burbrink , C. , Zha , Y. , Whitacre , S. et al. Internal Diesel Injector Deposits: Theory and Investigations into Organic and Inorganic Based Deposits SAE Int. J. Fuels Lubr. 772 784 2013 https://doi.org/10.4271/2013-01-2670
  15. Barker , J. , Cook , S. , and Richards , P. Sodium Contamination of Diesel Fuel, Its Interaction with Fuel Additives and the Resultant Effects on Filter Plugging and Injector Fouling SAE Int. J. Fuels Lubr. 826– 838 2013 https://doi.org/10.4271/2013-01-2687
  16. Reid , J. , Cook , S. , and Barker , J. Internal Injector Deposits from Sodium Sources SAE Int. J. Fuels Lubr. 436 444 2014 https://doi.org/10.4271/2014-01-1388
  17. Barker , J. , Snape , C. , and Scurr , D. A Novel Technique for Investigating the Characteristics and History of Deposits Formed within High Pressure Fuel Injection Equipment SAE Int. J. Fuels Lubr. 1155 1164 2012 https://doi.org/10.4271/2012-01-1685
  18. Feld , H. , and Oberender , N. Characterization of Damaging Biodiesel Deposits and Biodiesel Samples by Infrared Spectroscopy (ATR-FTIR) and Mass Spectrometry (TOF-SIMS) SAE Int. J. Fuels Lubr. 717 724 2016 https://doi.org/10.4271/2016-01-9078
  19. Passarelli , M.K. , Pirkl , A. , Moellers , R. , Grinfeld , D. et al. The 3D OrbiSIMS-Label-Free Metabolic Imaging with Subcellular Lateral Resolution and High Mass-Resolving Power Nat. Methods 1175 1183 2017 10.1038/nmeth.4504
  20. Edney , M.K. , Lamb , J.S. , Spanu , M. , Smith , E.F. 10.26434/chemrxiv.12666470.v1
  21. www.XPSFitting.com
  22. Omori , T. , Tanaka , A. , Yamada , K. , and Bunne , S. Biodiesel Deposit Formation Mechanism and Improvement of Fuel Injection Equipment (FIE) SAE Technical Paper 2011-01-1935 2011 https://doi.org/10.4271/2011-01-1935
  23. 2013
  24. Lacey , P. , Gail , S. , Kientz , J.M. , Milovanovic , N. et al. Internal Fuel Injector Deposits SAE Int. J. Fuels Lubr. 132 145 2012 https://doi.org/10.4271/2011-01-1925
  25. da Cunha , A. , Sa , A. , Mello , S.C. , Vasquez-Castro , Y.E. , et al. Determination of Nitrogen-Containing Polycyclic Aromatic Compounds in Diesel and Gas Oil by Reverse-Phase High Performance Liquid Chromatography Using Introduction of Sample as Detergentless Microemulsion Fuel 119 129 2016 10.1016/j.fuel.2016.02.035
  26. Taylor , R.S. , and Garrison , B.J. Hydrogen Abstraction Reactions in the Kiloelectronvolt Particle Bombardment of Organic Films J. Am. Chem. Soc. 4465 4466 1994 10.1021/ja00089a041
  27. Batts , B. , and Fathoni , A.Z. A Literature Review on Fuel Stability Studies with Particular Emphasis on Diesel Oil Energy & Fuels 2 21 1991 10.1021/ef00025a001
  28. Giakoumis , E.G. , and Sarakatsanis , C.K. A Comparative Assessment of Biodiesel Cetane Number Predictive Correlations Based on Fatty Acid Composition Energies 2019 10.3390/en12030422
  29. 2016
  30. Binkley , R.W. , Flechtner , T.W. , Tevesz , M.J. , Winnik , W. et al. Rearrangement of Aromatic Sulfonate Anions in the Gas Phase Org. Mass Spectrom. 769– 772 1993 10.1002/oms.1210280708
  31. Stepien , Z. , and Krasodomski , W. Effect of Trace Zinc Amounts Introduced in Various Chemical Structures in Diesel Fuel on Coke Deposits of Fuel Injectors of a CI Engine Int. J. Engine Res. 755 765 2020 10.1177/1468087418777175
  32. Barbour , R.H. , Quigley , R. , and Panesar , A. Investigations into Fuel Additive Induced Power Gain in the CEC F-98-08 DW10B Injector Fouling Engine Test SAE Technical Paper Series 2014 https://doi.org/10.4271/2014-01-2721

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